scholarly journals Content and Accumulation of Oxalic Acid in Edible Species of Xanthosoma.

Author(s):  
Dolores Cuebas de Escabí ◽  
Arturo Cedeño-Maldonado

A study was conducted to determine the content and accumulation of oxalic acid in tissues of three edible species of the genus Xanthosoma: X. caracu, X. atrovirens and X. violaceum. Oxalic acid determinations were performed by atomic absorption spectrophotometry. Significant differences were found among the species and tissues studied. Oxalate content was higher in leaf blade and petiole tissues and lower in the pulp of the cormels or rhizomes. Oxalate content in the rhizomes was lowest in X. violaceum and highest in X. caracu. Accumulation in different tissues was progressive and simultaneous with tissue development. No evidence of acid translocation was detected. Postharvest storage of rhizomes resulted in progressive reduction in oxalate content. In all samples analyzed throughout the study the oxalate content of cormels never exceeded 3% of their dry weight.

1989 ◽  
Vol 52 (3) ◽  
pp. 204-206
Author(s):  
ANTHONY LOPEZ ◽  
HARRIET L. WILLIAMS

Ten essential elements were determined in dry and canned butter beans (Phaseolus limensis L.) by atomic absorption spectrophotometry. Samples were taken at different stages during the canning process to determine where changes in element content occurred. The content of each sample was compared statistically to other samples taken within the process. Element retention, excluding chloride and sodium, ranged from 51 to 84% on a dry weight basis, and 14 to 24% on wet weight basis.


1988 ◽  
Vol 51 (7) ◽  
pp. 574-576 ◽  
Author(s):  
ANTHONY LOPEZ ◽  
HARRIET L. WILLIAMS

Ten essential elements were determined in dry and canned chick peas (Cicer arietinum L.) by atomic absorption spectrophotometry. Samples were taken at different stages during the canning process to determine where changes in element content occurred. The content of each sample was compared statistically to other samples taken within the process. Element retention, excluding chloride and sodium, ranged from 12 to 127% on a dry weight basis and 4 to 45% on wet weight basis.


1985 ◽  
Vol 63 (2) ◽  
pp. 159-161 ◽  
Author(s):  
I. Mody ◽  
J. J. Miller

Hippocampal calcium and zinc content was determined using atomic absorption spectrophotometry in control and commissural-kindled rats. In animals exhibiting 5–10 consecutive motor seizures hippocampal calcium was slightly elevated (356.7 parts per million (ppm), dry weight) but not significantly different from controls (329.8 ppm), whereas the amount of zinc was significantly higher (101.6 ppm) than in nonstimulated animals (88.3 ppm). These results are indicative of certain pathophysiological changes in kindled hippocampi, most likely localized to the granule cells of the dentate gyrus where the bulk of hippocampal zinc is confined.


1974 ◽  
Vol 20 (11) ◽  
pp. 1444-1445 ◽  
Author(s):  
R Menachè

Abstract The method of Gitelson et al. was modified to a microscale procedure and adapted for atomic absorption spectrophotometry. Oxalic acid in urine is precipitated with excess of calcium ions at pH 5. The excess of calcium present in the supernate and the total calcium added and present in the urine at pH 2 are determined by atomic absorption spectrophotometry. The oxalic acid present in the precipitate is calculated indirectly from the difference between the two determinations of calcium. This method is useful for routine determination of urinary oxalic acid.


1974 ◽  
Vol 22 (2) ◽  
pp. 104-109 ◽  
Author(s):  
THOMAS H. ROSENQUIST ◽  
JUDITH W. ROSENQUIST

In this quantitative histochemical study, tissues were sectioned, then stained with procedures that conferred a metallic precipitate. Sections were photographed, removed from the slides, air-dried and weighed and then dissolved in acid and the metal content analyzed by atomic absorption spectrophotometry. The stains used in this study were the Alcian Blue (copper phthalocyanin) critical electrolyte concentration procedure on sections of the heart and duodenum from young male rats, colloidal iron on sections of the kidney from adolescent and senescent rats, silver impregnation on sections of the kidney of adolescent and senescent rats and an adenosine triphosphatase lead precipitation reaction on sections of the liver, kidney and heart from adolescent and senescent mice. The objective data obtained by the use of atomic absorption spectrophotometry, reported as micrograms of metal per milligram of dry weight of tissue, allowed statistical analysis of any differences in stain intensity of metallic dyes or metal-precipitating histochemical reactions. Attributes of atomic absorption spectrophotometry which make it desirable for use in this application include accuracy, ease of operation, low cost and ready availability.


