Grain Refinement and Hardening Induced by Heavy Deformation Using Low Energy High Current Pulsed Electron Beam Surface Treatment

2010 ◽  
Vol 667-669 ◽  
pp. 499-504 ◽  
Author(s):  
Thierry Grosdidier ◽  
Y. Samih ◽  
Nathalie Allain-Bonasso ◽  
Bernard Bolle ◽  
Z.X. Zou ◽  
...  
Keyword(s):  
Grain Size ◽  
Electron Beam ◽  
Pulse Electron Beam ◽  
Low Energy ◽  
Temperature Fields ◽  
Material Surface ◽  
High Current ◽  
Pulsed Electron Beam ◽  
Size Refinement ◽  
Texture Modification

The low energy high current pulse electron beam (LEHCPEB) irradiation induces ultra fast dynamic temperature fields in the surface of the material to which is associated dynamic stress fields that causes intense deformation at the material surface and sub-surface. Improved surface properties (hardness, corrosion resistance) can be obtained using the LEHCPEB treatment. Under the “Melting” mode, the top surface (few µm) which is melted and rapidly solidified (107 K/s), can solidify has nano-domains formed from the highly under-cooled melt. The thermal stress wave that propagates in the sub-surface imposes strain hardening and grain size refinement. This induces a sub-surface hardening that can extent over about 100 µm. The use of the “Heating” mode is less conventional. This mode can promote grain size refinement, hardening as well as texture modification without modification of the sample geometry.

scholarly journals Preparation and Electron-Beam Surface Modification of Novel TiNi Material for Medical Applications

2021 ◽  
Vol 11 (10) ◽  
pp. 4372
Author(s):  
Sergey G. Anikeev ◽  
Anastasiia V. Shabalina ◽  
Sergei A. Kulinich ◽  
Nadezhda V. Artyukhova ◽  
Daria R. Korsakova ◽  
...  
Keyword(s):  
Electron Beam ◽  
Material Surface ◽  
High Current ◽  
New Materials ◽  
New Approach ◽  
Pulsed Electron Beam ◽  
Beam Surface ◽  
Compositional Changes ◽  
Unmodified Sample ◽  
Mcf 7

A new approach to fabricate TiNi surfaces combining the advantages of both monolithic and porous materials for implants is used in this work. New materials were obtained by depositing a porous TiNi powder onto monolithic TiNi plates followed by sintering at 1200 °C. Then, further modification of the material surface with a high-current-pulsed electron beam (HCPEB) was carried out. Three materials obtained (one after sintering and two after subsequent beam treatment by 30 pulses with different pulse energy) were studied by XRD, SEM, EDX, surface profilometry, and by means of electrochemical measurements, including OCP and EIS. Structural and compositional changes caused by HCPEB treatment were investigated. Surface properties of the samples during their storage in saline for 10 days were studied and a model experiment with cell growth (MCF-7) was carried out for the unmodified sample with an electron beam to detect cell appearance on different surface locations.

scholarly journals Preparation and Electron-Beam Surface Modification of Novel TiNi Material for Medical Applications

2021 ◽  
Author(s):  
Sergey G. Anikeev ◽  
Anastasiia V. Shabalina ◽  
Sergei A. Kulinich ◽  
Nadezhda V. Artyukhova ◽  
Darya R. Korsakova ◽  
...  
Keyword(s):  
Electron Beam ◽  
Model Experiment ◽  
Material Surface ◽  
High Current ◽  
New Materials ◽  
New Approach ◽  
Pulsed Electron Beam ◽  
Beam Surface ◽  
Compositional Changes ◽  
Mcf 7

A new approach to fabricate TiNi surfaces combining the advantages of both monolithic and porous materials for implants is used in this work. New materials were obtained by depositing a porous TiNi powder onto monolithic TiNi plates followed by sintering at 1200°C. Then, further modification of the material surface with a high-current-pulsed electron beam (HCPEB) was carried out. Three materials obtained (one after sintering and two after subsequent beam treatment by 20 and 30 pulses, respectively) were studied by XRD, SEM, EDX, EIS methods, profilometry and OCP measurements. Structural and compositional changes caused by HCPEB treatment were investigated. Surface properties of the samples during their storage in saline for 10 days were studied and a model experiment with cell growth (MCF-7) was carried out for the sample unmodified with electron beam to detect cell appearance on different surface locations.

Microstructure, Texture and Residual Stresses Induced by Surface Thermo-Mechanical Treatments

2011 ◽  
Vol 675-677 ◽  
pp. 9-14
Author(s):  
Thierry Grosdidier ◽  
Bernard Bolle ◽  
J.D. Puerta Velásquez ◽  
J.X. Zou ◽  
Jean-Jacques Fundenberger ◽  
...  
Keyword(s):  
Electron Beam ◽  
Residual Stresses ◽  
High Speed ◽  
Processing Parameters ◽  
Low Energy ◽  
Difficult Case ◽  
High Speed Machining ◽  
High Current ◽  
Pulsed Electron Beam ◽  
Ti Alloys

This paper reviews some recent results concerning surface integrity of materials processed with two important developing techniques: high speed machining (HSM) – here applied to the difficult case of Ti alloys – and low energy high current pulsed electron beam (LEHCPEB) surface treatment of steels. The effect of the processing parameters on the development of microstructure, texture and residual stresses is detailed for modifications occurring both at the surfaces and sub-surfaces.

Low Energy High Current Pulsed Electron Beam (LEHCPEB) Treatment: An Effective Way for Improving Surface Microstructure and Properties

2010 ◽  
Vol 636-637 ◽  
pp. 1091-1096
Author(s):  
Thierry Grosdidier ◽  
Jian Xin Zou ◽  
K.M. Zhang ◽  
Sheng Zhi Hao ◽  
Chuang Dong
Keyword(s):  
Electron Beam ◽  
Surface Modifications ◽  
Metastable Phases ◽  
Low Energy ◽  
Surface Microstructure ◽  
High Current ◽  
Present Contribution ◽  
Corrosion Properties ◽  
Pulsed Electron Beam ◽  
Wear And Corrosion

Low energy high current pulsed electron beam (LEHCPEB) is a fairly new technique for surface modifications, including hardening, alloying and formation of metastable phases as well as improvement in wear and corrosion properties. The present contribution gives some new insights on the microstructure modifications encountered at the top surface of HCPEB treated metals. In particular, the potential of the technique for structure modifications associated with the use of the pulsed electron beam under “heating” and “melting” conditions are highlighted.

scholarly journals Surface modification of structural materials by low-energy high-current pulsed electron beam treatment

2014 ◽  
Author(s):  
A. V. Panin ◽  
M. S. Kazachenok ◽  
O. M. Borodovitsina ◽  
E. A. Sinyakova ◽  
Yu. F. Ivanov ◽  
...  
Keyword(s):  
Surface Modification ◽  
Electron Beam ◽  
Structural Materials ◽  
Low Energy ◽  
Electron Beam Treatment ◽  
High Current ◽  
Pulsed Electron Beam
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