Effect of Holding Time on Microstructure and Mechanical Properties of Diffusion-Bonded Mg1/Pure Ag Foil/1060Al Joints

2014 ◽  
Vol 616 ◽  
pp. 280-285 ◽  
Author(s):  
Yi Yu Wang ◽  
Qiang Guo Luo ◽  
Qiang Shen ◽  
Chuan Bin Wang ◽  
Lian Meng Zhang

Mg1 and 1060 Al were diffusion-bonded by using pure silver foil under different holding times (10 min~120 min). The interface of the joint consists of Mg-Ag diffusion zone, Ag foil interlayer and Ag-Al diffusion zone. The distributions of Mg, Ag and Al show ladder-like distributions at the interface of the joints. When the holding time is below 90 min, silver foil has impeded the inter-diffusion of Mg and Al. When the holding time is beyond 90 min, the brittle eutectic Mg-Al intermetallic compounds (IMCs) cannot be avoided. Mg3Ag and MgAg intermetallic compounds formed on Mg base side. Ag2Al intermetallic compound grew on Al base side. The thicknesses of Mg3Ag, MgAg and Ag2Al increased linearly with the increasing holding time, which is contrary to that of the silver foil. The growth rate relationship of the formed IMCs is MgAg > Ag2Al > Mg3Ag according the slope values of the fitted lines. The hardness sharply increased at the interface because of the formation of IMCs. The maximum hardness values of three IMCs Mg3Ag, MgAg and Ag2Al are 287.5 HV, 196.5 HV and 175.7 HV respectively. The hardness of each IMC layer increased with the extension of holding time. The shear strength of the joints decreased from 10.5 MPa to 4.6 MPa with the rising holding time.

2011 ◽  
Vol 239-242 ◽  
pp. 2976-2980 ◽  
Author(s):  
Ying Hui Zhang ◽  
Jing Qin ◽  
Hong Jin Zhao ◽  
Gao Lei Xu

The interfacial microstructure evolution of copper/aluminium laminates with different annealing processes was studied. It was found that the formation and growth of intermetallic compounds in the interface during metallurgical combination process have four stages: the incubation period, the formation of island-like new phases in local areas, the transverse-lengthwise-transverse growth of diffusion zone, the formation of new intermetallic compounds and thickening of diffusion zone.


2020 ◽  
Vol 34 (33) ◽  
pp. 2050385
Author(s):  
Ye Wang ◽  
Maoliang Hu ◽  
Hongyu Xu ◽  
Zesheng Ji ◽  
Xuefeng Wen ◽  
...  

A typical Al–Cu–Mn–Ti aluminum alloy chip was adopted to prepare semi-solid billets by a Strain-Induced Melt Activation (SIMA) method, and the effects of isothermal process parameters on the semi-solid microstructure evolution of the alloy were investigated in this work. The result showed that semi-solid billets with highly spheroidal and homogeneous fine grains could be prepared from chips by the SIMA method. With the increase of isothermal temperature, the finer and near-spherical grains are obtained, the grains coarsen and became ellipse at 903 K because of the coarsening mechanisms of coalescence and Ostwald ripening. The relationship of isothermal holding time and grains size followed the LSW theory well, and more spherical microstructure can be brought by prolonging the holding time until 3000 s. Thus, the optimal isothermal treatment temperature is 893 K and holding time is 3000 s, the corresponding average size and roundness of grains are 137 [Formula: see text]m and 1.108, respectively.


Materials ◽  
2019 ◽  
Vol 12 (12) ◽  
pp. 1967
Author(s):  
Qiong Wan ◽  
Fuguo Li ◽  
Wenjing Wang ◽  
Junhua Hou ◽  
Wanyue Cui ◽  
...  

In this study, ball-milled powder of Ti and Al was used to fabricate Ti–Al intermetallic compound-reinforced Al matrix composites by an in-situ reaction in cold-pressing sintering and hot-pressing sintering processes. The detailed microstructure of the Ti–Al intermetallic compound-reinforced Al composite was characterized by optical microscopy (OM), X-ray diffraction (XRD), energy dispersive spectrometry (EDS), and electron backscattered diffraction (EBSD). The results indicate that a typical core–shell-like structure forms in the reinforced particles. The shell is composed of a series of Ti–Al intermetallic compounds and has good bonding strength and compatibility with the Al matrix and Ti core. With cold-pressing sintering, the shell around the Ti core is closed, and the shell thickness increases as the milling time and holding time increase. With hot-pressing sintering, some radiating cracks emerge in the shell structure and provide paths for further diffusion of Ti and Al atoms. The Kirkendall effect, which is caused by the difference between the diffusion coefficients of Ti and Al, results in the formation of cavities and a reduction in density degree. When the quantity of the intermetallic compounds increases, the hardness of the composites increases and the plasticity decreases. Therefore, factors that affect the quantity of the reinforcements, such as the milling time and holding time, should be determined carefully to improve the comprehensive properties of the composites.


2002 ◽  
Vol 73 (2-3) ◽  
pp. 197-201 ◽  
Author(s):  
Carmen Pin ◽  
Gonzalo D Garcı́a de Fernando ◽  
Juan A Ordóñez ◽  
József Baranyi

2016 ◽  
Vol 673 ◽  
pp. 107-115
Author(s):  
W. Rahman ◽  
J.B. Shamsul ◽  
M.N. Mazlee

In this study, the effect of holding time on the microwave sintered 84Fe-11Cr-5Al2O3 metal matrix composite (MMC) was investigated. Sintering was carried out in a tubular microwave furnace HAMiLab-V3 under N2 atmosphere. The holding time was selected between 0 to 75 minutes with increment of 15 minutes respectively. A study of microstructure and physical properties was carried out on sintered samples. It was discovered that, when the samples sintered at 1400oC with 20oC/min heating rate, the hardness was significantly increased from 110Hv to 160 Hv for holding time ranging from 30 to 45oC/min. Further increment until 75 minutes of holding time, no significant changes were obtained and hardness values were at steady state. The enhancement of bulk density and reduction of porosity were observed commences at 30 minutes until 45 minutes holding time. However, the results showed that the optimum holding time was at 45 minutes where the micro hardness is at the highest point which is about 160Hv.


2018 ◽  
Vol 2 (2) ◽  
Author(s):  
Sri Widodo ◽  
Kun Suharno ◽  
Hasyim Tri Gustomo ◽  
Fuad Hilmy

Now, many of piston ring parts have been on the market. The products are often encountered are the 5MX-E160-10 series piston ring and the SLW-E1603-20 series piston ring which have different qualities. In this study, the hardness of the two piston ring products was analyzed by heat treatment. The heat holding time was varied 15 minutes, 30 minutes and 45 minutes at 8000C and the quenching media of SAE 40 oil. The results of the hardness of the 5MX-E160-10 series raw material were 105.97 HRB and the highest hardness value after treatment decreased 34.02% were 71.95 HRB. While the hardness value of the SLW-E160-20 series raw material were 90.26 HRB and after the heat treatment has decreased by 19%, were 71.26 HRB. The best microstructure test results were found at the 30 minute holding time series 5MX-E160-10 with a temperature of 8000C and the quenching media of SAE 40 oil. In addition, the results showed that the longer holding time in the SLW-E1603-20 series resulted in decreased hardness values.


Sign in / Sign up

Export Citation Format

Share Document