scholarly journals Microstructure and Tribological Properties of Micro-arc Oxidation TiO2 Coating Before and After SiC Particles Incorporation

2019 ◽  
Vol 25 (3) ◽  
pp. 270-275
Author(s):  
Limei REN ◽  
Tengchao WANG ◽  
Zhaoxiang CHEN ◽  
Xipeng REN ◽  
Xiaowen QI
Keyword(s):  
Composite Coating ◽  
Tribological Properties ◽  
Pure Titanium ◽  
Tio2 Coating ◽  
Commercially Pure Titanium ◽  
Sic Particles ◽  
Micro Cracks ◽  
Before And After ◽  
Micro Arc Oxidation ◽  
Steel Balls

In this work, porous TiO2 coating was fabricated on the surface of commercially pure titanium using the micro-arc oxidation (MAO) technique, and the effect of SiC particles incorporation on the microstructure and tribological properties of MAO TiO2 coating was investigated. Results show that submicron SiC particles dispersed in the MAO electrolyte were incorporated into the TiO2 coating during the MAO process and the fabricated TiO2/SiC composite coating mainly consisted of rutile, anatase and SiC phases. The pore size and surface roughness of TiO2/SiC composite coating decreased with the increasing addition amount of SiC particles in the electrolyte. Furthermore, the incorporation of SiC particles in the TiO2 coating suppressed the initiation and propagation of micro-cracks. The tribological test of coatings against GCr15 stainless steel balls show that the incorporation of submicron SiC particles in the MAO TiO2 coating decreased the friction coefficient and wear rate. DOI: http://dx.doi.org/10.5755/j01.ms.25.3.20089

scholarly journals Self-Lubricating PEO–PTFE Composite Coating on Titanium

Metals ◽  
2019 ◽  
Vol 9 (2) ◽  
pp. 170 ◽  
Author(s):  
Limei Ren ◽  
Tengchao Wang ◽  
Zhaoxiang Chen ◽  
Yunyu Li ◽  
Lihe Qian
Keyword(s):  
Composite Coating ◽  
Tribological Properties ◽  
Plasma Electrolytic Oxidation ◽  
Composite Coatings ◽  
Pure Titanium ◽  
Tio2 Coating ◽  
Commercially Pure Titanium ◽  
Ptfe Composite ◽  
Electrolytic Oxidation ◽  
Plasma Electrolytic

A self-lubricating plasma electrolytic oxidation–polytetrafluoroethylene (PEO–PTFE) composite coating was successfully fabricated on the surface of commercially pure titanium by a multiple-step method of plasma electrolytic oxidation, dipping and sintering treatment. The microstructure and tribological properties of the PEO–PTFE composite coating were investigated and compared with the PEO TiO2 coating and the PTFE coating on titanium. Results show that most of the micro-pores of the PEO TiO2 coating were filled by PTFE and the surface roughness of PEO–PTFE composite coating was lower than that of the PEO TiO2 coating. Furthermore, the PEO–PTFE composite coating shows excellent tribological properties with low friction coefficient and low wear rate. This study provides an insight for guiding the design of self-lubricating and wear-resistant PEO composite coatings.

In vitro Behaviour of Alumina-Hydroxiapatite Composites Coatings

2018 ◽  
Vol 69 (6) ◽  
pp. 1416-1418
Author(s):  
Alexandru Szabo ◽  
Ilare Bordeasu ◽  
Ion Dragos Utu ◽  
Ion Mitelea
Keyword(s):  
Pure Titanium ◽  
Titanium Substrate ◽  
High Strength ◽  
Biological Properties ◽  
Commercially Pure Titanium ◽  
Hvof Spraying ◽  
Before And After ◽  
Sbf Solution ◽  
Oxygen Fuel

Hydroxyapatite (HA) is a very common material used for biomedical applications. Usually, in order to improve its poor mechanical properties is combined or coated with other high-strength materials.The present paper reports the manufacturing and the biocompatibility behaviour of two different biocomposite coatings consisting of alumina (Al2O3) and hydroxyapatite (HA) using the high velocity oxygen fuel (HVOF) spraying method which were deposited onto the surface of a commercially pure titanium substrate. The biological properties of the Al2O3-HA materials were evaluated by in vitro studies. The morphology of the coatings before and after their immersing in the simulated body fluid (SBF) solution was characterized by scanning electron microscopy (SEM). The results showed an important germination of the biologic hydroxyapatite crystallite on the surface of both coatings.

