Interpretation of sedimentary subpopulations extracted from grain size distributions of loess deposits in the Sea of Azov, Russia

Author(s):  
Jie Chen

<p>Loess-paleosol sequences in eastern Europe, especially those at the Azov region, are among the sensitive terrestrial archives for past aeolian dynamics identification and paleoclimatic reconstruction within the Quaternary. Grain size analyses of loess sediments are widely used to interpret these transporting mechanisms and paleoclimatic changes, based on granulometric parameters and statistical decomposition methods. It is therefore of growing interest in the Earth Sciences and has been a major focus of sedimentary studies. Here, we present the unmixing grain size distribution results of a loess-paleosol section by jointly applying the standard deviation method and the end-member modeling in the Sea of Azov, Russia. The results indicated that two methods can produce the similar result on grain size decomposition, while the end-member modeling has advantage on quantitative and objective character. In addition, three main loess subpopulations or end-members with mode sizes of 8 μm, 18 μm and 32 μm respectively which represent distinct aerodynamic environments are identified from the grain size distribution in the Azov region. Thereinto, EM1 with mode size of 8 μm is the integrative result of combining atmosphere circulation with other environmental processes. EM2 with mode size of 18 μm is inferred to represent continuous background dust under non-dust storm conditions. EM3 with mode size of 32 μm is fraction that being transported in short-term, low-altitude suspension clouds during dust storm outbreaks. Of the three EMs, EM1 and EM2 have multiple origins due to their complex formation, whereas EM3 are primarily derived from the alluvial plains of different rivers in the Sea of Azov.</p>

1970 ◽  
Vol 2 (2) ◽  
pp. K69-K73 ◽  
Author(s):  
M. Reinbold ◽  
H. Hoffmann

Materials ◽  
2021 ◽  
Vol 14 (11) ◽  
pp. 2849
Author(s):  
Marcin Jan Dośpiał

This paper presents domain and structure studies of bonded magnets made from nanocrystalline Nd-(Fe, Co)-B powder. The structure studies were investigated using scanning electron microscopy (SEM), high-resolution transmission electron microscopy (HRTEM), Mössbauer spectroscopy and X-ray diffractometry. On the basis of performed qualitative and quantitative phase composition studies, it was found that investigated alloy was mainly composed of Nd2(Fe-Co)14B hard magnetic phase (98 vol%) and a small amount of Nd1.1Fe4B4 paramagnetic phase (2 vol%). The best fit of grain size distribution was achieved for the lognormal function. The mean grain size determined from transmission electron microscopy (TEM) images on the basis of grain size distribution and diffraction pattern using the Bragg equation was about ≈130 nm. HRTEM images showed that over-stoichiometric Nd was mainly distributed on the grain boundaries as a thin amorphous border of 2 nm in width. The domain structure was investigated using a scanning electron microscope and metallographic light microscope, respectively, by Bitter and Kerr methods, and by magnetic force microscopy. Domain structure studies revealed that the observed domain structure had a labyrinth shape, which is typically observed in magnets, where strong exchange interactions between grains are present. The analysis of the domain structure in different states of magnetization revealed the dynamics of the reversal magnetization process.


Author(s):  
Anna Dobkowska ◽  
Boguslawa Adamczyk – Cieślak ◽  
Dariusz Kuc ◽  
Eugeniusz Hadasik ◽  
Tomasz Płociński ◽  
...  

Author(s):  
Mo Ji ◽  
Martin Strangwood ◽  
Claire Davis

AbstractThe effects of Nb addition on the recrystallization kinetics and the recrystallized grain size distribution after cold deformation were investigated by using Fe-30Ni and Fe-30Ni-0.044 wt pct Nb steel with comparable starting grain size distributions. The samples were deformed to 0.3 strain at room temperature followed by annealing at 950 °C to 850 °C for various times; the microstructural evolution and the grain size distribution of non- and fully recrystallized samples were characterized, along with the strain-induced precipitates (SIPs) and their size and volume fraction evolution. It was found that Nb addition has little effect on recrystallized grain size distribution, whereas Nb precipitation kinetics (SIP size and number density) affects the recrystallization Avrami exponent depending on the annealing temperature. Faster precipitation coarsening rates at high temperature (950 °C to 900 °C) led to slower recrystallization kinetics but no change on Avrami exponent, despite precipitation occurring before recrystallization. Whereas a slower precipitation coarsening rate at 850 °C gave fine-sized strain-induced precipitates that were effective in reducing the recrystallization Avrami exponent after 50 pct of recrystallization. Both solute drag and precipitation pinning effects have been added onto the JMAK model to account the effect of Nb content on recrystallization Avrami exponent for samples with large grain size distributions.


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