Brazing Vacuum Ceramic Tubes - A Diffusion Profile in the Joint

The Sirius Project is an initiative of the Brazilian Synchrotron Light Laboratory - LNLS (CNPEM - MCTI), for the design, construction and operation of a new synchrotron radiation source 3rd generation, with high brightness and energy of the electrons of 3.0 GeV. Among many other components there will be built 80 ceramic cameras embedded in special magnets, whose function is to act to correct the orbit of the electron beam in the storage ring. The ceramic chamber is crucial for this application because this material is transparent to the magnetic field generated in the electro magnet and thus acts directly on the electron beam. The difficulty of these constructive components lies in the fact that, the ceramic components must be attached to metal components will join vacuum chambers that make up the ring, and then must present excellent mechanical and vacuum tight. The process of chemical bonding between the ceramic and metal components is performed by brazing in high vacuum. After brazing, a film is deposited of copper with 7 micrometers thickness. The objective of this paper is to describe the process of film deposition and brazing of copper and the excellent results obtained in the production, mechanical characterization, microstructural and tightness.

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Advanced electron beam source for ultrahigh vacuum (molecular beam epitaxy) and high vacuum applications of thin film deposition

Journal of Vacuum Science & Technology A Vacuum Surfaces and Films ◽

10.1116/1.579026 ◽

1994 ◽

Vol 12 (4) ◽

pp. 1628-1630 ◽

Cited By ~ 1

Author(s):

J. W. Moore ◽

N. K. Tsujimoto

Keyword(s):

Thin Film ◽

Electron Beam ◽

Molecular Beam Epitaxy ◽

Molecular Beam ◽

High Vacuum ◽

Ultrahigh Vacuum ◽

Thin Film Deposition ◽

Film Deposition ◽

Beam Source

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Girder integration NSLS-II

Diamond Light Source Proceedings ◽

10.1017/s2044820111000219 ◽

2011 ◽

Vol 1 (MEDSI-6) ◽

Author(s):

L. Doom ◽

M. Anerella ◽

T. Dilgen ◽

R. Edwards ◽

R. Faussete ◽

...

Keyword(s):

Synchrotron Radiation ◽

Light Source ◽

Storage Ring ◽

Third Generation ◽

National Synchrotron Light Source ◽

High Brightness ◽

Vacuum Chambers ◽

Synchrotron Light ◽

Low Emittance ◽

Ancillary Equipment

National Synchrotron Light Source II (NSLS-II) will be a 3-GeV 792 m circumference third generation synchrotron radiation facility with ultra low emittance and extremely high brightness. There will be a total of 90 multipole storage ring girders supporting the vacuum chambers, multipole magnets and various pieces of ancillary equipment. A major effort is being made to meet the stringent assembly and alignment requirements for the girder assemblies using relatively few and removable positioning fixtures. Girder assembly and alignment will be accomplished in four phases. Each of these phases will be described along with the fixtures required.

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Materials for Electron Beam Information Storage

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100062671 ◽

1969 ◽

Vol 27 ◽

pp. 152-153 ◽

Cited By ~ 1

Author(s):

D. E. Speliotis

Keyword(s):

Magnetic Field ◽

Electron Beam ◽

Recent Literature ◽

Electron Beams ◽

Information Storage ◽

The Subject ◽

The Magnetic Field

The interaction of electron beams with a large variety of materials for information storage has been the subject of numerous proposals and studies in the recent literature. The materials range from photographic to thermoplastic and magnetic, and the interactions with the electron beam for writing and reading the information utilize the energy, or the current, or even the magnetic field associated with the electron beam.

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A theory of contamination in electron microscopes by surface diffusion

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100107721 ◽

1978 ◽

Vol 36 (1) ◽

pp. 116-117

Author(s):

J.T. Fourie

Keyword(s):

Electron Beam ◽

Surface Diffusion ◽

High Vacuum ◽

Ultra High Vacuum ◽

Physical Parameters ◽

Carbon Compounds ◽

Hydrocarbon Molecules ◽

Electron Microscopes ◽

Primary Electrons ◽

Long Chain

Contamination in electron microscopes can be a serious problem in STEM or in situations where a number of high resolution micrographs are required of the same area in TEM. In modern instruments the environment around the specimen can be made free of the hydrocarbon molecules, which are responsible for contamination, by means of either ultra-high vacuum or cryo-pumping techniques. However, these techniques are not effective against hydrocarbon molecules adsorbed on the specimen surface before or during its introduction into the microscope. The present paper is concerned with a theory of how certain physical parameters can influence the surface diffusion of these adsorbed molecules into the electron beam where they are deposited in the form of long chain carbon compounds by interaction with the primary electrons.

