Effects of Calcination Conditions on Particle Size and Morphology of NiFe2O4 Nanoparticles Synthesized by Solid-State Reaction

2012 ◽  
pp. 67-74
Author(s):  
Zhigang Zhang ◽  
Yihan Liu ◽  
Guangchun Yao ◽  
Di Wu ◽  
Junfei Ma
Keyword(s):  
Particle Size ◽  
Solid State ◽  
Solid State Reaction ◽  
Nife2o4 Nanoparticles ◽  
Particle Size And Morphology ◽  
Size And Morphology

Preparation of High-Purity Ultrafine α-Al2O3 by Solid-State Reaction at Room Temperature

2008 ◽  
Vol 368-372 ◽  
pp. 683-685
Author(s):  
Cheng Wei Hao ◽  
Bo Lin Wu ◽  
Ji Yan Li
Keyword(s):  
Solid State ◽  
High Purity ◽  
Solid State Reaction ◽  
Room Temperature ◽  
Raw Materials ◽  
Phase Particle ◽  
Phase Transformation Temperature ◽  
Particle Size And Morphology ◽  
Size And Morphology ◽  
Α Al2o3

Ammonium aluminium carbonate hydroxide (AACH), with a small quantity of γ-AlOOH, was synthesized through solid-state reaction at room temperature using AlCl3·6H2O and NH4HCO3 as raw materials and polyethylene glycol (PEG-10000) as the dispersant. After calcined at 1100°C for 1.5h, α-Al2O3 powders with primary particle sizes of 20~30nm were obtained. The crystal phase, particle size and morphology of the high-purity ultrafine α-Al2O3 were characterized. The results showed that a small quantity of γ-AlOOH in the AACH decomposed and formed crystal seeds. The presence of crystal seeds reduced the nucleation activation energy and therefore reduced the phase transformation temperature.

Direct manipulation of particle size and morphology of ordered mesoporous silica by flow synthesis

RSC Advances ◽  
2015 ◽  
Vol 5 (18) ◽  
pp. 13331-13340 ◽  
Author(s):  
T. N. Ng ◽  
X. Q. Chen ◽  
K. L. Yeung
Keyword(s):  
Particle Size ◽  
Mesoporous Silica ◽  
Hollow Spheres ◽  
Ordered Mesoporous Silica ◽  
Direct Manipulation ◽  
Flow Synthesis ◽  
Precise Control ◽  
Ordered Mesoporous ◽  
Particle Size And Morphology ◽  
Size And Morphology

Flow-synthesis of mesoporous silica allows deliberate and precise control over the size and shapes and enables the preparation of complex microstructures (i.e., hollow spheres).

scholarly journals Dehumidified Air-Assisted Spray-Drying of Cloudy Beetroot Juice at Low Temperature

2021 ◽  
Vol 11 (14) ◽  
pp. 6578
Author(s):  
Aleksandra Jedlińska ◽  
Alicja Barańska ◽  
Dorota Witrowa-Rajchert ◽  
Ewa Ostrowska-Ligęza ◽  
Katarzyna Samborska
Keyword(s):  
Particle Size ◽  
Physicochemical Properties ◽  
Spray Drying ◽  
Low Temperatures ◽  
Beetroot Juice ◽  
Particle Size And Morphology ◽  
Size And Morphology ◽  
Tapped Density ◽  
Lower Loss ◽  
Better Than

This paper discusses the physicochemical properties of powders obtained by spray drying of cloudy beetroot juice, using dehumidified air in variants with or without carriers. The inlet air temperature was 130 °C or 90 °C, and the addition of the carriers was at a ratio of juice to carrier solids of 3:2. In the obtained powders, the following physicochemical properties were determined: water content and water activity, apparent density, loose and tapped density, porosity, flowability, particle size and morphology, and the content and retention of betalains. It was possible to dry cloudy beetroot juice without the use of carriers at low temperatures (90 or 130 °C). The 100% beetroot powders were characterized by satisfactory physicochemical properties, often better than those with carriers (including lower hygroscopicity and higher color saturation and yield). A lower loss of betalains was found for the powders with the addition of carriers. The best process yields were obtained for the powder without carriers at 130 °C and 90 °C.

