Mechanical Properties of Bulk Glassy Metal after Deformation under High Temperature Conditions

2007 ◽  
Vol 340-341 ◽  
pp. 113-118
Author(s):  
Takamasa Yoshikawa ◽  
Masataka Tokuda ◽  
Tadashi Inaba

Bulk glassy metal is an alloy with the vitreous amorphous structure. Because of various excellent properties, this material is expected to use as an alternative structural material for several engineering applications very well. Although bulk glassy metal is very little deformed plastically in the room temperature, it shows the huge super-plastic behavior over the high temperature. However, there is not many reports mentioned about the mechanical properties of bulk glassy metal after plastic deformation under high temperature condition. From the above point of view, in this study, we have investigated the lower bound of temperature at which Zr55Cu30Al10Ni5 bulk glassy metal can be plastically deformed in uniaxial tensile load. Furthermore, it is focused on the strength property of bulk glassy metal in the room temperature after deformed under various high-temperature conditions. In the experimental result, when this material was heated at temperature of 685[K] or higher, this material crystallized and the mechanical strength in room temperature drastically decreased to 200[MPa], although this material as cast had the strength over 1500[MPa]. However, this material showed sufficiently the plastic deformation at temperatures of 643[K] and the strength in room temperature after cooling was equal to as cast. It is supposed that the strength depend on its atomic structure, i.e., amorphous or crystalline, and the change of its structure is affected strongly by heating process.

2021 ◽  
Author(s):  
Wenqi Liu ◽  
Zinan Li ◽  
Sven Bossuyt ◽  
Antti Forsström ◽  
Zaiqing Que ◽  
...  

Metals made by additive manufacturing (AM) have intensely augmented over the past decade for customizing complex structured products in the aerospace industry, automotive, and biomedical engineering. However, for AM fabricated steels, the correlation between the microstructure and mechanical properties is yet a challenging task with limited reports. To realize optimization and material design during the AM process, it is imperative to understand the influence of the microstructural features on the mechanical properties of AM fabricated steels. In the present study, three material blocks with 120×25×15 mm3 dimensions are produced from PH1 steel powder using powder bed fusion (PBF) technology to investigate the anisotropic plastic deformation behavior arising from the manufacturing process. Despite being identical in geometrical shape, the manufactured blocks are designed distinguishingly with various coordinate transformations, i.e. alternating the orientation of the block in the building direction (z) and the substrate plate (x, y). Uniaxial tensile tests are performed along the length direction of each specimen to characterize the anisotropic plastic deformation behavior. The distinctly anisotropic plasticity behavior in terms of strength and ductility are observed in the AM PH1 steel, which is explained by their varied microstructure affected by the thermal history of blocks. It could also be revealed that the thermal history in the AM blocks is influenced by the block geometry even though the same process parameters are employed.


2020 ◽  
Vol 34 (3) ◽  
pp. 8-17
Author(s):  
Su-Gil Choi ◽  
Yeong-Jae Nam ◽  
Se-Young Jin ◽  
Si-Kuk Kim

In this study, the characteristics of HFIX insulated wire sheaths contaminated by pollutants were examined. KS C IEC 60811-1-3 standard was followed in performing the water-resistance wire tests. Pollutants were selected, and the specimens were exposed to the pollutants for a maximum duration of four weeks. The maximum tensile load and the elongation rate were measured each week. As the period of pollution exposure increased, the maximum tensile load of the specimens decreased by 6.22% and 6.52% at room temperature and high temperature, respectively, and 19.94% for specimens coated with a rust-proof lubricant. The elongation rate also decreased rapidly, such that the reductions in the properties of the sheath were significant. From the analysis of the surfaces using a scanning microscope, as the contamination period increased, structural changes such as perforation, split, and melting occurred, and the mechanical properties of the specimens decreased. Therefore, it is necessary to develop and follow an inspection cycle and periodically carry out repairs to prevent the deterioration of insulated wires.


Materials ◽  
2021 ◽  
Vol 14 (15) ◽  
pp. 4339
Author(s):  
Guanqiang Wang ◽  
Mingsong Chen ◽  
Yongcheng Lin ◽  
Yumin Lou ◽  
Hongbin Li ◽  
...  

