Particle Size Analysis by Laser Diffraction Method Using Reference Particles

2012 ◽  
Vol 508 ◽  
pp. 33-37 ◽  
Author(s):  
Yasushige Mori ◽  
Hideto Yoshida ◽  
Hiroaki Masuda
Keyword(s):  
Particle Size ◽  
Size Distribution ◽  
Diffraction Method ◽  
Particle Size Analysis ◽  
Laser Diffraction ◽  
Round Robin ◽  
Size Analysis ◽  
Silica Sample ◽  
Round Robin Test ◽  
Em Method

The particle size analysis (PSA) by laser diffraction (LD) method can be used for monitor or control of particulate process, because it has the advantages of shorter measurement time and good repeatability, and a variety of commercial instruments is available. However particle size distribution (PSD) measured by LD method depends a great deal on not only optical detector configuration and calculation procedure but also on the system of sample loading into the measuring zone. From this fact, the validation of PSA by LD method should be done using reference particles (RP), whose size distribution is better to have a range over one decade of size, according to ISO 13320-1. For this purpose, the Association of Powder Process Industry and Engineering, Japan (APPIE) distribute the spherical barium titanate glass particles as RP of JIS Z 8900-1, whose size ranges are 1 - 10 µm (MBP 1 - 10), 3 - 30 µm (MBP 3 - 30) and 10 - 100 µm (MBP 10 - 100). This paper shows why LD method needs to check its performance by using RP, and then reports the results of the round robin test of two kinds of RP (MBP 1 - 10 and MBP 10 - 100) and silica RP candidate with 0.1 1.0 µm size measured by LD instruments, which was conducted by the Technical Group of Measurement and Control in APPIE. PSD results measured by LD instruments were almost same as each other for both RP samples. MBP 1 - 10 sample was well dispersed in water without detergent, but a few drops of detergent sometimes needed for dispersing MBP 10 - 100 sample. For MBP 1 - 10 sample, PSD by LD method was slightly smaller than that measured by scanning electro microscopy (SEM) or electro sensing zone (ESZ) methods. For MBP 10 - 100 sample, PSD by LD method agreed well with that by SEM or ESZ methods. Silica sample can be supplied to the users as the dry powder, which can be re-dispersed in water with small amount of surfactant. From the results of the round robin test using silica sample, PSD measured by LD method roughly agreed with EM method.

Size Reduction of Clay Particles in Nanometer Dimensions

2002 ◽  
Vol 740 ◽  
Author(s):  
Gopinath Mani ◽  
Qinguo Fan ◽  
Samuel C. Ugbolue ◽  
Isabelle M. Eiff
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Specific Surface ◽  
Size Distribution ◽  
Research Work ◽  
Particle Size Analysis ◽  
Laser Diffraction ◽  
Size Analysis ◽  
Clay Particles ◽  
Nano Size

ABSTRACTThis research work focuses on combining ball milling and ultrasonication to produce nano-size clay particles. Our work also emphasizes on increasing the specific surface area of montmorillonite clay particles by reducing the particle size to nanometer dimensions. We have characterized the as-received clay particles by using particle size analysis based on laser diffraction and found that the size of the clay particles is not consistent and the particle size distribution is very broad. However, after the unique treatment and processing, the clay particles were obtained in nanometer dimensions with narrowed particle size distribution.

How does pretreatment of dry steppe soils affect particle size analysis by laser diffraction?

2020 ◽  
Author(s):  
Moritz Koza ◽  
Aleksey Prays ◽  
Andrej Bondarovich ◽  
Kanat Akshalov ◽  
Christopher Conrad ◽  
...  
Keyword(s):  
Particle Size ◽  
Diffraction Method ◽  
Particle Size Analysis ◽  
Laser Diffraction ◽  
Size Analysis ◽  
Dry Steppe ◽  
Land Use Types ◽  
Wide Range ◽  
Binding Agents ◽  
Sample Dispersion

