Study on Physical and Mechanical Properties of Cu/MoS2 Composites

2013 ◽  
Vol 575-576 ◽  
pp. 156-159
Author(s):  
Dou Qin Ma ◽  
Jing Pei Xie ◽  
Ji Wen Li ◽  
Ai Qin Wang ◽  
Wen Yan Wang ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Diffraction Analysis ◽  
Electric Conductivity ◽  
Hot Pressing ◽  
Physical And Mechanical Properties ◽  
Micro Hardness ◽  
X Ray Diffraction ◽  
X Ray ◽  
Vacuum Hot Pressing

Cu-3wt. %MoS2-7wt. %Mo and Cu-3wt. %MoS2 composites were prepared by repressing, re-sintering and vacuum hot pressing, respectively. Microstructures were characterized by optical metallographic microscope, EDS, SEM and X-ray diffraction analysis, respectively. The micro hardness, electric conductivity and density of samples were separately measured as well. Results show that the micro hardness of Cu-3wt. % MoS2-7wt. % Mo composites is about 33.3% higher than that of Cu-3wt. %MoS2 composites. The increase in micro hardness is attributed to the presence of Mo. The electric conductivity of Cu-3wt. %MoS2 and Cu-3wt. %MoS2-7wt. % Mo prepared by vacuum hot pressing were 80.6 % and 63.8% IACS, respectively, which is an increase compared with values of 80.2 % and 57.3% IACS of samples obtained by repressing and re-sintering.

Effects of NiO Nanoparticles on Physical and Mechanical Properties of BNKT Lead-Free Ceramics

2017 ◽  
Vol 866 ◽  
pp. 282-286 ◽  
Author(s):  
Chatchai Kruea-In ◽  
Suchittra Inthong ◽  
Wilaiwan Leenakul
Keyword(s):  
Mechanical Properties ◽  
Physical And Mechanical Properties ◽  
Micro Hardness ◽  
Nio Nanoparticles ◽  
X Ray Diffraction ◽  
Solid State Reaction Technique ◽  
X Ray ◽  
Hardness Tester ◽  
Lead Free Ceramics ◽  
Vickers Micro Hardness

In this research, The effects of NiO nanoparticles on the physical and mechanical properties of Bi0.5(Na0.81,K0.19)0.5TiO3 (BNKT) were investigated. The ceramics were synthesized by solid state reaction technique. The powder of BNKT was calcined at 850 °C for 4 h. The ceramics of BNKT/x NiO vol.% ( i.e. x= 0.0, 1.0, 2.0 and 3.0) were sintered at 1000-1150 °C for 2 h for optimize condition. Densification, phase formation, microstructure and micro hardness of samples were characterized via Archimedes method, X-ray diffraction techniques (XRD), scanning electron microscope (SEM) and Vickers micro hardness tester. The X-ray diffraction analysis of the ceramics suggests that all samples exhibited a perovskite structure. Densification of samples tended to increase with increasing amount of NiO content with minimun at 1.0 vol.% NiO additive. The NiO additive influenced densification as well as the mechanical properties of the samples. The results of this research suggest that NiO nanoparticles have influence on physical and mechanical properties of BNKT ceramics.

Physical and Mechanical Properties of Cement Paste Were Used Partially with Fly Ash and Kaolin Waste

2017 ◽  
Vol 866 ◽  
pp. 199-203
Author(s):  
Chidchanok Chainej ◽  
Suparut Narksitipan ◽  
Nittaya Jaitanong
Keyword(s):  
Mechanical Properties ◽  
Fly Ash ◽  
Room Temperature ◽  
Physical And Mechanical Properties ◽  
Partial Replacement ◽  
X Ray Diffraction ◽  
X Ray ◽  
Lime Water ◽  
Diffraction Patterns ◽  
Iron Mold

The aims of this research were study the microstructures and mechanical properties for partial replacement of cement with Fly ash (FA) and kaolin waste (KW). Ordinary Portland cement were partially replaced with FA and KW in the range of 25-35% and 10-25% by weight of cement powder. The kaolin waste was ground for 180 minutes before using. The specimen was packing into an iron mold which sample size of 5×5×5 cm3. Then, the specimens were kept at room temperature for 24 hours and were moist cured in the incubation lime water bath at age of 3 days. After that the specimens were dry cured with plastic wrap at age of 3, 7, 14 and 28 days. After that the compounds were examined by x-ray diffraction patterns (XRD) and the microstructures were examined by scanning electron microscopy (SEM). The compressive strength was then investigated.

scholarly journals Features of the hydration process of the modified blended cement for fiber cement panels

2018 ◽  
Vol 170 ◽  
pp. 03030 ◽  
Author(s):  
Rustem Mukhametrakhimov ◽  
Liliya Lukmanova
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Blended Cement ◽  
Physical And Mechanical Properties ◽  
Hydration Process ◽  
Cement Matrix ◽  
X Ray Diffraction ◽  
Structure Form ◽  
Silicate Phase ◽  
X Ray

The paper studies features of the hydration process of the modified blended cement for fiber cement panels (FCP) using differential thermal analysis, X-ray diffraction analysis, electron microscopy and infrared spectroscopy. It is found that deeper hydration process in silicate phase, denser and finer crystalline structure form in fiber cement matrix based on the modified blended cement. Generalization of this result to the case of fiber cement panels makes it possible to achieve formation of a denser and homogeneous structure with increased physical and mechanical properties.

