scholarly journals Study on the Microstructure and Wear Behavior of In-Situ Al3Ti/Al Composites Under Induction Heating

2021 ◽  
Author(s):  
Yuting YAN ◽  
Libin NIU ◽  
Anwen ZHANG ◽  
Chengxin LIU ◽  
Zhidong FAN ◽  
...  

In the study, Ti fiber (200 μm, 99.8 wt.%) and pure aluminum (99.6 wt.%) were respectively used as the reaction source and matrix to prepare Al-based composites by in-situ synthesis methods. During the stage of preparing the preform, Ti fibers were fixed in the matrix at equal intervals to pre-control the initial position of the product. The preform was heated in an induction heating device finally, at the same time, parameter combinations of different frequencies and currents were applied to promote the in-situ reaction between Al-Ti, thereby the Al matrix composites reinforced by Al3Ti were obtained. The phase composition, microstructure and wear resistance of the composites were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and wear testers. The results show that when the frequency and current are 5 kHz and 15 A respectively, the Ti fiber is completely reacted, and the product is the isometric Al3Ti with a size of 1 – 2 μm and a particle spacing of about 5 μm, reaching the optimal microstructure under all parameters. Under the condition of a load of 9.8 N, the wear rate of the composites at 5 kHz and 15 A is 2.325 mg/mm2, indicating the best values in this experiment.

2017 ◽  
Vol 52 (1) ◽  
pp. 123-134 ◽  
Author(s):  
Mohammad Senemar ◽  
Behzad Niroumand ◽  
Ali Maleki ◽  
Pradeep K Rohatgi

In this study, in situ aluminum matrix composites were synthesized through pyrolysis of high temperature vulcanization silicone in commercially pure aluminum melt. For this purpose, 1 to 4 wt% of high temperature vulcanization silicone was added to a vortex of molten aluminum at 750℃ and the resulting slurries were cast in steel dies. Microstructure, hardness, and tensile properties of the as-cast samples were examined at ambient and high temperatures. The results revealed the in situ formation and distribution of reinforcement particles in the matrix. Energy-dispersive X-ray analysis indicated that the formed reinforcement particles consisted of O and Si elements. This confirms the in situ reinforcement formation by pyrolysis of high temperature vulcanization silicone in the melt. The size of the in situ formed particles was mostly in the range of 200–2000 nm. It was shown that the composites synthesized by the addition of 4 wt% high temperature vulcanization had the highest mechanical properties both at ambient and high temperatures. Room temperature hardness, tensile strength, and yield strength of this sample were increased by about 50%, 23%, and 19% compared to the monolithic sample, respectively.


2016 ◽  
Vol 684 ◽  
pp. 287-292 ◽  
Author(s):  
Hrusikesh Nath

The in-situ synthesis of ceramic particles in Al-matrix composites gives an uniform and homogeneous microstructure. The matrix reinforcement interface is compatible with the matrix, interface is clean and provides good interface bonding. The evenly distributed sub micron sized reinforcement particles in Al-matrix enhances the strength and toughness of the composite. The formation of particle clusters and agglomerations are minimized or eliminated by suitably choosing the in-situ process parameters. Large particles and agglomerate are easily fractured where as evenly distributed fine particles are resistant to crack propagation and improves the strength of the composites. The problem encountered with the formation of secondary intermetallic Al3Ti and Al4C3 phases are addressed.


2016 ◽  
Vol 25 (5-6) ◽  
pp. 165-169
Author(s):  
C. Rajaravi ◽  
P.R. Lakshminarayanan

AbstractThe paper describes a different condition of pouring temperature by sand and permanent mould to produce A356-6 wt% TiB2 metal matrix composites by in-situ method salt metal reaction route. The observation of SEM micrographs shows particle distribution of the TiB2 and it appears in hexagonal shape in Al matrix. The results of X-ray diffraction (XRD) analysis confirmed the formation of those TiB2 particulates and the results showed TiB2 particles are homogeneously dispersed throughout the matrix metal. Subsequent structure-property evaluation studies indicated sub-micron size reinforcement of in-situ formed TiB2 particles with improved physical and mechanical properties as compared to sand and permanent mould of Al-TiB2 composites. From, the permanent mould Al-TiB2 composite has an advantage of increase the properties over sand mould Al-TiB2 composite.


2014 ◽  
Vol 53 ◽  
pp. 475-481 ◽  
Author(s):  
Sachin Vijay Muley ◽  
Satya Prakash Singh ◽  
Piyush Sinha ◽  
P.P. Bhingole ◽  
G.P. Chaudhari

Nanomaterials ◽  
2019 ◽  
Vol 9 (4) ◽  
pp. 550 ◽  
Author(s):  
Oleg Tolochko ◽  
Tatiana Koltsova ◽  
Elizaveta Bobrynina ◽  
Andrei Rudskoy ◽  
Elena Zemtsova ◽  
...  

Aluminum-based metallic matrix composites reinforced by carbon nanofibers (CNFs) are important precursors for development of new light and ultralight materials with enhanced properties and high specific characteristics. In the present work, powder metallurgy technique was applied for production of composites based on reinforcement of aluminum matrices by CNFs of different concentrations (0~2.5 wt%). CNFs were produced by chemical vapor deposition (CVD) and mechanical activation. We determined that in situ synthesis of carbon nanostructures with subsequent mechanic activation provides satisfactory distribution of nanofibers and homogeneous composite microstructure. Introduction of 1 vol% of flux (0.25 NaCl + 0.25 KCl + 0.5 CaF2) during mechanic activation helps to reduce the strength of the contacts between the particles. Additionally, better reinforcement of alumina particles and strengthening the bond between CNFs and aluminum are observed due to alumina film removal. Introduction of pure aluminum into mechanically alloyed powder provides the possibility to control composite durability, plasticity and thermal conductivity.


2019 ◽  
Vol 29 (6) ◽  
pp. 1169-1183 ◽  
Author(s):  
Mohammad ROUHI ◽  
Mohammad MOAZAMI-GOUDARZI ◽  
Mohammad ARDESTANI

2011 ◽  
Vol 415-417 ◽  
pp. 170-173
Author(s):  
Jing Wang ◽  
Si Jing Fu ◽  
Yi Chao Ding ◽  
Yi San Wang

A wear resistant TiC-Cr7C3/Fe surface composite was produced by cast technique and in-situ synthesis technique. The microstructure and dry-sliding wear behavior of the surface composite was investigated using scanning electron microscope(SEM), X-ray diffraction(XRD) and MM-200 wear test machine. The results show that the surface composite consists of TiC and Cr7C3as the reinforcing phase, α-Fe and γ-Fe as the matrix. The surface composite has excellent wear-resistance under dry-sliding wear test condition with heavy loads.


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