Using Your Beam Efficiently: Reducing Electron Dose in the STEM via Flyback Compensation

In the scanning transmission electron microscope, fast-scanning and frame-averaging are two widely used approaches for reducing electron-beam damage and increasing image signal noise ratio which require no additional specialized hardware. Unfortunately, for scans with short pixel dwell-times (less than 5 μs), line flyback time represents an increasingly wasteful overhead. Although beam exposure during flyback causes damage while yielding no useful information, scan coil hysteresis means that eliminating it entirely leads to unacceptably distorted images. In this work, we reduce this flyback to an absolute minimum by calibrating and correcting for this hysteresis in postprocessing. Substantial improvements in dose efficiency can be realized (up to 20%), while crystallographic and spatial fidelity is maintained for displacement/strain measurement.

In-Plane Strain Measurement in Composite Structures with Fiber Bragg Grating Written in Side-Hole Elliptical Core Optical Fiber

In this paper, the application of a fiber Bragg grating written in a highly birefringent side-hole elliptical core optical fiber for two-axial strain measurement is presented. Hybrid optical fiber structures achieved by combining large side-holes and elliptical core result in a very high birefringence of 1 × 10−3 and thus high initial Bragg peak spectral separation of 1.16 nm, as well as a very high transverse force sensitivity, of up to 650 pm/(N/mm) or even −1150 pm/(N/mm), depending on the fiber orientation with respect to the applied force. Due to the ~22 %m/m GeO2 concentration in the core the fiber being highly photosensitive, which significantly simplifies FBG fabrication by UV illumination without the need for prior hydrogen loading, which worsens thermal stability. Finally, the developed FBGs written in the highly birefringent side-hole elliptical core optical fiber were embedded in the square composite plates and applied for strain measurements. Tests of two-directional four-point bending have shown usability of such FBG for two-axial in-plane strain measurement with a single FBG in iso-thermal conditions.

Uncertainty Analysis of an Optoelectronic Strain Measurement System for Flywheel Rotors

The strain in a fast spinning carbon fiber flywheel rotor is of great interest for condition monitoring, as well as for studying long-term aging effects in the carbon fiber matrix. Optoelectronic strain measurement is a contactless measurement principle where a special reflective pattern is applied to the rotor which is scanned by a stationary optical setup. It does not require any active electronic components on the rotor and is suited for operation in a vacuum. In this paper, the influences of the key parts comprising the optoelectronic strain measurement are analyzed. The influence of each part on the measurement result including the uncertainty is modeled. The total uncertainty, as well as each part’s contribution is calculated. This provides a valuable assessment of requirements for component selection, as well as tolerances of mechanical parts and processes to reach a final target measurement uncertainty or to estimate the uncertainty of a given setup. We have shown that the edge quality of the special reflective pattern has the strongest influence, and how to improve it. Considering all influences, it is possible to measure strain with an uncertainty of less than 1% at a rotation speed of 500Hz.