Influence of Aging Treatments on the Structural and Mechanical Properties of AGS Alloy Wire Cold Drawn

2018 ◽  
Vol 18 ◽  
pp. 73-78
Author(s):  
Mokhtar Bayarassou ◽  
Mosbah Zidani ◽  
Hichem Farh
Keyword(s):  
Mechanical Properties ◽  
Plastic Deformation ◽  
Electron Microscope ◽  
Artificial Ageing ◽  
Micro Hardness ◽  
X Ray Diffraction ◽  
Alloy Wire ◽  
X Ray ◽  
Plastic Deformation Rate ◽  
Scanning Electron

The scope of this work is to study of microstructural changes and mechanical properties during natural and artificial ageing treatment of AGS Alloy wire cold drawn with different deformation at ENICAB in Biskra. And as well to know the phase formation during different deformation of aluminum alloys wires. as well as the combined influence of the plastic deformation rate and the aging temperature. Wire section reduction shows a change in microstructure and texture. The methods of characterization used in this work are: scanning electron microscope and X-ray diffraction, micro hardness (Hv).

Contribution of the hybrid component to the structure and properties of ceramics based on metastable phases Al2O3

2021 ◽  
pp. 127-136
Author(s):  
A. V. Maletsky ◽  
T. E. Konstantinova ◽  
D. R. Belichko ◽  
G. K. Volkova ◽  
V. V. Burkhovetsky
Keyword(s):  
Mechanical Properties ◽  
Yttrium Aluminum Garnet ◽  
Metastable Phase ◽  
Physical And Mechanical Properties ◽  
Structure And Properties ◽  
X Ray Diffraction ◽  
Mutual Inhibition ◽  
X Ray ◽  
Tetragonal Lattice ◽  
Yttrium Aluminum

The paper presents results of the study of the effect of doping with yttrium oxide on ceramics of the composition (γ + θ) Al2O3 + nY2O3 (n = 0, 1, 2, 3 wt%), sintered at 1550°C for 2 h, from powders of the specified composition annealed at temperatures of 500 , 800, 1000°С. X-ray diffraction analysis established the formation in ceramics of yttrium aluminum garnet Y3Al5O12 (YAG) and a metastable phase of the same composition with a tetragonal lattice type in powders at temperatures above 1200°C. The effect of YAG on the physical and mechanical properties was established: high properties were demonstrated by ceramics of the composition α-Al2O3 + 2wt% Y2O3, obtained from a powder annealed at 1000°C. In addition, high physical and mechanical properties were observed in ceramics of the composition α-Al2O3 + 0wt% Y2O3, obtained from a powder annealed at 800°C. The effect of the so-called “mutual protection against crystallization” was discovered, which consists in the mutual inhibition of crystallization processes in powders of the Al2O3 – Y2O3 system.

Microstructure and Mechanical Properties of Fe-Cu-Ni Sinters Prepared by Ball Milling and Hot Pressing

2020 ◽  
Vol 405 ◽  
pp. 379-384
Author(s):  
Joanna Borowiecka-Jamrozek ◽  
Jan Lachowski
Keyword(s):  
Mechanical Properties ◽  
Hot Pressing ◽  
High Hardness ◽  
X Ray Diffraction ◽  
X Ray ◽  
Powder Composition ◽  
Microstructure And Mechanical Properties ◽  
Static Tensile ◽  
Iron Based ◽  
Surface Observations

The main purpose of this work was to determine the effect of the powder composition on the microstructure and properties of iron-based sinters used as a matrix in diamond tools. The Fe-Cu-Ni sinters obtained from a mixture of ground powders were used for experiments. The influence of manufacturing process parameters on the microstructure and mechanical properties of sinters was investigated. Sintering was performed using hot-pressing technique in a graphite mould. The investigations of obtained sinters included: density, hardness, static tensile test, X-ray diffraction analysis, microstructure and fracture surface observations. The obtained results indicate that the produced sinters have good plasticity and relatively high hardness.

Physical and Mechanical Properties of Bi0.5(Na0.81K0.19)0.5TiO3 Ceramic Modified by KNbO3

2019 ◽  
Vol 805 ◽  
pp. 71-75
Author(s):  
Suchittra Inthong ◽  
Chatchai Kruae-In ◽  
Wuttikrai Thanomsiang ◽  
Suppanat Kosolwattana ◽  
Denis Russell Sweatman ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Mixed Oxides ◽  
Perovskite Phase ◽  
Physical And Mechanical Properties ◽  
X Ray Diffraction ◽  
Solid State Reaction Technique ◽  
X Ray ◽  
Ceramic Samples ◽  
Pure Phase ◽  
Knoop Microhardness

