The Influences of NP100 Surfactant and Pine-Oil Concentrations on Filtrate Volume and Filter-Cake Thickness of Microemulsion-Based Drilling Fluids (O/W)

In this work, nonionic surfactant NP100 and pine oil influences on the filtrate volume (FV) and the filter-cake thickness (thkns) of microemulsified drilling fluids were studied. A ternary phase diagram was obtained to define the microemulsion region, where a 2k factorial design was used with the addition of four center points and axial points. Twelve microemulsion points were defined and used later in the formulation of the investigated drilling fluids. The results showed that the increase in the surfactant and pine oil’s concentration increased FV and thkns, withthe oil phase being the most influential component in the filtrate volume and the surfactant being the most influential in the filter-cake thickness. Statistically significant models were obtained. The optimal concentrations were determined for the lowest FV and thkns; 45% of surfactant and 5% of pine oil for the filtrate volume (1.3 mL), and 45% of surfactant and 15% of pine oil for the filter-cake thickness (0.64 mm).

Experimental Investigation of Pomegranate Peel and Grape Seed Powder Additives on the Rheological and Filtration Properties of Un-Weighted WBM

The chemical additives used to enhance the properties of drilling mud cause damage to humans and the environment. Therefore, it is necessary to search for alternative additives to add them to the drilling mud. Thus, this study investigates the effects of pomegranate peel and grape seed powders as natural waste when added to un-weighted water-based mud. The test includes measurements of the rheological properties and filtration, as well as the alkanity and density of the drilling mud. The results showed a decrease in PH values ​​with an increase in the concentrations of pomegranate peel or grapeseed, and a decrease in mud density with an increase in powders of pomegranate peel and grape seed concentrations that resulted from the formation of foam. The rheological properties appeared with increasing except for the plastic viscosity. Grape seed powders reduce the filter cake thickness required to solve drilling problems caused by an increase in the mud cake thickness. From the laboratory results, it's possible to use powders of pomegranate peel and grape seed as additives to reduce plastic viscosity and filtrate volume.

Improvement of Filtration Properties of Treated Nigerian Bentonitic Clay Using Locally Sourced Bio-Materials

Exploitation of Nigerian bentonitic clay deposit will offer economic advantage in terms of utilization for drilling purpose and prevent money spent on importation. Clay used for this analysis was beneficiated using sodium Carbonate (Na2CO3) and the change in the elemental composition of the raw clay sample and treated clay with was estimated using X-ray fluorescence spectroscopy (XRF). The treated clay and locally sourced bio-materials were added to the formulation of drilling fluid using Reduced Central Composite Design (RCCD). The fluid loss and cake thickness of prepared drilling fluid were determined using filter loss test kit. The result of the investigation show that the maximum recorded fluid loss was 14.4 ml/30mins at 100 psi while cake thickness values improved with addition of the bio-materials to the drilling fluid formulation when compared with the standard values.

Experimental Analysis of Persea americana as Filtration Loss Control Additive for Non-Aqueous Drilling Fluid

Persea Americana is well known for its short shelf life while the seed is widely considered a waste material by domestic consumers and industry processors. This paper presents the results of the study carried out to evaluate the possibility of using three parts of the Persea Americana namely: its seed, a combination of the Persea Americana seed and its pulp and the Persea Americana pulp as filtration loss control additives in a non-aqueous drilling fluid while using Sodium Asphalt Sulfonate as a control. The evaluation was conducted under high pressure, high temperature (HPHT) static filtration test conditions (at 250°F and 500 psi) based on American Petroleum Institute Standard. From the study, the result showed that all three samples from the Persea Americana fruit showed good potential to control filtration loss when used to formulate a synthetic oil based mud. The filtration control capacity increased as their concentration in the mud was increased. However, in comparison, the pulp was 2.5 times and 1.5 times more efficient in controlling filtration loss when compared to the seed only and the seed and pulp combination respectively. Also, in terms of filtrate volume and filtered cake thickness, an equal concentration of Sodium Asphalt Sulfonate and the proposed additive gave good results; but the existing filtration loss control additive is slightly better than the proposed one. The low fluid loss volumes recorded with Persea Americana as fluid loss additives at HPHT conditions is an indication of its stability at elevated temperature conditions. The cake thickness was thin, impermeable and 1mm in size for all the samples of the Persea Americana. This meets the API requirement of mud cake thickness of less than 2mm.