1977 ◽  
Vol 60 (4) ◽  
pp. 813-825 ◽  
Author(s):  
Milan Ihnat ◽  
Hanford J Miller

Abstract A method based on acid digestion, hydride evolution atomic absorption spectrophotometry for estimating microgram and submicrogram quantities of As and Se in foods was developed and evaluated. Samples up to 3 g dry weight were digested with HNO3-HClO4-H2SO4. As and Se in aliquots of the digests were reduced with NaBH4 to volatile hydrides, using laboratory-constructed and commercially available generators. As and Se were estimated by transient signal atomic absorbance measurements as the hydrides were decomposed in an Ar-H2-entrained air flame. Recoveries of inorganic As and Se added at levels of 0.1—1.0 μg/g to a variety of foods ranged from 70 to 125%. Analyses of several standard reference samples indicated the method is capable of recovering native analytes. Detection limits for the determinative step and the method as a whole were as low as 5 and 25 ng, respectively, for both elements.


2020 ◽  
Vol 2 (1) ◽  
Author(s):  
Rizki Andalia ◽  
Mulia Aria Suzanni ◽  
Rini Rini

Lipstick or lip dye is a cosmetic dose that serves to coloring, decorative the lips, as a moisturizing material and protect the lips from exposure the sun to provide optimum results. Lipstick should not contain chemicals such as lead (Pb) because the Pb is a heavy metal that is very dangerous when continuously used on the skin, because it will be absorbed into the blood and attack the body organ causing the onset of disease. According to BPOM that the lead rate on the lipstick does not exceed the permissible limit of 20 mg/kg or 20 ppm.This research aims to know the levels contained in the samples are 4 brands of matte lipstick that are sold in the Aceh market in Banda Aceh City with the method of atomic absorption spectrophotometry (AAS). The results showed that on the 4 brands of lipstick matte contain heavy metal lead (Pb) with a rate still qualified allowed by BPOM  is samples A, B, C, and D, respectively at 0.24 ppm; 0.10 ppm; 2.87 ppm and 1.32 ppm, so that the 4 brands of lipstick matte are still used.


2015 ◽  
Vol 1 (1) ◽  
pp. 41
Author(s):  
Bella Santa Rossi ◽  
Paryanti Paryanti ◽  
Yuli Ristianingsih ◽  
Abubakar Tuhuloula

Pewarnaan pada proses produksi kain sasirangan menghasilkan limbah yang mengandung logam berat, diantaranya adalah timbal (Pb2+) dan kadmium (Cd2+). Penelitian ini bertujuan untuk mengetahui pengaruh proses fitoremediasi terhadap konsentrasi logam Pb2+ dan Cd2+ dari limbah cair industri sasirangan di Kalimantan Selatan, serta mengetahui pertambahan berat basah eceng gondok. Eceng gondok yang sudah dibersihkan dan diaklimatisasi ditanam dalam reaktor berisi larutan limbah dengan konsentrasi 3% (v/v); 9% (v/v); dan 15% (v/v). Sampel diambil setiap 2 hari sekali sebanyak 100 ml dan dianalisis menggunakan AAS (Atomic Absorption Spectrophotometry). Hasil penelitian ini menunjukkan bahwa konsentrasi logam Pb2+ dan Cd2+ dalam limbah setelah proses fitoremediasi terjadi penurunan. Kadar Pb2+ pada konsentrasi 3% (v/v) semula 0,197 ppm menjadi 0,062 ppm, pada konsentrasi 9% (v/v) semula 0,200 ppm menjadi 0,077 ppm dan untuk 15% (v/v) adalah 0,225 ppm menjadi 0,093 ppm. Sedangkan untuk Cd2+ konsentrasi 3% (v/v) semula 0,110 ppm menjadi 0,059 ppm, konsentrasi 9% (v/v) adalah 0,127 ppm menjadi 0,045 ppm dan untuk konsentrasi 15% (v/v) semula 0,144 ppm menjadi 0,047 ppm.


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