Synthesis and Properties of (Bi0.5Na0.5)TiO3 Powders by Hydrothermal Method

2007 ◽  
Vol 336-338 ◽  
pp. 140-142
Author(s):  
Jun Jie Hao ◽  
Xiao Hui Wang ◽  
Shi Yun Lin ◽  
Long Tu Li
Keyword(s):  
Particle Size ◽  
Hydrothermal Method ◽  
Single Phase ◽  
Piezoelectric Ceramics ◽  
Treatment Temperature ◽  
Lead Free ◽  
Excellent Candidate ◽  
Traditionally Prepared ◽  
Particle Size And Morphology ◽  
Size And Morphology

Na0.5Bi0.5TiO3 (NBT) is considered to be an excellent candidate for lead-free piezoelectric ceramics. In this study, we propose a hydrothermal method for the preparation of single phase NBT powder at relatively low treatment-temperature. The particle size and morphology of the synthesized powders were examined by SEM. The powders were further pressed into disk and sintered at 1120°C/2h in air, and its properties and microstructure were compared with traditionally prepared samples.

High Tc Oxide Solid State Reaction Kinetics Via Complex Impedance Spectroscopy

1989 ◽  
Vol 169 ◽  
Author(s):  
E. A. Cooper ◽  
T. O. Mason ◽  
U. Balachandran ◽  
M. L. Kullberg
Keyword(s):  
Activation Energy ◽  
Particle Size ◽  
Solid State ◽  
Solid State Reaction ◽  
Complex Impedance ◽  
Particle Size Effect ◽  
Large Temperature ◽  
Impedance Spectra ◽  
High Tc ◽  
Solid State Reaction Kinetics

AbstractImpedance spectra (5Hz ‐ 13MHz) were collected during the solid state reaction of Yba2Cu2O6+y from large monosized CuO particles imbedded in a finely divided Y2 O3 /BaCO3 matrix. No particle size effect was observed, but a large temperature effect was observed corresponding to an activation energy of approximately 1.8eV (175kJ/mol) over the range 700‐900°C.

Solid state reaction synthesis of NiFe2O4 nanoparticles

2008 ◽  
Vol 320 (6) ◽  
pp. 857-863 ◽  
Author(s):  
Abdullah Ceylan ◽  
Sadan Ozcan ◽  
C. Ni ◽  
S. Ismat Shah
Keyword(s):  
Solid State ◽  
Solid State Reaction ◽  
Reaction Synthesis ◽  
Nife2o4 Nanoparticles

scholarly journals Synthesis and Characterization of Rutile Pigments with Cr and Nb

2014 ◽  
Vol 2014 ◽  
pp. 1-8
Author(s):  
Jan Večeřa ◽  
Iveta Šedová ◽  
Petr Mikulášek ◽  
Petra Šulcová
Keyword(s):  
Particle Size ◽  
Solid State ◽  
Particle Size Distribution ◽  
Solid State Reaction ◽  
Organic Matrix ◽  
Synthesis And Characterization ◽  
Visual Color ◽  
Rutile Pigments ◽  
Titanium Compounds

Rutile pigments Ti1-3xCrxNb2xO2±δ (where x=0, 0.05, 0.10, 0.20, 0.30 and 0.50) prepared by solid-state reaction are investigated. Chromium is chromophore (coloring ion) and niobium is counterion (charge-compensating element for electroneutrality). The effect of composition (x), calcination temperature (850, 900, 950, 1000, 1050, 1100 and 1150°C), and starting titanium compounds (anatase TiO2, hydrated anatase paste, TiOSO4·2H2O, and hydrated Na2Ti4O9 paste) on their color properties into organic matrix and particle size distribution was observed. According to the highest chroma C and visual color evaluation, yellow and orange pigments were selected as in color the most interesting. They have concentration x=0.05 or 0.10 and are prepared from anatase TiO2 and TiOSO4·2H2O at temperature ≥1050°C.

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