This study takes large size samples after hot-upsetting as research objects and aims to investigate the optimization double-stage annealing parameters for improving the mechanical properties of hot-upsetting samples. The double-stage annealing treatments and uniaxial tensile tests for hot-upsetting GH4169 superalloy were finished firstly. Then, the fracture mode was also studied. The results show that the strength of hot-upsetting GH4169 superalloy can be improved by the double-stage annealing treatment, but the effect of annealing parameters on the elongation of GH4169 alloy at high temperature and room temperature is not significant. The fracture mode of annealed samples at high-temperature and room-temperature tensile tests is a mixture of shear fracture and quasi-cleavage fracture while that of hot-upsetting sample is a shear fracture. The macroscopic expressions for the two fracture modes belong to ductile fracture. Moreover, it is also found that the improvement of strength by the double-stage annealing treatment is greater than the single-stage annealing treatment. This is because the homogeneity of grains plays an important role in the improvement of strength for GH4169 superalloy when the average grain size is similar. Based on a comprehensive consideration, the optimal annealing route is determined as 900 °C × 9–12 h(water cooling) + 980 °C × 60 min(water cooling).


2015 ◽  
Vol 830-831 ◽  
pp. 191-194
Author(s):  
M. Venkateswara Rao

Conventional tensile test methods are used for service exposed high temperature boiler tubes to evaluate the deterioration in mechanical properties such as tensile strength, yield strength and percentage elongation. The mechanical properties are required to be evaluated periodically as the boiler components undergo material degradation due to aging phenomena. The aging phenomena occurs due to continuous exposure of tubes to high temperature & pressure steam prevailing inside the tubes and high temperature exposure to corrosive combustible gases from the external surfaces within the boiler.A recent developed new technique called small punch testing has been used to evaluate the tensile properties of SA 213T22 grade steel predominantly exists in super-heater and re-heater sections of boiler. The small punch tests have been carried out on the miniature disk shaped specimens of diameter of 8.0 mm and 0.5 mm thickness extracted from both the new and service exposed tubes. Conventional uniaxial tensile tests on standard specimens from the same tube material have also been performed for comparison. The service exposed tubes showed considerable loss in mechanical properties in both the conventional and small punch test results. Correlations of tensile properties have been obtained based on the comparative analysis of both small punch and uniaxial tensile test results. Further, the study showed that an appropriate empirical relation could be generated for new and service exposed materials between both the techniques. Conventional test methods require large quantity of material removal for test samples from in-service components whereas small punch test method needs only a miniature sample extraction. This small punch test technique could also be extended to evaluate the thicker section boiler components such as pipelines and headers in the boiler as a part of remaining life assessment study. Also this technique could be a useful tool to any metallic component where large quantity of sample removal may be difficult or may not be feasible.


Author(s):  
Georg Frommeyer ◽  
Sven Knippscheer

Aluminum-rich intermetallic compounds of the Al3X-type with transmission metals (X = Ti. Zr, Nb, V) of Groups IVb and Vb are of interest in the development of novel high-temperature and lightweight structural materials. This article describes the important physical and mechanical properties of trialuminides with DO22 structure and their L12 variations. Topical coverage includes: crystal structure and selected physical properties, plastic deformation, oxidation behavior, and applications.


Author(s):  
Pradeep Lall ◽  
Vikas Yadav ◽  
Jeff Suhling ◽  
David Locker

Electronics in automotive underhood and downhole drilling applications may be subjected to sustained operation at high temperature in addition to high strain-rate loads. SAC solders used for second level interconnects have been shown to experience degradation in high strain-rate mechanical properties under sustained exposure to high temperatures. Industry search for solutions for resisting the high-temperature degradation of SAC solders has focused on the addition of dopants to the alloy. In this study, a doped SAC solder called SAC-Q solder have been studied. The high strain rate mechanical properties of SAC-Q solder have been studied under elevated temperatures up to 200°C. Samples with thermal aging at 50°C for up to 6-months have been used for measurements in uniaxial tensile tests. Measurements for SAC-Q have been compared to SAC105 and SAC305 for identical test conditions and sample geometry. Data from the SAC-Q measurements has been fit to the Anand Viscoplasticity model. In order to assess the predictive power of the model, the computed Anand parameters have been used to simulate the uniaxial tensile test and the model predictions compared with experimental data. Model predictions show good correlation with experimental measurements. The presented approach extends the Anand Model to include thermal aging effects.