This research reports the physical and mechanical properties of (1-x) Bi0.5(Na0.81K0.19)0.5TiO3-xKNbO3 (x=0.00-0.06) ceramics. The Modified Bi0.5(Na0.81K0.19)0.5TiO3 ceramics were synthesized by solid state reaction technique. The mixed oxides powders were calcined at 850 °C, 4 h and sintered at 1120 °C, 2 h to form pure phase perovskite and the optimum bulk density, respectively. The phase formation of the modified ceramic samples was determined by X-ray diffraction technique. All of the modified Bi0.5(Na0.81K0.19)0.5TiO3 ceramics exhibited a single perovskite phase. The bulk densities of the modified ceramic samples were 5.41±0.27-5.75±0.28 g/cm3 using the Archimedes’ method. The microstructure was revealed by the scanning electron microscope. The rectangular-like shape was found of all studied ceramics which had the grain size between 1.31±0.02-1.56±0.03 mm. The mechanical properties were studied by both Vickers and Knoop microhardness tester. The results are discussed in term of the relation among hardness properties, Young’s modulus, and fracture toughness.

Fabrication and Mechanical Properties of SiC/Cu Composites with Zn Addition by Hot Pressing Sintering

2013 ◽  
Vol 745-746 ◽  
pp. 700-705
Author(s):  
Huang Liu ◽  
Guo Qiang Luo ◽  
Pin Gan Chen ◽  
Qiang Shen ◽  
Lian Meng Zhang
Keyword(s):  
Mechanical Properties ◽  
Vickers Hardness ◽  
Hot Pressing ◽  
Bending Strength ◽  
Coefficient Of Thermal Expansion ◽  
High Volume ◽  
X Ray Diffraction ◽  
X Ray ◽  
Zn Addition ◽  
Hot Pressing Sintering

SiC/Cu composites exhibit low density, low coefficient of thermal expansion and excellent mechanical properties. In this study, Zn of 2 wt. % was added as the sintering activator, and the high volume faction (60%) SiC/Cu composites was fabricated by hot pressing sintering technology. The phase composition and morphology of as-prepare samples were characterized by X-ray diffraction (XRD) system and scanning electron microscopy (SEM) equipped with an energy-dispersive spectroscopy (EDS) system. The as-prepared SiC/Cu composites were dense and uniform as well as void free. The results show that SiC/Cu composites can reach excellent mechanical properties of SiC/Cu composites. With the increase of sintering temperature, Vickers hardness and the bending strength of the samples increased obviously and the as-prepared SiC/Cu composites achieved a maximum Vickers hardness and bending strength respectively of 195MPa and 140MPa.

SYNERGISTIC REINFORCEMENT OF ORGANOCLAY AND DOUBLE NETWORKING IN NATURAL RUBBER

2013 ◽  
Vol 86 (2) ◽  
pp. 205-217 ◽  
Author(s):  
Hedayatollah Sadeghi Ghari ◽  
Zahra Shakouri
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Natural Rubber ◽  
Physical And Mechanical Properties ◽  
X Ray Diffraction ◽  
Double Network ◽  
X Ray ◽  
Extension Ratio ◽  
Curing Characteristics ◽  
Scanning Electron

ABSTRACT Research was undertaken on natural rubber (NR) nanocomposites with organoclays. A double-network (DN) structure is formed when a partially cross-linked elastomer is further cross-linked during a state of strain. Two methods were used in the preparation of NR/organoclay nanocomposites: the ordinary method (single-network NR nanocomposite) and double-networked NR (DN-NR) nanocomposites. The single-networked NR nanocomposites were used for comparison. The effects of organoclay (5 phr) with a different extension ratio on curing characteristics, mechanical properties, hardness, swelling behavior, and morphology of single- and double-networked NR nanocomposites were studied. The results showed that double-networked NR nanocomposites exhibited higher physical and mechanical properties. The tensile strength of DN-NR nanocomposites increased up to 33 MPa (more than four times greater than that of pure NR) and then decreased with an increasing extension ratio. Modulus and hardness continuously increased with an increased extension ratio. The microstructure of the NR/organoclay systems was studied by X-ray diffraction and field emission scanning electron microscopy. The effects of different extension ratios on the dispersion of organoclay layers in the nanocomposites were investigated. Generally, results showed that the optimized extension ratio in DN nanocomposites was equal (or about or around) to α= 2.

scholarly journals Investigation of deformation and microstructure of bainite in Cu-9.97%Al-4.62%mn alloy

2014 ◽  
Vol 50 (1) ◽  
pp. 87-90 ◽  
Author(s):  
E. Aldirmaz ◽  
I. Aksoy
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Physical And Mechanical Properties ◽  
Compression Stress ◽  
X Ray Diffraction ◽  
Deformation Effect ◽  
X Ray ◽  
Deformation Test ◽  
Scanning Electron

In this study, some physical and mechanical properties in Cu-9.97%Al-4.62%Mn (wt%) alloy were investigated by X-ray diffraction (XRD), Scanning Electron Microscopy (SEM) and compression deformation test. Bainite phase were obtained in the samples according to SEM and XRD analyses. Compression stress was applied on the alloy in order to investigate the deformation effect on the bainite phase transformation. On the surface of the Cu-9.97%Al-4.62%Mn alloy after the deformation, both bainite and martensite variants formed.

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