Evaluation of Material Characteristics with Sintering Temperature in Ti2AlC MAX Phase Material using Spark Plasma Sintering Method

2015 ◽  
Vol 22 (3) ◽  
pp. 175-180
Author(s):  
Chang-Hun Lee ◽  
Gyung Rae Baek ◽  
Hee Sang Jung ◽  
Young-Keun Jeong ◽  
Myung Chang Kang
Keyword(s):  
Spark Plasma Sintering ◽  
Sintering Temperature ◽  
Max Phase ◽  
Material Characteristics ◽  
Plasma Sintering ◽  
Spark Plasma ◽  
Sintering Method

Fabrication of Ti-Based Biodegradable Material Composites Prepared by Spark Plasma Sintering Method

2010 ◽  
Vol 654-656 ◽  
pp. 2158-2161 ◽  
Author(s):  
Eri Miura-Fujiwara ◽  
Takeshi Teramoto ◽  
Hisashi Sato ◽  
Equo Kobayashi ◽  
Yoshimi Watanabe
Keyword(s):  
Spark Plasma Sintering ◽  
Sintering Temperature ◽  
Holding Time ◽  
X Ray Diffraction ◽  
Powder Mixtures ◽  
X Ray ◽  
Porous Ti ◽  
Plasma Sintering ◽  
Spark Plasma ◽  
Sintering Method

This study aims at producing porous Ti filled with biodegradable materials for biomedical implants by means of spark plasma sintering method (SPS). To improve bone fixation and to obtain appropriate Young’s modulus as a medical implant material, we applied -tri calcium phosphate (-TCP) to the Ti-based composite. Ti/-TCP powder mixtures were sintered by SPS under applied stress of 45MPa with various temperatures and holding time. Vickers hardness (Hv) of obtained composite increased with increasing the holding time up to 10 min, and saturated hardness was approximately 750 Hv, which is extremely higher than that of bulk Ti. Hardness also increased as sintering temperature increased up to 1473 K. From the results of microstructure observations by scanning electron microscopy with energy dispersive X-ray spectroscopy (SEM-EDXS), O- and P- containing Ti surrounded around Ti particle, and O diffused into Ti particle to a certain extent. X-ray diffraction results indicated several kinds of Ti-O and/or Ti-P formed in the specimen. Results indicated that it is the brittle phases formed during sintering that increased the hardness.

Preparation and Electrical Properties of Dense Bi4Ti3O12 Ceramics by Spark Plasma Sintering

2007 ◽  
Vol 280-283 ◽  
pp. 141-144
Author(s):  
Jun Jie Hao ◽  
Xiao Hui Wang ◽  
Long Tu Li ◽  
Zhi Lun Gui
Keyword(s):  
Electrical Properties ◽  
Spark Plasma Sintering ◽  
Electronic Materials ◽  
Sintering Temperature ◽  
Sintering Process ◽  
Plasma Sintering ◽  
The Family ◽  
Conventional Sintering ◽  
Spark Plasma ◽  
Sintering Method

The family of bismuth layer-structured ferroelectrics is attractive from the viewpoint of their application as electronic materials such as dielectrics, piezoelectrics and pyroelectrics. However, during conventional sintering method, high sintering temperature and long sintering time were needed and it is difficult to get BIT ceramic with a density more than 95% of its theoretic value. In the present paper, we produce dense BIT pellet using a spark plasma sintering process. The results show that at a sintering temperature as low as 7000C/5min under a pressure of 25MPa, BIT ceramics with a density about 99% of its theoretic can be produced. The densities, grain size and electrical properties of the resulting ceramic were also investigated.

Microstructure and Mechanical Properties of Magnesium Prepared by Spark Plasma Sintering

2010 ◽  
Vol 129-131 ◽  
pp. 764-768 ◽  
Author(s):  
Wan Nur Azrina Wan Muhammad ◽  
Yoshiharu Mutoh ◽  
Yukio Miyashita
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Ultimate Tensile Strength ◽  
Spark Plasma Sintering ◽  
Sintering Temperature ◽  
Pressureless Sintering ◽  
Microstructure And Mechanical Properties ◽  
Plasma Sintering ◽  
Spark Plasma ◽  
Sintering Method

Magnesium powders were sintered by using spark plasma sintering (SPS) and conventional pressureless sintering (PLS) techniques at sintering temperatures ranged from 552°C to 605°C to investigate effect of sintering method on microstructure and mechanical properties of sintered magnesium. High densed magnesium could be obtained by using spark plasma sintering technique compared to conventional presureless sintering at the same sintering temperature. It was found that the ultimate tensile strength increased with increasing sintering temperature for both the materials sintered by PLS and SPS. The magnesium samples prepared by SPS showed better mechanical properties than those prepared by PLS. The microstructural observations revealed that the grain growth was not significant in SPS process compared to PLS, which would enhance the mechanical properties of the SPS sintered magnesium.

Effect of spark plasma sintering temperature on structure and phase composition of Ti-Al-Nb-based alloys

2017 ◽  
Vol 59 (11-12) ◽  
pp. 1033-1036 ◽  
Author(s):  
Sherzod Kurbanbekov ◽  
Mazhyn Skakov ◽  
Viktor Baklanov ◽  
Batyrzhan Karakozov
Keyword(s):  
Phase Composition ◽  
Spark Plasma Sintering ◽  
Sintering Temperature ◽  
Plasma Sintering ◽  
Spark Plasma

scholarly journals Microstructure and properties of nano-laminated Y3Si2C2 ceramics fabricated via in situ reaction by spark plasma sintering

2021 ◽  
Vol 10 (3) ◽  
pp. 578-586
Author(s):  
Lin-Kun Shi ◽  
Xiaobing Zhou ◽  
Jian-Qing Dai ◽  
Ke Chen ◽  
Zhengren Huang ◽  
...  
Keyword(s):  
Spark Plasma Sintering ◽  
Atomic Scale ◽  
Max Phase ◽  
X Ray Diffraction ◽  
Selected Area Electron Diffraction ◽  
Plasma Sintering ◽  
Transmission Electron ◽  
Spark Plasma ◽  
Diffraction Patterns

AbstractA nano-laminated Y3Si2C2 ceramic material was successfully synthesized via an in situ reaction between YH2 and SiC using spark plasma sintering technology. A MAX phase-like ternary layered structure of Y3Si2C2 was observed at the atomic-scale by high resolution transmission electron microscopy. The lattice parameters calculated from both X-ray diffraction and selected area electron diffraction patterns are in good agreement with the reported theoretical results. The nano-laminated fracture of kink boundaries, delamination, and slipping were observed at the tip of the Vickers indents. The elastic modulus and Vickers hardness of Y3Si2C2 ceramics (with 5.5 wt% Y2O3) sintered at 1500 °C were 156 and 6.4 GPa, respectively. The corresponding values of thermal and electrical conductivity were 13.7 W·m-1·K-1 and 6.3×105 S·m-1, respectively.

Microstructure investigation of V2AlC MAX phase synthesized through spark plasma sintering using two various sources V and V2O5 as the starting materials

2019 ◽  
Vol 45 (18) ◽  
pp. 23902-23916 ◽  
Author(s):  
Mohsen Hossein-Zadeh ◽  
Omid Mirzaee ◽  
Hamidreza Mohammadian-Semnani ◽  
Mansour Razavi
Keyword(s):  
Spark Plasma Sintering ◽  
Max Phase ◽  
Plasma Sintering ◽  
Spark Plasma
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