Influence of compaction and degassing on the properties of submicron
WCCo produced by the PPS method
Influence of compaction and degassing on the properties of submicron WCCo produced by the PPS method. The present study is concerned with the effect of the parameters of the degassing operation (temperature, load and heating rate) conducted at the initial stage of the Pulse Plasma Sintering (PPS) process and the sintering temperature at the final stage of the process, on the properties and microstructure of WCCo with a 6wt% cobalt content sintered by this method. The results of the study have shown that when the heating rate is too high, the material obtained is porous. In most experiments, the sintering temperature of 1050°C appeared to be too low to obtain WCCo composites with density close to the theoretical value (GT). Sintering at the temperature increased to 1070°C yielded sinters with density above 99%GT, with hardness of about 1900 HV30 and fracture toughness KIC=9.3 MNm-3/2.