Investigation on Ce Addition on Microstructure and Martensitic Transformation of a Ti51Ni49 Shape Memory Alloy

2016 ◽  
Vol 852 ◽  
pp. 28-32
Author(s):  
Ai Lian Liu ◽  
Nan Nan Mao ◽  
Jia Wen Xu ◽  
Wei Cai
Keyword(s):  
Martensitic Transformation ◽  
Shape Memory Alloy ◽  
Shape Memory ◽  
Ternary Alloys ◽  
Tini Alloy ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
The Matrix ◽  
One Step ◽  
Electronic Microscope

The effect of rare earth element Ce addition on the microstructure and martensitic transformation behavior of Ti51Ni49 shape memory alloy was investigated by scanning electronic microscope (SEM), X-ray diffraction (XRD) and differential scanning calorimetry (DSC). The results show that the microstructure of TiNiCe ternary alloy consists of Ti2Ni phase, CeNi phase and the matrix. One-step martensitic transformation is observed in quenched TiNiCe ternary alloys, which is the same as that in quenched TiNi binary alloys. The martensitic transformation temperatures of Ti-rich TiNi alloy hardly increase with Ce addition.

scholarly journals Microstructure and phase transformation of Ni-Ti-Fe-Nd quaternary shape memory alloy

2019 ◽  
pp. 38-42
Author(s):  
Dovchinvanchig Maashaa
Keyword(s):  
Phase Transformation ◽  
Martensitic Transformation ◽  
Shape Memory Alloy ◽  
Shape Memory ◽  
Quaternary Alloy ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
Nd Addition ◽  
One Step ◽  
Electronic Microscope

The effect of rare earth element neodymium (Nd) addition on the microstructure and phase transformation behavior of Ni50Ti47Fe2Nd1 shape memory alloy was investigated by scanning electronic microscope, X-ray diffraction and differential scanning calorimetry. The results show that the microstructure of Ni-Ti-Fe-Nd quaternary alloy consists of NiNd3 phase, NiTi2 and the NiTi matrix. A one-step martensitic transformation is observed in the alloys. The martensitic transformation start temperature Ms 54.110C.

scholarly journals Nanocrystal, phase transformation and microstructure of Ni50Ti50 shape memory alloy

2018 ◽  
Vol 24 (02) ◽  
pp. 22-25
Author(s):  
Dovchinvanchig M ◽  
Chunwang Zhao
Keyword(s):  
Differential Scanning Calorimetry ◽  
Phase Transformation ◽  
Shape Memory Alloy ◽  
Shape Memory ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
One Step ◽  
Niti Matrix ◽  
Electronic Microscope

The nanocrystal, phase transformation and microstructure behavior of Ni50Ti50 shape memory alloy was investigated by scanning electronic microscope, X-ray diffraction and differential scanning calorimetry. The results showed that the microstructure of Ni-Ti binary alloy consists of the NiTi2 phase and the NiTi matrix phase. One-step phase transformation was observed alloy.

Investigation on microstructure and martensitic transformation of neodymium-added NiTi shape memory alloys

2016 ◽  
Vol 30 (28) ◽  
pp. 1650286
Author(s):  
Dovchinvanchig Maashaa ◽  
Ulzii-Orshikh Dorj ◽  
Malrey Lee ◽  
Min Hi Lee ◽  
Chunwang Zhao ◽  
...  
Keyword(s):  
Martensitic Transformation ◽  
Shape Memory ◽  
X Ray Diffraction ◽  
Martensitic Transformation Temperature ◽  
Scanning Calorimetry ◽  
Nd Addition ◽  
One Step ◽  
Niti Shape Memory Alloys ◽  
Niti Matrix ◽  
Electronic Microscope

The effect of rare earth element neodymium (Nd) addition on the microstructure and martensitic transformation behavior of Ni[Formula: see text]Ti[Formula: see text]Nd[Formula: see text] ([Formula: see text] = 0, 0.1, 0.3, 0.5 and 0.7 at.%) shape memory alloy was investigated by scanning electronic microscope, X-ray diffraction and differential scanning calorimetry. The results show that the microstructure of Ni–Ti–Nd ternary alloy consists of NiNd phase, NiTi2 and the NiTi matrix. A one-step martensitic transformation is observed in the alloys. The martensitic transformation temperature Ms increases sharply increasing 0.1–0.7 at.% Nd content is added.

scholarly journals Effect of Nd Addition on the Microstructure and Martensitic Transformation of Ni-Ti Shape Memory Alloys

