Study of Fracture Resistance of Nanolaminate Coatings Using Indentation and Impact Tests

2016 ◽  
Vol 258 ◽  
pp. 318-321 ◽  
Author(s):  
Vilma Buršíková ◽  
Jaroslav Sobota ◽  
Jan Grossman ◽  
Tomáš Fořt ◽  
Libor Dupák ◽  
...  

The aim of the present work was to study the mechanical properties of thin nanocomposite Mo-B-C coatings consisting of nanocrystalline Mo2BC embedded in amorphous Mo-B-C matrix. Magnetron sputtering of three targets, B4C, C and Mo, was used for coatings preparation. The Mo-B-C coatings were deposited on high speed steel substrates. The fracture resistance of Mo-B-C coatings was studied by both indentation and dynamic impact tests. The impact tests enabled us to predict the load limit causing the coating destruction.

2015 ◽  
Vol 220-221 ◽  
pp. 737-742
Author(s):  
Krzysztof Gocman ◽  
Tadeusz Kałdoński ◽  
Waldemar Mróz ◽  
Bogusław Budner

Boron nitride coatings have been deposited onto high-speed steel substrates using pulsed laser deposition technique combined with RF-discharge. In order to improve adhesion and reduce internal stresses, substrates were subjected to gas nitriding. The structure and morphology of coatings were investigated applying atomic force microscopy (AFM) and FTIR spectroscopy. Nanohardness and elastic modulus were examined employing a nanoanalyzer (CETR). On the basis of the conducted experiments, stable, crystalline, multiphase coatings have been obtained. It has been proved that morphology, structure and mechanical properties strongly depend on the parameters of the PLD process; in particular, the temperature of the substrate has a crucial influence on the properties of BN coatings.


2011 ◽  
Vol 391-392 ◽  
pp. 714-718
Author(s):  
Rui Zhou ◽  
Jian Fei Sun ◽  
Ying Jun Yang

Microstructure and mechanical properties of W9Mo3Cr4V high speed steel fabricated by spray deposition have been studied. Spray deposited W9Mo3Cr4V high speed steel has a typical equiaxed structure which is finer and more homogeneous with a grain size of 20-30 micrometer compared with conventional casted counterparts. There are pores in the matrix of the deposited steel, which involve gas porosity, filling porosity and solidification shrinkage. As-deposited high speed steel is mainly composed of martensite, austenite and carbides which comprise MC carbide and M6C carbide. Mechanical properties show that the hardness and bending strength of the as-deposited steel are higher than that of the conventionally casted ones. However, impact toughness of the high speed steel is lower than that of the conventionally casted steel, which can be attributed to the existence of porosities and M6C carbides which reduce the impact toughness of high speed steels.


2007 ◽  
Vol 336-338 ◽  
pp. 2605-2608 ◽  
Author(s):  
Yan Pei Song ◽  
Xie Min Mao ◽  
Qi Ming Dong ◽  
Liu Ding Tang ◽  
Zhi Ying Ouyang ◽  
...  

Two kinds of thick-walled rings, consisted of WCP/Fe-C gradient composites layers containing about 54 and 70 vol.% of WCP and Fe-C alloy core, were cast by centrifugal casting method. The microstructure, mechanical properties and wear resistance of the gradient composites were investigated. Meanwhile the results were compared with those made of the high speed steel. It was found that WCP in the two kind of gradient composites layers were even well distributed, WCP/Fe-C composites layer of 23-28mm was obtained, the transition layer between the composites layer and matrix alloy core was perfect. The tensile strengths of the two gradient composites layers achieved 345MPa, 460MPa and the impact toughness were 4.6J/cm2, 6.2J/cm2 respectively. Moreover the hardness of the composites layers attained HRA81 and HRA 78. The result of the comparison among the gradient composites layers and that made of the high speed steel showed that the wear resistance of the gradient composites layers containing about 50 and 70 vol.% of WCP was more than 20 times higher than that of the high speed steel under loads of 100N and 200N and sliding velocity of 60 m/s. Finally, the wear-mechanism was discussed.


