Grain Refinement Mechanisms Oterative during Equal Channel Angular Pressing of Aluminium

2011 ◽  
Vol 702-703 ◽  
pp. 135-138
Author(s):  
Rampada Manna ◽  
N.K. Mukhopadhyay ◽  
G.V.S. Sastry

Grain refinement of aluminum deformed by equal channel angular pressing is strongly dependent on the amount of strain. The refinement process at low to high strain level involves elongation of the existing grains by shear deformation, their subdivision into bands and subgrain formation within bands, intersection of the bands during subsequent passes and finally conversion of the subgrains to grains by continuous dynamic recrystallization process. At room temperature the conversion of subgrains to grains takes place by progressive lattice rotation.

2014 ◽  
Vol 783-786 ◽  
pp. 2641-2646 ◽  
Author(s):  
Rustam Kaibyshev ◽  
Sergey Malopheyev ◽  
Vladislav Kulitskiy ◽  
Marat Gazizov

The mechanism of grain refinement in an Al-5.4Mg-0.4Mn-0.2Sc-0.09Zr alloy subjected to equal-channel angular pressing (ECAP) at 300°C through route BC is considered. It was shown that the formation of geometrically necessary boundaries (GNB) aligned with a {111} plane at ε≤1 initiates the occurrence of continuous dynamic recrystallization (CDRX). Upon further strain the GNBs transform to low-to-moderate angle planar boundaries that produces lamellar structure. In the strain interval 2-4, 3D arrays of planar boundaries evolve due to inducing the formation of 2nd order and higher orders families of GNBs in new {111} planes. GNBs gradually convert to high-angle boundaries (HAB) with strain. A uniform recrystallized structure is produced at a true strain of ∼8. The role of slip concentration and shearing patterns in the formation of GNBs is discussed.


2011 ◽  
Vol 409 ◽  
pp. 41-46
Author(s):  
Marat Gazizov ◽  
Rustam Kaibyshev

A novel Al-Cu-Mg-Ag alloy with small additions of zirconium and scandium was subjected to equal channel angular pressing (ECAP) by using route BC at 300°C to strains ranging from ~1 to ~12. Initially, the alloy was subjected to solution treatment followed by water quenching; subsequent overageing was carried out at 380°C for 3 h. It was shown that continuous dynamic recrystallization (CDRX) occurs during ECAP resulting in partially recrystallized structure; at a total strain of ~12, the portion of high-angle boundaries (HAB) attains 50 pct., average misorientation is ~25°. Crystallites having elongated shape and an average size of ~1 μm are evolved after a total strain of ~12.


2014 ◽  
Vol 794-796 ◽  
pp. 784-789 ◽  
Author(s):  
Rustam Kaibyshev ◽  
Sergey Malopheyev

Mechanisms of dynamic recrystallization operating at severe plastic deformation in a wide temperature range are reviewed for aluminum alloys. The main mechanism of grain refinement in all aluminum alloys is continuous dynamic recrystallization (CDRX). Temperature, deformation process and distribution of secondary phases strongly affect the CDRX mechanism. Initial formation of geometrically necessary boundaries (GNBs) and a dispersion of nanoscale particles accelerate CDRX facilitating the formation of a 3D network of low-angle boundaries (LAB) followed by their gradual transformation to high-angle boundaries (HAB). At high and intermediate temperatures, 3D networks of LABs may evolve due to rearrangement of lattice dislocations by climb, and mutual intersection of GNB, respectively. At high temperatures, in aluminum alloys containing no nanoscale dispersoids the CDRX occurs through the impingement of initial boundaries forced by deformation-induced LABs. This recrystallization process is termed as geometric dynamic recrystallization (GDRX). At low temperatures, the extensive grain refinement occurs through a continuous reaction which is distinguished from CDRX by restricted rearrangement of lattice dislocation. Introduction of large misorientation may occur through the formation of 3D networks of GNBs, only.


2010 ◽  
Vol 667-669 ◽  
pp. 583-588
Author(s):  
Mehdi Shaban Ghazani ◽  
Beitallah Eghbali

In the present research, a combined forward extrusion-equal channel angular pressing (FE-ECAP) was developed and used for production of bulk ultrafine grained steel in the high temperature conditions. In this method, two different deformation steps including forward extrusion and equal channel angular pressing takes place successively in a single die. The deformation process was performed at different deformation start temperatures (800, 930, and 1100 °C). In addition, 3D finite element simulation was used to predict the hot/warm deformation parameters such as strain and temperature variations within the samples during deformation. The results show that the EF-ECAP process is effective in refining the grains from initial size of 32 m to final size of 0.9 m after executing of extrusion and ECAP on as received samples. The main mechanisms of grain refinement were considered to be strain assisted transformation, dynamic strain-induced transformation, and continuous dynamic recrystallization.