scholarly journals Tribological functionalization of titanium alloys by Micro-Arc Oxidation for marine applications

2020 ◽  
Vol 321 ◽  
pp. 09001
Author(s):  
Aude MATHIS ◽  
Thierry MILLOT ◽  
Vincent BRANGER ◽  
Remy MULLER ◽  
Jean-Yves GUENEHEUX
Keyword(s):  
Friction Coefficient ◽  
Titanium Alloys ◽  
Pure Titanium ◽  
Dynamic Contact ◽  
Electrochemical Process ◽  
Commercially Pure Titanium ◽  
Tribological Behaviour ◽  
Stick Slip ◽  
Micro Arc Oxidation ◽  
Slip Phenomenon

Micro-arc Oxidation (MAO) process is a plasma assisted electrochemical process, which allows formation of ceramic-like dry oxides on top of light alloys surfaces. The good corrosion resistance as well as the low density of titanium alloys are recognized and so required for conception of structural parts in marine environment. However, their tribological behaviour reveals an important tendency to stick-slip phenomenon, which makes use of these alloys for dynamic contact mechanisms difficult. Through the MAO project from IRT M2P, formation of a MAO coating composed of aluminium titanate has been investigated to improve tribological behaviour of a commercially pure titanium (Grade 2) and an α+β alloy (TA6V, Grade 5). Pin-on-disc testing has been carried out to evaluate friction coefficient and the presence or not of stick-slip phenomenon in various contact configurations (involving non-treated titanium surfaces, MAO treated surfaces, with steel or titanium balls …) in dry or artificial seawater media. Those test campaigns are completed by evaluation of fatigue behaviour, and tribological testing on a demonstrator. Finally, this study highlights influence of MAO coating on diminishing (to removed) stick-slip phenomenon, accompanied by a reduction of friction coefficient, whatever the kind of contact (single treated surface or both ones) and the medium.

Fit of cast commercially pure titanium and Ti-6Al-4V alloy crowns before and after marginal refinement by electrical discharge machining

2002 ◽  
Vol 88 (5) ◽  
pp. 467-472 ◽  
Author(s):  
Edwin Fernando Ruiz Contreras ◽  
Guilherme Elias Pessanha Henriques ◽  
Suely Ruiz Giolo ◽  
Mauro Antonio Arruda Nobilo
Keyword(s):  
Electrical Discharge ◽  
Electrical Discharge Machining ◽  
Pure Titanium ◽  
Commercially Pure Titanium ◽  
Commercially Pure ◽  
Before And After

TRIBOLOGICAL PROPERTIES OF TiO2/SiO2 DOUBLE LAYER COATINGS DEPOSITED ON CP-Ti

2016 ◽  
Vol 24 (06) ◽  
pp. 1750082 ◽  
Author(s):  
O. ÇOMAKLI ◽  
M. YAZICI ◽  
T. YETIM ◽  
A. F. YETIM ◽  
A. ÇELIK
Keyword(s):  
Double Layer ◽  
Tribological Properties ◽  
Phase Structure ◽  
Sol Gel ◽  
Pure Titanium ◽  
Commercially Pure Titanium ◽  
Cross Sectional ◽  
Adhesion Properties ◽  
Wear Rates ◽  
Cp Ti

In the present paper, the influences of different double layer on wear and scratch performances of commercially pure Titanium (CP-Ti) were investigated. TiO2/SiO2 and SiO2/TiO2 double layer coatings were deposited on CP-Ti by sol–gel dip coating process and calcined at 750[Formula: see text]C. The phase structure, cross-sectional morphology, composition, wear track morphologies, adhesion properties, hardness and roughness of uncoated and coated samples were characterized with X-ray diffraction, scanning electron microscopy (SEM), nano-indentation technique, scratch tester and 3D profilometer. Also, the tribological performances of all samples were investigated by a pin-on-disc tribo-tester against Al2O3 ball. Results showed that hardness, elastic modulus and adhesion resistance of double layer coated samples were higher than untreated CP-Ti. It was found that these properties of TiO2/SiO2 double layer coatings have higher than SiO2/TiO2 double layer coating. Additionally, the lowest friction coefficient and wear rates were obtained from TiO2/SiO2 double layer coatings. Therefore, it was seen that phase structure, hardness and film adhesion are important factors on the tribological properties of double layer coatings.