2014 ◽  
Vol 2014 ◽  
pp. 1-6 ◽  
Author(s):  
M. Dovchinvanchig ◽  
C. W. Zhao ◽  
S. L. Zhao ◽  
X. K. Meng ◽  
Y. J. Jin ◽  
...  
Keyword(s):  
Rare Earth ◽  
Martensitic Transformation ◽  
Shape Memory Alloy ◽  
Shape Memory ◽  
Earth Element ◽  
Transformation Behavior ◽  
Nd Addition ◽  
One Step ◽  
Niti Matrix ◽  
Start Temperature

The effect of rare earth element Nd addition on the microstructure and martensitic transformation behavior of Ni50Ti50−xNdx(x=0, 1, 3, 7, 20) shape memory alloy was investigated experimentally. The results showed that the microstructure of Ni-Ti-Nd ternary alloy consists of the NiNd phase and the NiTi matrix. One-step martensitic transformation was observed in all alloys. The martensitic transformation start temperatureMsincreased gradually with increasing Nd content for Ni-Ti-Nd alloys.

Effect of Electroplastic Deformation on Martensitic Transformation in Coarse Grained and Ultrafine Grained Ni-Ti Shape Memory Alloy

2008 ◽  
Vol 584-586 ◽  
pp. 127-132 ◽  
Author(s):  
Anastasia E. Sergeeva ◽  
Daria Setman ◽  
Michael Zehetbauer ◽  
Sergey Prokoshkin ◽  
Vladimir V. Stolyarov
Keyword(s):  
Differential Scanning Calorimetry ◽  
Martensitic Transformation ◽  
Shape Memory Alloy ◽  
Cold Rolling ◽  
Shape Memory ◽  
Coarse Grained ◽  
Scanning Calorimetry ◽  
Structure Relaxation ◽  
Differential Scanning Calorimetry Method ◽  
Ultrafine Grained

The aim of this paper is the investigation of electroplastic deformation (EPD) and subsequent annealing influence on martensitic transformation in the shape memory Ni50.7Ti49.3 alloy. Using differential scanning calorimetry method it was shown that EPD at the low strain stimulates structure relaxation and recovers martensitic transformation in cooling, which is usually suppressed by cold rolling.

Phase Transformation in Ti-Ni-Ta Shape Memory Alloy

2007 ◽  
Vol 130 ◽  
pp. 147-150 ◽  
Author(s):  
Zdzisław Lekston ◽  
Tomasz Goryczka
Keyword(s):  
Phase Transformation ◽  
Martensitic Transformation ◽  
Shape Memory Alloy ◽  
Shape Memory ◽  
Medical Application ◽  
Precipitation Process ◽  
X Ray Diffraction ◽  
Martensitic Transformation Temperature ◽  
X Ray ◽  
Solution Treated

A new Ti50Ni48.7Ta1.3 shape memory alloy was designed for medical application. In order to influence the martensitic transformation temperature the alloy was solution treated and additionally aged at 400oC for various time. Phase transformation was studied applying differential scanning calorimeter (DSC) and X-ray diffraction techniques. The ageing causes that the martensitic transformation occurs in two steps: B2↔R↔B19’ during cooling and heating. During cooling the transformations: B2→R and R→B19’ are well separated whereas on heating they are overlapped. Also ageing causes a shift of temperatures of the martensitic transformation into the higher region. It is due to the precipitation process. Precipitates of the Ni4Ti3 phase were observed. Applied thermal treatment leads to shift of the transformation temperatures below temperature of a human body. This makes the Ti-Ni-Ta alloy attractive for application in medicine.

Effects of High Temperature ECAE Process on Microstructures and Martensitic Transformation of TiNi Shape Memory Alloy

2006 ◽  
Vol 503-504 ◽  
pp. 1013-0 ◽  
Author(s):  
Chao Ying Xie ◽  
Z.G. Fan ◽  
Z.H. Li ◽  
G.Q. Xiang ◽  
X.H. Cheng
Keyword(s):  
Phase Transformation ◽  
High Temperature ◽  
Martensitic Transformation ◽  
Shape Memory Alloy ◽  
Shape Memory ◽  
Tini Alloy ◽  
Behavior Changes ◽  
Transformation Behavior ◽  
Coarse Grains ◽  
Short Annealing

Microstructures and transformation behavior of TiNi shape memory alloy after high temperature ECAE process have been investigated. It is found that the initial coarse grains were refined after high temperature ECAE processes and short annealing at 750°C. Transformation temperatures of TiNi alloy sharply decreased after two ECAE processes, rose obviously when annealed at 750°C for 5min, and quickly rose back after annealing at 500°C for 2 hours. Reasons for phase transformation behavior changes have been discussed.