2005 ◽  
Vol 488-489 ◽  
pp. 177-180
Author(s):  
T. Liu ◽  
Yan Dong Wang ◽  
Shi Ding Wu ◽  
Shou Xin Li ◽  
Ru Lin Peng ◽  
...  

The room temperature tensile strength and ductility of Mg-3.3%Li alloy were improved simultaneously by two kinds of different equal channel angular pressing (ECAP) treatments. Microstructural analyses showed that grain refinement and texture modification are the principal reasons for the improvement of mechanical properties.


Author(s):  
Anna Morozova ◽  
Elijah Borodin ◽  
Vladimir Bratov ◽  
Sergey Zherebtsov ◽  
Andrey Belyakov ◽  
...  

The microstructure evolution and grain refinement kinetics of a solution treated Cu – 0.1Cr – 0.06Zr alloy during equal channel angular pressing (ECAP) at a temperature of 673 K via route BC were investigated. The microstructure change during plastic deformation was accompanied by the microband formation and an increase in the misorienations of strain-induced subboundaries. The refinement of initial coarse grains was considered as a result of continuous dynamic recrystallization. The dynamic recrystallization kinetics was discussed in terms of grain/subgrain boundary triple junction evolution. The strain dependence of the triple junctions of high-angle boundaries can be expressed by a modified Johnson-Mehl-Avrami-Kolmogorov relationship with a strain exponent of about 1.49. Severe plastic deformation by ECAP led to substantial strengthening of the Cu-0.1Cr-0.06Zr alloy. The yield strength increased from 60 MPa in the initial state to 445 MPa after the total strain of 12.


Metals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 607
Author(s):  
A. I. Alateyah ◽  
Mohamed M. Z. Ahmed ◽  
Yasser Zedan ◽  
H. Abd El-Hafez ◽  
Majed O. Alawad ◽  
...  

The current study presents a detailed investigation for the equal channel angular pressing of pure copper through two regimes. The first was equal channel angular pressing (ECAP) processing at room temperature and the second was ECAP processing at 200 °C for up to 4-passes of route Bc. The grain structure and texture was investigated using electron back scattering diffraction (EBSD) across the whole sample cross-section and also the hardness and the tensile properties. The microstructure obtained after 1-pass at room temperature revealed finer equiaxed grains of about 3.89 µm down to submicrons with a high density of twin compared to the starting material. Additionally, a notable increase in the low angle grain boundaries (LAGBs) density was observed. This microstructure was found to be homogenous through the sample cross section. Further straining up to 2-passes showed a significant reduction of the average grain size to 2.97 µm with observable heterogeneous distribution of grains size. On the other hand, increasing the strain up to 4-passes enhanced the homogeneity of grain size distribution. The texture after 4-passes resembled the simple shear texture with about 7 times random. Conducting the ECAP processing at 200 °C resulted in a severely deformed microstructure with the highest fraction of submicron grains and high density of substructures was also observed. ECAP processing through 4-passes at room temperature experienced a significant increase in both hardness and tensile strength up to 180% and 124%, respectively.


2007 ◽  
Vol 539-543 ◽  
pp. 2904-2909 ◽  
Author(s):  
Vàclav Sklenička ◽  
Jiří Dvořák ◽  
Marie Kvapilová ◽  
Milan Svoboda ◽  
Petr Král ◽  
...  

This paper examines the effect of equal-channel angular pressing (ECAP) on creep behaviour of pure aluminium, binary Al-0.2wt.%Sc alloy and ternary Al-3wt.%Mg-0.2wt.%Sc alloy. The ECAP was conducted at room temperature with a die that had a 90° angle between the channels and 8 repetitive ECAP passes followed route BC. Constant stress compression creep tests were performed at 473 K and stresses ranging between 16 to 80 MPa on ECAP materials and, for comparison purposes, on the initial coarse-grained materials. The results showed that the creep resistance of the ECAP processed Al-Sc and Al-Mg-Sc alloys was markedly deteriorated with respect to unpressed coarse-grained materials.


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