2019 ◽  
Vol 2 (2) ◽  
pp. 126-136
Author(s):  
M.I Retno Susilorini ◽  
Budi Eko Afrianto ◽  
Ary Suryo Wibowo

Concrete building safety of fire is better than other building materials such as wood, plastic, and steel,because it is incombustible and emitting no toxic fumes during high temperature exposure. However,the deterioration of concrete because of high temperature exposure will reduce the concrete strength.Mechanical properties such as compressive strength and modulus of elasticity are absolutely corruptedduring and after the heating process. This paper aims to investigate mechanical properties of concrete(especially compressive strength and modulus of elasticity) with various water-cement ratio afterconcrete suffered by high temperature exposure of 500oC.This research conducted experimental method and analytical method. The experimental methodproduced concrete specimens with specifications: (1) specimen’s dimension is 150 mm x 300 mmconcrete cylinder; (2) compressive strength design, f’c = 22.5 MPa; (3) water-cement ratio variation =0.4, 0.5, and 0.6. All specimens are cured in water for 28 days. Some specimens were heated for 1hour with high temperature of 500oC in huge furnace, and the others that become specimen-controlwere unheated. All specimens, heated and unheated, were evaluated by compressive test.Experimental data was analyzed to get compressive strength and modulus of elasticity values. Theanalytical method aims to calculate modulus of elasticity of concrete from some codes and to verifythe experimental results. The modulus elasticity of concrete is calculated by 3 expressions: (1) SNI03-2847-1992 (which is the same as ACI 318-99 section 8.5.1), (2) ACI 318-95 section 8.5.1, and (3)CEB-FIP Model Code 1990 Section 2.1.4.2.The experimental and analytical results found that: (1) The unheated specimens with water-cementratio of 0.4 have the greatest value of compressive strength, while the unheated specimens with watercementratio of 0.5 gets the greatest value of modulus of elasticity. The greatest value of compressivestrength of heated specimens provided by specimens with water-cement ratio of 0.5, while the heatedspecimens with water-cement ratio of 0.4 gets the greatest value of modulus of elasticity, (2) Allheated specimens lose their strength at high temperature of 500oC, (3) The analytical result shows thatmodulus of elasticity calculated by expression III has greater values compares to expression I and II,but there is only little difference value among those expressions, and (4)The variation of water-cementratio of 0.5 becomes the optimum value.


Crystals ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1330
Author(s):  
Muhammad Farzik Ijaz ◽  
Mahmoud S. Soliman ◽  
Ahmed S. Alasmari ◽  
Adel T. Abbas ◽  
Faraz Hussain Hashmi

Unfolding the structure–property linkages between the mechanical performance and microstructural characteristics could be an attractive pathway to develop new single- and polycrystalline Al-based alloys to achieve ambitious high strength and fuel economy goals. A lot of polycrystalline as-cast Al-Cu-Mg-Ag alloy systems fabricated by conventional casting techniques have been reported to date. However, no one has reported a comparison of mechanical and microstructural properties that simultaneously incorporates the effects of both alloy chemistry and mechanical testing environments for the as-cast Al-Cu-Mg-Ag alloy systems. This preliminary prospective paper presents the examined experimental results of two alloys (denoted Alloy 1 and Alloy 2), with constant Cu content of ~3 wt.%, Cu/Mg ratios of 12.60 and 6.30, and a constant Ag of 0.65 wt.%, and correlates the synergistic comparison of mechanical properties at room and elevated temperatures. According to experimental results, the effect of the precipitation state and the mechanical properties showed strong dependence on the composition and testing environments for peak-aged, heat-treated specimens. In the room-temperature mechanical testing scenario, the higher Cu/Mg ratio alloy with Mg content of 0.23 wt.% (Alloy 1) possessed higher ultimate tensile strength when compared to the low Cu/Mg ratio with Mg content of 0.47 wt.% (Alloy 2). From phase constitution analysis, it is inferred that the increase in strength for Alloy 1 under room-temperature tensile testing is mainly ascribable to the small grain size and fine and uniform distribution of θ precipitates, which provided a barrier to slip by deaccelerating the dislocation movement in the room-temperature environment. Meanwhile, Alloy 2 showed significantly less degradation of mechanical strength under high-temperature tensile testing. Indeed, in most cases, low Cu/Mg ratios had a strong influence on the copious precipitation of thermally stable omega phase, which is known to be a major strengthening phase at elevated temperatures in the Al-Cu-Mg-Ag alloying system. Consequently, it is rationally suggested that in the high-temperature testing scenario, the improvement in mechanical and/or thermal stability in the case of the Alloy 2 specimen was mainly due to its compositional design.


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