<p>After extensive research on different methods to measure<strong> particle size distribution</strong> (PSD), soil scientists are proposing the<strong> laser diffraction method</strong> (LDM) as a standard method for soil texture analysis. However, the effects of different pretreatments on particle size analysis of dry steppe soils with LDM has not been tested so far. This study aims to evaluate <strong>different pretreatment methods</strong> with the purpose to disperse aggregates and remove binding agents in <strong>Chernozem and Kastanozem</strong> soils. To cover a wide range of different land-use types and farming methods, 112 surface soil samples were taken from 13 fields on four different test sites in <strong>Kazakhstan</strong>. Before LDM analysis, all samples were pretreated with either H<sub>2</sub>O<sub>2</sub> to remove organic carbon or HCl to remove carbonates. The results showed that removing organic matter with H<sub>2</sub>O<sub>2</sub> led to complete sample dispersion while HCl pretreatment caused incomplete dispersion, likely due to aggregation by calcium ions released by the dissolution of carbonates.</p>

scholarly journals Particle Size Distribution of Various Soil Materials Measured by Laser Diffraction—The Problem of Reproducibility

Minerals ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 465
Author(s):  
Cezary Polakowski ◽  
Magdalena Ryżak ◽  
Agata Sochan ◽  
Michał Beczek ◽  
Rafał Mazur ◽  
...  
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Normal Distribution ◽  
Size Distribution ◽  
Precise Measurement ◽  
Soil Analysis ◽  
Statistical Tests ◽  
Diffraction Method ◽  
Laser Diffraction ◽  
Method Analysis

Particle size distribution is an important soil parameter—therefore precise measurement of this characteristic is essential. The application of the widely used laser diffraction method for soil analysis continues to be a subject of debate. The precision of this method, proven on homogeneous samples, has been implicitly extended to soil analyses, but this has not been sufficiently well confirmed in the literature thus far. The aim of this study is to supplement the information available on the precision of the method in terms of reproducibility of soil measurement and whether the reproducibility of soil measurement is characterized by a normal distribution. To estimate the reproducibility of the laser diffraction method, thirteen various soil samples were characterized, and results were analysed statistically. The coefficient of variation acquired was lowest (3.44%) for silt and highest for sand (23.28%). Five of the thirteen tested samples were characterized by a normal distribution. The fraction content of eight samples was not characterized by normal distribution, but the extent of this phenomenon varied between soils. Although the laser diffraction method is repeatable, the measurement of soil particle size distribution can have limited reproducibility. The main cause seems to be small amounts of sand particles. The error can be amplified by the construction of the dispersion unit. Non-parametric statistical tests should be used by default for soil laser diffraction method analysis.

X-ray fluorescence spectrometry for rapid screening of particle size in soils

2021 ◽  
Author(s):  
Maame Croffie ◽  
Paul N. Williams ◽  
Owen Fenton ◽  
Anna Fenelon ◽  
Karen Daly
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Soil Texture ◽  
Particle Size Analysis ◽  
Parent Material ◽  
Fluorescence Spectrometry ◽  
Rapid Screening ◽  
Size Analysis ◽  
X Ray

<p>Soil texture is an essential factor for effective land management in agricultural production. Knowledge of soil texture and particle size at field scale can aid with on-going soil management decisions. Standard soil physical and gravimetric methods for particle size analysis are time-consuming and X-ray fluorescence spectrometry (XRF) provides a rapid and cost-effective alternative. The objective of this study was to explore the use of XRF as a predictor for particle size. An extensive archive of Irish soils with particle size and soil texture data was used to select samples for XRF analysis. Regression and correlation analyses on XRF determined results showed that the relationship between Rb and % clay varied with soil type and was dependent on the parent material. There was a strong relationship (R > 0.62, R<sup>2</sup>>0.30, p<0.05) between Rb and clay for soils originating from bedrock such as limestones and slate. Contrastingly, no significant relationship (R<0.03, R<sup>2</sup>=0.00, p>0.05) exists between Rb and % clay for soils originating from granite and gneiss. Furthermore, there was a significant negative correlation (p<0.05) between Rb and % sand. The XRF is a useful technique for rough screening of particle size distribution in soils originating from certain parent materials. Thus, this may contribute to the rapid prediction of soil texture based on knowledge of the particle size distribution.</p><p> </p>

scholarly journals Application of Particle-Size Analysis Data for the Determination of Air/Cleaner Performance