Influence of Deformation Substructures on the Early Mechanisms of Recrystallization in Cold-Rolled Titanium and Zirconium

2005 ◽  
Vol 495-497 ◽  
pp. 711-718 ◽  
Author(s):  
N. Dewobroto ◽  
Nathalie Bozzolo ◽  
Francis Wagner
Keyword(s):  
Pure Titanium ◽  
Local Deformation ◽  
Commercially Pure Titanium ◽  
Titanium Sheet ◽  
Commercially Pure ◽  
Before And After ◽  
Nucleation Mechanisms ◽  
Grain Fragmentation ◽  
Cold Rolled ◽  
Short Times

The mechanisms governing the very first stage of static recrystallization in two hexagonal alloys (commercially pure titanium and low alloyed zirconium) are investigated in this paper. Initially fully recrystallized and equiaxed materials were cold-rolled to 80% thickness reduction and subsequently recrystallized at 500°C for short times. High resolution EBSD maps were acquired in a FEG-SEM before and after annealing in order to see where and how the new grains appear. Nonoriented nucleation mechanisms are involved in both materials, and there is a strong correlation between the local deformation substructures and the recrystallization kinetics. Recrystallization is extremely fast in the areas where the deformation cells are small and highly misoriented, i.e. in the areas which underwent severe grain fragmentation. Twinning plays an important role for that purpose in the studied titanium sheet.

scholarly journals Corrosion Resistance of Ti-29Nb-13Ta-4.6Zr Alloy in a Fluoride-Containing Solution

2012 ◽  
Vol 529-530 ◽  
pp. 584-587
Author(s):  
Shinji Takemoto ◽  
Masaaki Nakai ◽  
Masayuki Hattori ◽  
Masao Yoshinari ◽  
Eiji Kawada ◽  
...  
Keyword(s):  
Oxide Film ◽  
Saline Solution ◽  
Pure Titanium ◽  
Marked Change ◽  
Commercially Pure Titanium ◽  
Subsequent Increase ◽  
Commercially Pure ◽  
Outermost Surface ◽  
Before And After ◽  
Constituent Elements

The objective of this study was to evaluate the corrosion behavior of Ti-29Nb-13Ta-4.6Zr alloy (TNTZ) with immersion in an acidic saline solution containing fluoride by investigating change in color and the surface structure of the oxide film. With immersion in fluoride-containing solution, TNTZ showed a less marked change in color than commercially pure titanium (TI), and a smaller decrease in glossiness. The outermost surface was covered with oxides from its constituent elements at before and after immersion in solution with or without fluoride. When immersed in fluoride-containing solution, the film consisted of larger niobium and tantalum oxides than that before or after immersion in solution without fluoride. In summary, TNTZ showed superior resistance to discoloration to TI after immersion in fluoride-containing solution. The results suggest that the subsequent increase in niobium and tantalum fractions in the oxide film in TNTZ improves resistance to corrosion.

FABRICATION OF TI/SIC SURFACE NANO-COMPOSITE LAYER BY FRICTION STIR PROCESSING

2012 ◽  
Vol 05 ◽  
pp. 367-374 ◽  
Author(s):  
ALI SHAMSIPUR ◽  
SEYED FARSHID KASHANI-BOZORG ◽  
ABBAS ZAREIE-HANZAKI
Keyword(s):  
Friction Stir Processing ◽  
Composite Layer ◽  
Pure Titanium ◽  
Titanium Substrate ◽  
Commercially Pure Titanium ◽  
Nano Composite ◽  
Composite Surface ◽  
Friction Stir ◽  
Commercially Pure ◽  
Sic Particles

In the present investigation, novel Ti / SiC surface nano-composite layer was successfully fabricated by dispersing nano-sized SiC particles into commercially pure titanium plates employing friction stir processing technique. The process parameters such as tool rotation and advancing speeds were adjusted to produce defect-free surface composite layer, however, uniform distribution of the nano-size SiC particles in a matrix of titanium was achieved after the second pass. The micro hardness value of the Ti / SiC nano-composite surface layer was found to be ~534 HV; this is 3.3 times higher than that of the commercially pure titanium substrate. No reaction was detected between SiC powders and the titanium matrix after friction stir processing.

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