INFLUENCE OF POROSITY ON SHAPE MEMORY BEHAVIOR OF POROUS TiNi SHAPE MEMORY ALLOY

2008 ◽  
Vol 01 (03) ◽  
pp. 215-219 ◽  
Author(s):  
JIANYU XIONG ◽  
YUNCANG LI ◽  
PETER D. HODGSON ◽  
CUI'E WEN
Keyword(s):  
Shape Memory Alloy ◽  
Shape Memory ◽  
Tini Alloy ◽  
Compression Tests ◽  
X Ray Diffraction ◽  
Recoverable Strain ◽  
Strain Concentration ◽  
X Ray ◽  
Shape Memory Behavior ◽  
Porous Ti

Porous Ti -50.5at.% Ni shape memory alloy (SMA) samples with a range of porosities were prepared by spacer sintering. The porous structure of the alloy was examined using scanning electron microscopy (SEM). The phase constituents of the porous TiNi alloy were determined by X-ray diffraction (XRD). The shape memory behavior of the porous TiNi alloy was investigated using loading–unloading compression tests. Results indicate that the porous TiNi alloy exhibits superelasticity and the recoverable strain by the superelasticity decreases with the increase of porosity. After a prestrain of 7%, the superelastically recovered strains for the porous TiNi alloy samples with porosities of 46%, 59%, 69% and 77% are 2.0%, 1.8%, 1.5% and 1.3%, respectively. The pores in the TiNi alloy samples cause stress/strain concentration, as well as crack initiation, which adversely affect the shape memory behavior of the porous TiNi alloy.

Shape Memory Characteristics of Ti50Ni50-xCux(x=35, 40) Alloy Strips

2008 ◽  
Vol 47-50 ◽  
pp. 463-466
Author(s):  
Yeon Wook Kim ◽  
Tae Hyun Nam ◽  
Sang Hoon Lee
Keyword(s):  
Martensitic Transformation ◽  
Shape Memory ◽  
Alloy Strip ◽  
X Ray Diffraction ◽  
Strip Surface ◽  
X Ray ◽  
Columnar Grains ◽  
One Step ◽  
Transformation Hysteresis ◽  
Memory Characteristics

The shape memory alloy strips of Ti50Ni15Cu35 and Ti50Ni10Cu40 had been fabricated by arc melt overflow. Their microstructures and shape memory characteristics were investigated by means of X-ray diffraction, optical microscopy and differential scanning calorimetries. The microstructure of as-cast strips exhibited columnar grains normal to the strip surface. X-ray diffraction analysis showed that one-step martensitic transformation of B2-B19 occurred in the alloy strips. According to the DSC analysis, it was known that the martensitic transformation temperature (Ms) of B2→B19 was 71.2°C in Ti50Ni15Cu35 and 64.5°C in Ti50Ni10Cu40 alloy strip, respectively. During thermal cyclic deformation with the applied stress of 60 MPa, transformation hysteresis and elongation associated with the B2-B19 transformation were observed to be 4.9°C and 1.4% in Ti50Ni15Cu35 alloy strip. However, Ti50Ni10Cu40 alloy strip was so brittle that its mechanical properties could not be measured.

Response of Optical Fiber Bragg Sensors With a Thin Film Shape Memory Alloy Coating

2008 ◽  
Author(s):  
K. P. Mohanchadra ◽  
Michael C. Emmons ◽  
Sunny Karnani ◽  
Gregory P. Carman ◽  
W. Lance Richards
Keyword(s):  
Thin Film ◽  
Shape Memory Alloy ◽  
Optical Fiber ◽  
Shape Memory ◽  
Alloy Coating ◽  
Niti Shape Memory Alloy ◽  
Alloy Thin Film ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
Transformation Temperatures

This paper describes the sputter deposition and characterization of nickel titanium (NiTi) shape memory alloy thin film onto the surface of an optical fiber Bragg sensor. The NiTi coating uniformity, crystallinity and transformation temperatures are measured using scanning electron microsocopy, x-ray diffraction and differential scanning calorimetry respectively. The strain in the optical fiber is measured using centroid calculation of wavelength shifts. Results show distinct and abrupt changes in the optical fiber signal with the four related transformation temperatures represented by the austenite-martensite forward and reverse phase transformations. These tests demonstrate a coupling present between optical energy and thermal energy, i.e. a modified multiferroic material.

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