Polyacrylonitrile solution homogeneity study by dynamic shear rheology and the effect on the carbon fiber tensile strength

2016 ◽  
Vol 56 (3) ◽  
pp. 361-370 ◽  
Author(s):  
Bradley A. Newcomb ◽  
Prabhakar V. Gulgunje ◽  
Yaodong Liu ◽  
Kishor Gupta ◽  
Manjeshwar G. Kamath ◽  
...  
Buildings ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 300
Author(s):  
Md. Safiuddin ◽  
George Abdel-Sayed ◽  
Nataliya Hearn

This paper presents the water absorption and strength properties of short carbon fiber reinforced mortar (CFRM) composite. Four CFRM composites with 1%, 2%, 3%, and 4% short pitch-based carbon fibers were produced in this study. Normal Portland cement mortar (NCPM) was also prepared for use as the control mortar. The freshly mixed mortar composites were tested for workability, wet density, and entrapped air content. In addition, the hardened mortar composites were examined for compressive strength, splitting tensile strength, flexural strength, and water absorption at the ages of 7 and 28 days. The effects of different carbon fiber contents on the tested properties were observed. Test results showed that the incorporation of carbon fibers decreased the workability and wet density, but increased the entrapped air content in mortar composite. Most interestingly, the compressive strength of CFRM composite increased up to 3% carbon fiber content and then it declined significantly for 4% fiber content, depending on the workability and compaction of the mortar. In contrast, the splitting tensile strength and flexural strength of the CFRM composite increased for all fiber contents due to the greater cracking resistance and improved bond strength of the carbon fibers in the mortar. The presence of short pitch-based carbon fibers significantly strengthened the mortar by bridging the microcracks, resisting the propagation of these minute cracks, and impeding the growth of macrocracks. Furthermore, the water absorption of CFRM composite decreased up to 3% carbon fiber content and then it increased substantially for 4% fiber content, depending on the entrapped air content of the mortar. The overall test results suggest that the mortar with 3% carbon fibers is the optimum CFRM composite based on the tested properties.


2012 ◽  
Vol 182-183 ◽  
pp. 76-79 ◽  
Author(s):  
Lei Lei Song ◽  
Quan Rong Liu ◽  
Jia Lu Li

In this paper, carbon fiber reinforced resin matrix composites were produced by stacking eight pieces of carbon fiber woven plain fabric and subjected to accelerated ageing. Accelerated ageing was carried out in oven at 180°C for three different time intervals (60 hours, 120 hours and 180 hours). The influence of different ageing time intervals at 180°C on tensile properties of laminated composites was examined, compared with the composites without aging. The appearance and damage forms of these laminated composites were investigated. The results revealed that the tensile strength of the laminates declined significantly after long term accelerated aging at 180°C. The average tensile strengths of composite samples aged 60 hours, 120 hours, and 180 hours period of time at 180°C are 80.36%, 79.82%, 76.57% of average tensile strength of composite samples without aging, respectively. The high temperature accelerated aging makes the resin macromolecular structure in the composites changed, and then the adhesive force between fiber bundles and resin declines rapidly which result in the tensile strength of composites aged decrease. This research provides a useful reference for long term durability of laminated/epoxy resin composites.


2010 ◽  
Vol 148-149 ◽  
pp. 410-415
Author(s):  
Xiao Ping Luo ◽  
Ming Gang Zhang ◽  
Chun Xiang Lv

A new procedure of surface activation without using palladium salt is proposed for electroless nickel plating (Ni-P) on carbon fiber. The optimal formula and technical conditions for palladium-free activated electroless Ni-P were obtained by orthogonal experiments. The effects of nitric acid processing time on the quality of nickel coating was investigated .The effects of varying concentrations of Ni2 + on the rate of weight gain during the Ni2 + complex adsorption process were also analyzed and the kinetic equation of the process was established. The theoretical values calculated by the equation were proven to be consistent with the experimental verification. The material characteristics of the deposited layers were analyzed by scanning electron microscopy (SEM), energy-dispersive x-ray spectroscopy (EDX) and X-ray diffraction (XRD). The tensile strength of the carbon fibers was analyzed by the Weibull method, and this showed that when the thickness of the Ni-P coating reached 0.150μm, the tensile strength reached a maximum value. The experimental results showed that the nickel deposition on the carbon fiber surface obtained by this method, had the same uniformity, compactness and adhesive properties as the one by conventional electroless Ni-P.


2011 ◽  
Vol 343-344 ◽  
pp. 142-149 ◽  
Author(s):  
Jian Shi ◽  
Kiyoshi Kemmochi ◽  
Li Min Bao

The objective of the present study is to investigate the effect of pyrolysis time and temperature on the mechanical properties of recycled carbon fiber, based on tensile strength measurements, determining the optimum decomposition conditions for carbon fiber-reinforced polymers (CFRPs) by superheated steam. In this research, CFRPs were efficiently depolymerized and reinforced fibers were separated from resin by superheated steam. Tensile strength of fibrous recyclates was measured and compared to that of virgin fiber. Although tensile strength of recycled fibers were litter lower than that of virgin fiber, under some conditions tensile strength of recycled fibers were close to that of virgin fiber. With pyrolysis, some char residue from the polymer remains on the fibers and degrees of char on the recycled fibers were closely examined by scanning electron microscopy.


2018 ◽  
Vol 59 (3) ◽  
pp. 478-482 ◽  
Author(s):  
Vijay Raghavan ◽  
Prabhakar V. Gulgunje ◽  
Kishor K. Gupta ◽  
Manjeshwar G. Kamath ◽  
Yaodong Liu ◽  
...  

2010 ◽  
Vol 4 (4) ◽  
pp. 329-337
Author(s):  
Fabio Pereira ◽  
◽  
Fabiana Vieira ◽  
Luiz de Castro ◽  
Ricardo Michel ◽  
...  

In this work the influence of different configurations in the sample preparation process on commercial polyacrylonitrile-based carbon fibers mechanical tests were studied. Mechanical properties, such as tensile strength, Young’s modulus, elongation and Weibull modulus, were evaluated. The results showed that all sample preparation steps may have strong influence on the results.


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