1965 ◽  
Author(s):  
Lawrence J. Czerwonka ◽  
Jack M. Carey
Keyword(s):  
Particle Size ◽  
Size Distribution ◽  
Analysis Data ◽  
Particle Size Analysis ◽  
General Purpose ◽  
Size Analysis ◽  
Air Filter ◽  
Performance Curves ◽  
Air Cleaner

A general purpose centrifuge method for measuring particle-size distribution of air-filter inlet, outlet and catch dust samples is demonstrated. Treatment and analysis of data to determine air-cleaner performance based on size distribution is shown for two types of air filters, a louver and a glass-fiber media filter. The advantages and limitations of the method and interpretations of results associated with the application of these procedures for arriving at efficiency versus particle-size performance curves, and for predicting filter efficiency for any given dust are discussed.

scholarly journals Digital microscopic image application (DMIA), an automatic method for particle size distribution analysis in waste activated sludge

2021 ◽  
Author(s):  
S. Cazares ◽  
J. A. Barrios ◽  
C. Maya ◽  
G. Velásquez ◽  
M. Pérez ◽  
...  
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Activated Sludge ◽  
Size Distribution ◽  
Particle Diameter ◽  
Diffraction Method ◽  
Laser Diffraction ◽  
Waste Activated Sludge ◽  
Equivalent Diameter ◽  
Distribution Analysis

Abstract An important physical property in environmental samples is particle size distribution. Several processes exist to measure particle diameter, including change in electrical resistance, blocking of light, the fractionation of field flow and laser diffraction (these being the most commonly used). However, their use requires expensive and complex equipment. Therefore, a Digital Microscopic Imaging Application (DMIA) method was developed adapting the algorithms used in the Helminth Egg Automatic Detector (HEAD) software coupled with a Neural Network (NN) and Bayesian algorithms. This allowed the determination of particle size distribution in samples of waste activated sludge (WAS), recirculated sludge (RCS), and pretreated sludge (PTS). The recirculation and electro-oxidation pre-treatment processes showed an effect in increasing the degree of solubilization (DS), decreasing particle size and breakage factor with ranges between 44.29%, and 31.89%. Together with a final NN calibration process, it was possible to compare results. For example, the 90th percentile of Equivalent Diameter (ED) value obtained by the DMIA with the corresponding result for the laser diffraction method. DMIA values: 228.76 μm (WAS), 111.18 μm (RCS), and 84.45 μm (PTS). DMIA processing has advantages in terms of reducing complexity, cost and time, and offers an alternative to the laser diffraction method.

scholarly journals Adequacy of laser diffraction for soil particle size analysis

PLoS ONE ◽  
2017 ◽  
Vol 12 (5) ◽  
pp. e0176510 ◽  
Author(s):  
Peter Fisher ◽  
Colin Aumann ◽  
Kohleth Chia ◽  
Nick O'Halloran ◽  
Subhash Chandra
Keyword(s):  
Particle Size ◽  
Particle Size Analysis ◽  
Laser Diffraction ◽  
Soil Particle ◽  
Size Analysis ◽  
Soil Particle Size

scholarly journals Application of laser diffraction method for determination

2008 ◽  
Vol 53 (No. 1) ◽  
pp. 34-38 ◽  
Author(s):  
M. Ryzak ◽  
A. Bieganowski ◽  
R.T. Walczak
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Podzolic Soil ◽  
Diffraction Method ◽  
Laser Diffraction ◽  
Soil Material ◽  
New Methods ◽  
Particle Size Distribution Measurement ◽  
Straight Lines

Particle size distribution affects many physical soil properties and processes taking place in soil. There are many methods to determine the particle size distribution. The most frequently used are the sieve, sieve-pipette and sedimentation methods. Technological progress in electronics permitted a wide use of new methods of particle size distribution measurement in soil, e.g. the laser diffraction method. A comparison of particle size distribution obtained with the universally used areometer method (Cassagrande, modified by Prószynski) with results from the laser diffraction method for soil material received from grey-brown podzolic soil is presented in this work. The largest differences between the results were obtained for the smallest fraction determined with the areometer and laser diffraction methods. In a majority of other cases the slopes of interpolated straight lines were contained within the range of 0.81 ÷ 1.09.

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