Formability of Ti–29Nb–13Ta–4.6Zr Biomaterial at High Temperatures

2010 ◽  
Vol 443 ◽  
pp. 620-625
Author(s):  
Ming Jen Tan ◽  
Syed Fida Hassan ◽  
Toshikazu Akahori ◽  
Mitsuo Niinomi

Ti-29Nb-13Ta-4.6Zr has been recently developed as a biomaterial showing most potential. The study here was conducted to investigate the high temperature deformation behavior under uniaxial tensile stress at various temperatures (i.e., 700°C, 800°C and 900°C) with different initial strain rates at atmospheric condition. Results of the high temperature tensile tests show a significant improved elongation-to-failure of this novel biomaterial at elevated temperatures compared to open literature, and hence its formability potential.

1995 ◽  
Vol 10 (1) ◽  
pp. 113-118 ◽  
Author(s):  
S.E. Dougherty ◽  
T.G. Nieh ◽  
J. Wadsworth ◽  
Y. Akimune

The high-temperature deformation behavior of a SiC whisker-reinforced, yttria-stabilized, tetragonal zirconia polycrystalline composite containing 20 vol % SiC whiskers (SiC/Y-TZP) has been investigated. Tensile tests were performed in vacuum at temperatures from 1450 °C to 1650 °C and at strain rates from 10−3 to 10−5 s−1. The material exhibits useful high-temperature engineering properties (e.g., ∼100 MPa and 16% elongation at T = 1550 °C and at a strain rate of ∼10−4 s−1). The stress exponent was determined to be n ≍ 2. Scanning electron microscopy was used to characterize the grain size and morphology of the composites, both before and after deformation. The grain size in the composite was initially fine, but coarsened at the test temperatures; both dynamic and static grain growth were observed. The morphology of ceramic reinforcements appears to affect strongly the plastic deformation properties of Y-TZP. A comparison is made between the properties of monolithic Y-TZP, 20 wt. % Al2O3 particulate-reinforced Y-TZP (Al2O3/Y-TZP), and SiC/Y-TZP composites.


2007 ◽  
Vol 551-552 ◽  
pp. 373-378 ◽  
Author(s):  
X.J. Zhu ◽  
Ming Jen Tan ◽  
K.M. Liew

In this work, studies were carried out to investigate the superplasticity of a commercially pure (CP) titanium alloy during high temperature deformation. Uniaxial tensile tests were carried out at 600, 750 and 800°C with an initial strain rate from 10-1s-1 to 10-4s-1. It was found that the alloy do not show good superplasticity due fast grain growth at high temperature and cavity. The effects of temperature on the grain growth and cavity phenomena as well as the dynamic recrystallization of the alloy were studied and a ‘two-step-method’ was introduced to increase the superplasticity of the alloy.


Metals ◽  
2019 ◽  
Vol 9 (2) ◽  
pp. 123 ◽  
Author(s):  
Zhubin He ◽  
Zhibiao Wang ◽  
Peng Lin

In order to thoroughly understand the quantitative relationships between the flow stress and deformation conditions for Ti2AlNb-based alloys at elevated temperatures, the Arrhenius and Johnson–Cook constitutive models are analyzed and identified on the basis of the uniaxial tensile tests. The Johnson–Cook model is modified so that the referenced temperature range can be randomly adjusted. By experimental verification, the Arrhenius model (including the Backofen model) is suitable for the deformation at relatively low strain-rate deformation, such as the superplastic forming, and the modified J–C model is applicable for the deformation within a wide range of strain rates. For deformation at high temperatures, the constitutive model enables a more precise description of the effect of strain on the flow stress through introducing as train-softening factor exp(sε).


2004 ◽  
Vol 449-452 ◽  
pp. 57-60
Author(s):  
I.G. Lee ◽  
A.K. Ghosh

In order to analyze high temperature deformation behavior of NiAl alloys, deformation maps were constructed for stoichiometric NiAl materials with grain sizes of 4 and 200 µm. Relevant constitute equations and calculation method will be described in this paper. These maps are particularly useful in identifying the location of testing domains, such as creep and tensile tests, in relation to the stress-temperature-strain rate domains experienced by NiAl.


2007 ◽  
Vol 539-543 ◽  
pp. 3678-3683
Author(s):  
Ming Jen Tan ◽  
X.J. Zhu ◽  
S. Thiruvarudchelvan ◽  
K.M. Liew

This work reports the influence of oxidation on the superplasticity of commercially pure titanium at high temperatures. Uniaxial tensile tests were conducted at temperatures in the range 600-800°C with an initial strain rate of 10s-1 to 10s-3. This study shows that oxidization at the surface of the alloy causes oxide film on the surface of commercially pure titanium alloy, and the thickness of oxide film increase with increasing exposure time and temperature. XRD analysis shows that the oxide film consists of TiO2. Because this oxide film is very brittle, it can induce clefts and degrade the ductility of the titanium at high temperatures. The mechanism of the initial clefts was investigated and a model for the cleft initiation and propagation during high temperature tensile test was proposed.