The Rheology and Performance of Geothermal Spring Water-Based Drilling Fluids

In this study, the rheological properties and performances of mud prepared with geothermal spring water to be used by geothermal drilling operators were examined at ambient and elevated temperatures. In this context, mud samples were prepared in the compositions detailed in the API specification by using five different geothermal spring water types and a distilled water type. Afterwards, density, apparent viscosity, plastic viscosity, yield point, gel strength, fluid loss, pH, and filter cake thickness of these samples were measured. The drilling muds were analyzed by means of rheological tests in accordance with the standards of the American Petroleum Institute (API). The experimental results have revealed that the mud prepared with geothermal water have lower viscosity and yield point compared to those prepared with freshwater at elevated temperatures. The stability of the muds decreases, especially at temperatures higher than 250°F, and they start to become flocculated. It was concluded that geothermal water-based muds have higher API fluid loss and cake thickness than the freshwater-based one. Therefore, it could be interpreted that the muds prepared with geothermal spring water will exhibit lower flow performance and lower ability of hole cleaning and rate of penetration compared to the freshwater muds. Hence, it is recommended that this kind of water should not be used to prepare drilling mud.

Enhancement in Lubricating, Rheological, and Filtration Properties of Unweighted Water-Based Mud Using XC Polymer NPs

In this research, an enhancement in lubricating, rheological, and filtration properties of unweighted water-based mud is fundamentally investigated using XC polymer NPs with 0.2gm, 0.5gm, 1gm, 2gm, and 4gm concentrations. Bentonite, that had been used in the preparation of unweighted water-based mud, was characterized using XRF-1800 Sequential X-ray Fluorescence Spectrometer, XRD-6100/7000 X-ray Diffractometer, and Malvern Mastersizer 2000 particle size analyzer, respectively. Lubricating, rheology and filtration properties of unweighted water-based mud were measured at room temperature (35°C) using OFITE EP and Lubricity Tester, OFITE Model 900 Viscometer, and OFITE Low-Pressure Filter Press, respectively. XC Polymer NPs show a good enhancement in lubricating, rheology and filtration properties of unweighted water-based mud. The effect of XC Polymer NPs on lubricating properties was denoted at 4gm concentration, where the reduction percentage in COF was 30%. An increase in PV, YP, AV, gel strength of unweighted water-based mud was obtained due to the addition of XC Polymer NPs at concentrations up to 4gm. A reduction in filtrate volume and mud cake thickness of unweighted water-based mud was obtained due to the addition of XC Polymer NPs at 2gm and 4gm concentrations, the best result was obtained with using 4gm concentration, the reduction percentage of filtrate volume was 20.7% and mud cake thickness was 41%.

The Influence of Foaming Agent and Cake Thickness on the Drying Process Tomatoes Using a Tray Dryer

Moisture content of tomato (Licopersicon esculentum Mill.) is very high, so easily damaged due to physical impact, enzyme and microbes activity. Further processing is necessary in order to improve shelf life, one way is drying method. This work studied the effect of foaming agent and cake thickness in tomato drying using tray dryer at various temperatures. Foaming agent is used to convert the material into foam, so that the drying temperature can be set relatively low to preserves color, aroma and nutrient composition of the material. The tray dryer is used, because it is simple and the operation cost is relatively cheap. In this work, tomatoes were sliced, crushed for 10 minutes using blender, separated from the seeds and residues with a 60 mesh sieve, and then mixed with dextrin and foaming agent Tween 80 each by 5% weight respectively. Each mixture was blended for 10 minutes. The tray dryer was filled with hot air at 2.0 m/sec with temperature variation of 40, 50, 60 and 70ºC and cake thickness variation of 2 and 4 mm. The results obtained, drying at 50° C is faster than 40º C, while 50 to 70º C is relatively the same. The thicker the cake, the slower the drying time. Performance of foaming agent Tween 80 compared to chemical foaming agent is a natural egg white powder. Drying with a foaming agent Tween 80 faster than egg white powder. Keywords: cake thickness; foaming agent; tomato; tray dryer

Experimental investigation of fluid loss and cake thickness control ability of zirconium (IV) oxide (Z_R O_2) nanoparticles in water based drilling mud.

A major technical and economical concern of the oil well drilling industry is the potential damage to productive formations because of excessive drilling fluid filtration and its multiplier effect on cake thickness. High fluid loss (high cake permeability) results in thick filter cake which reduces the effective diameter of the hole (tight holes) and causes various problems such as excessive torque when rotating the pipe, excessive drag when pulling it and high swab and surge pressures due to reduced hole diameter and differential pipe sticking due to increase in pipe contact.It is in this light that the potential of Zirconium (IV) oxide (Z_r O_2) nanoparticles in combating excessive filtration problem in Water Based Mud was investigated. Preliminary results show that addition of 0.50g (Z_r O_2) nanoparticle concentration brought about 19.10% reduction in fluid loss and 14.29 % reduction in cake thickness for the High Temperature/ High Pressure (HPHT) filtration test at 500psi and 250 OF. Similarly, the highest reduction of 48.31% and 38.10% in fluid loss and cake thickness respectively was achieved with addition of an optimum concentration of 2.0g of (Z_r O_2) nanoparticles for the HTHP filtration test at the same temperature and pressure.