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Performance and applications of the holography electron microscope

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100151222 ◽

1993 ◽

Vol 51 ◽

pp. 1078-1079

Author(s):

Akira Tonomura

Keyword(s):

Electron Beam ◽

Electron Microscope ◽

Phase Measurement ◽

Electron Holography ◽

Imaging Method ◽

High Contrast ◽

Magnetic Lens ◽

High Brightness ◽

Holographic Imaging ◽

Dynamic Observation

Electron holography is a two-step imaging method. However, the ultimate performance of holographic imaging is mainly determined by the brightness of the electron beam used in the hologram-formation process. In our 350kV holography electron microscope (see Fig. 1), the decrease in the inherently high brightness of field-emitted electrons is minimized by superposing a magnetic lens in the gun, for a resulting value of 2 × 109 A/cm2 sr. This high brightness has lead to the following distinguished features. The minimum spacing (d) of carrier fringes is d = 0.09 Å, thus allowing a reconstructed image with a resolution, at least in principle, as high as 3d=0.3 Å. The precision in phase measurement can be as high as 2π/100, since the position of fringes can be known precisely from a high-contrast hologram formed under highly collimated illumination. Dynamic observation becomes possible because the current density is high.

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Point-Cathode Electron Gun Using Electron-Beam Bombardment for Cathode Tip Heating

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100179749 ◽

1990 ◽

Vol 48 (1) ◽

pp. 198-199

Author(s):

Ryo Iiyoshi ◽

Susumu Maruse ◽

Hideo Takematsu

Keyword(s):

Electron Beam ◽

Tungsten Wire ◽

Local Heating ◽

Electron Gun ◽

Original Position ◽

Beam Power ◽

Radius Of Curvature ◽

High Brightness ◽

Beam Focusing ◽

Time Operation

Point cathode electron gun with high brightness and long cathode life has been developed. In this gun, a straightened tungsten wire is used as the point cathode, and the tip is locally heated to higher temperatures by electron beam bombardment. The high brightness operation and some findings on the local heating are presented.Gun construction is shown in Fig.l. Small heater assembly (annular electron gun: 5 keV, 1 mA) is set inside the Wehnelt electrode. The heater provides a disk-shaped bombarding electron beam focusing onto the cathode tip. The cathode is the tungsten wire of 0.1 mm in diameter. The tip temperature is raised to the melting point (3,650 K) at the beam power of 5 W, without any serious problem of secondary electrons for the gun operation. Figure 2 shows the cathode after a long time operation at high temperatures, or high brightnesses. Evaporation occurs at the tip, and the tip part retains a conical shape. The cathode can be used for a long period of time. The tip apex keeps the radius of curvature of 0.4 μm at 3,000 K and 0.3 μm at 3,200 K. The gun provides the stable beam up to the brightness of 6.4×106 A/cm2sr (3,150 K) at the accelerating voltage of 50 kV. At 3.4×l06 A/cm2sr (3,040 K), the tip recedes at a slow rate (26 μm/h), so that the effect can be offset by adjusting the Wehnelt bias voltage. The tip temperature is decreased as the tip moves out from the original position, but it can be kept at constant by increasing the bombarding beam power. This way of operation is possible for 10 h. A stepwise movement of the cathode is enough for the subsequent operation. Higher brightness operations with the rapid receding rates of the tip may be improved by a continuous movement of the wire cathode during the operations. Figure 3 shows the relation between the beam brightness, the tip receding rate by evaporation (αis the half-angle of the tip cone), and the cathode life per unit length, as a function of the cathode temperature. The working life of the point cathode is greatly improved by the local heating.

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