2020 ◽  
Vol 306 ◽  
pp. 53-61
Author(s):  
Sergey V. Astafurov ◽  
Galina G. Maier ◽  
Eugene V. Melnikov ◽  
Valentina A. Moskvina ◽  
Marina Yu. Panchenko ◽  
...  

The paper is devoted to an experimental investigation of a high-temperature deformation in V-alloyed high-nitrogen austenitic Fe-19Cr-22Mn-1.5V-0.3C-0.6N steel processed via different thermo-mechanical treatments. Simple thermo-mechanical processing regimes (cold rolling or rolling with single post-deformation anneal) do not allow to realize a substantial elongation in high-nitrogen steel during high-temperature tensile tests. For fine-grained austenitic structure with an average grain size of 3 µm, the maximal value of elongation to failure of 150% was realized at temperature 950 °C. Using a multi-stage thermo-mechanical treatment included cold rolling and intermediate anneals, a heterophase grain/subgrain structure with high density of deformation-induced defects and precipitates was produced. When heated to a deformation temperature, this deformation-assisted microstructure recrystallizes into a stable fine-grained structure and demonstrates the attributes of superplastic flow (values of elongation to failure higher than 400%) in the temperature range of 850-1000 °C. The maximum elongation of 900% is achieved at temperature of 950 °C and an initial strain rate of 10-4 s-1.


2014 ◽  
Vol 622-623 ◽  
pp. 508-513
Author(s):  
Yong Nam Kwon ◽  
S.S. Hong ◽  
H.G. Kim

Superplastic forming has been known for the ideal process for manufacturing complex parts. Also, diffusion bonding can give a higher design flexibility, which allows a better performance with a lower overall manufacturing cost. Fine grained INCONEL 718 alloy sheet has been known to show superplastic behavior with the combination of high strength and corrosion resistance at the elevated temperatures. In the present study, high temperature deformation characteristic of INCONEL 718 sheet with 15m was investigated firstly. Then, blow forming process with cylindrical cavity was tried. Also, best diffusion brazing and bonding condition was tried to be defined in terms of temperature, pressure and time. Bonding strength was characterized by using lap shear type test and interface observation. Characteristics of deformation and diffusion bonding at high temperature were influenced greatly with grain size while Nb precipitate also played an important role.


2012 ◽  
Vol 182-183 ◽  
pp. 189-193
Author(s):  
Ting Qu Li ◽  
M. Gao ◽  
S.H. Wang ◽  
Zhan Yi Cao

In this paper, the high temperature tensile properties of the LAZ532-2RE alloy prepared by hot extruded processing after vacuum casting was investaged. The tensile properties of the extruded LAZ532-2RE alloy specimens were tested at different temperature with different strain rate. The microstructures near the fractured surfaces were observed using microscope in order to investigate the dominant deformation mechanism. The activation energy was calculated to explain the high temperature deformation mechanism. The result indicated that the strength of LAZ532-2RE alloy was high at the temperature range from 398K to 423K. Meanwhile, the fracture elongation of the alloy reaches 121% at 523K under strain rate 1×10-3s-1.


2007 ◽  
Vol 551-552 ◽  
pp. 55-60 ◽  
Author(s):  
Yoshimasa Takayama ◽  
Y. Otsuka ◽  
Toshiya Shibayanagi ◽  
Hajime Kato ◽  
Kunio Funami

Grain refinement and high temperature deformation in two kinds of magnesium alloys subjected to friction stir processing (FSP) have been investigated. One was a rolled sheet of LA141Mg and another was a cast plate of AZ91Mg. FSP was developed by adapting the concepts of friction stir welding to obtain a fine grain size in a stirred zone. Grain refinement was achieved by FSP to give fine grain sizes of 11.4μm and 8.4μm for LA141 and AZ91 alloys, respectively. For LA141 alloy, the maximum stress of the FSPed sample was higher than that of the as-received one in the range of 300K to 523K while the elongation to failure of the former was considerably smaller than that of the latter. On the other hand, the elongation for the FSPed sample of AZ91Mg showed three times larger elongation with a lower maximum stress than the as-received cast one at 523K and 2.8×10-3s-1. Further difference in high temperature deformation for both magnesium alloys was discussed based on microstructural change and stress-strain curves.


2007 ◽  
Vol 340-341 ◽  
pp. 107-112 ◽  
Author(s):  
Hiroyuki Watanabe ◽  
Koichi Ishikawa ◽  
Toshiji Mukai

High temperature deformation behavior of AZ31 and AZ91 magnesium alloys was examined by compression tests over a wide strain rate range from 10–3 to 103 s–1 with emphasis on the behavior at high strain rates. The dominant deformation mechanism in the low strain rate range below 10–1 s–1 was suggested to be climb-controlled dislocation creep. On the other hand, experimental results indicated that the deformation at a high strain rate of ~103 s–1 proceeds by conventional plastic flow of dislocation glide and twinning even at elevated temperatures. The solid-solution strengthening was operative for high temperature deformation at ~103 s–1.


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