2010 ◽  
Vol 105-106 ◽  
pp. 488-491
Author(s):  
Yan Li ◽  
Shi Zhong Wei ◽  
Liu Jie Xu ◽  
Chun Wei Xu ◽  
Rui Long

The high-speed steel (HSS) reinforced by in-situ VC /35CrMo compound roll was produced by electromagnetic semicontinuous casting. The element distribution and the structure morphology of the interface were analysed, and the mechanical properties were tested. The results indicate that the thickness of diffusion layer is around 50μm. The microstructure of the diffusion layer is pearlite, and next to the diffusion layer, the microstructures are ferrite and pearlite at the alloyed steel side. There are in-situ VC particles in martensitic matrix. At the high-speed steel side. The microhardness of HSS and 35CrMo is about 700HV and 250HV, respectively, and that of diffusion layer is near 350HV, which is between that of HSS and 35CrMo. The impact toughness is 100 Jcm-2. On the basis of the experiment, the interface of compound roll prepared by electromagnetic semicontinuous casting obtains good microscopic structure and mechanical properties, which are the results of the metallurgically bonded interface.


2021 ◽  
pp. 002199832199945
Author(s):  
Jong H Eun ◽  
Bo K Choi ◽  
Sun M Sung ◽  
Min S Kim ◽  
Joon S Lee

In this study, carbon/epoxy composites were manufactured by coating with a polyamide at different weight percentages (5 wt.%, 10 wt.%, 15 wt.%, and 20 wt.%) to improve their impact resistance and fracture toughness. The chemical reaction between the polyamide and epoxy resin were examined by fourier transform infrared spectroscopy, differential scanning calorimetry and X-ray photoelectron spectroscopy. The mechanical properties and fracture toughness of the carbon/epoxy composites were analyzed. The mechanical properties of the carbon/epoxy composites, such as transverse flexural tests, longitudinal flexural tests, and impact tests, were investigated. After the impact tests, an ultrasonic C-scan was performed to reveal the internal damage area. The interlaminar fracture toughness of the carbon/epoxy composites was measured using a mode I test. The critical energy release rates were increased by 77% compared to the virgin carbon/epoxy composites. The surface morphology of the fractured surface was observed. The toughening mechanism of the carbon/epoxy composites was suggested based on the confirmed experimental data.


2014 ◽  
Vol 788 ◽  
pp. 329-333
Author(s):  
Rui Zhou ◽  
Xiao Gang Diao ◽  
Jun Chen ◽  
Xiao Nan Du ◽  
Guo Ding Yuan ◽  
...  

Effects of sintering temperatures on the microstructure and mechanical performance of SPS M3:2 high speed steel prepared by spark plasma sintering was studied. High speed steel sintering curve of continuous heating from ambient temperature to 1200°C was estimated to analyze the sintering processes and sintering temperature range. The sintering temperature within this range was divided into groups to investigate hardness, relative density and microstructure of M3:2 high-speed steel. Strip and quadrate carbides were observed inside the equiaxed grains. SPS sintering temperature at 900°C can lead to nearly full densification with grain size smaller than 20μm. The hardness and bending strength are higher than that of the conventionally powder metallurgy fabricated ones sintered at 1270°C. However, fracture toughness of the high speed steel is lower than that of the conventional powder metallurgy steels. This can be attributed to the shape and distribution of M6C carbides which reduce the impact toughness of high speed steels.


1993 ◽  
Vol 20 (5) ◽  
pp. 352-356 ◽  
Author(s):  
Z. Naeem ◽  
A. B. Smith ◽  
M. Lamsehchi ◽  
G. W. Critchlow

2001 ◽  
Vol 72 (2) ◽  
pp. 58-65 ◽  
Author(s):  
Saied El-Ghazaly ◽  
Tarek EI-Gammal ◽  
Ahmed EI-Sabbagh ◽  
Adel Nofal ◽  
Mohammed Abbas

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