Determination of vanillin by using gold nanoparticle-modified screen-printed carbon electrode modified with graphene quantum dots and Nafion

2018 ◽  
Vol 185 (3) ◽  
Author(s):  
Gema M. Durán ◽  
Eulogio J. Llorent-Martínez ◽  
Ana M. Contento ◽  
Ángel Ríos
Materials ◽  
2020 ◽  
Vol 13 (3) ◽  
pp. 781 ◽  
Author(s):  
Agnieszka Sasal ◽  
Katarzyna Tyszczuk-Rotko ◽  
Magdalena Wójciak ◽  
Ireneusz Sowa

A simple, sensitive and time-saving differential-pulse adsorptive stripping voltammetric (DPAdSV) procedure using a screen-printed carbon electrode modified with carboxyl functionalized multiwalled carbon nanotubes (SPCE/MWCNTs-COOH) for the determination of diclofenac (DF) is presented. The sensor was characterized using optical profilometry, SEM, and cyclic voltammetry (CV). The use of carboxyl functionalized MWCNTs as a SPCE modifier improved the electron transfer process and the active surface area of sensor. Under optimum conditions, very sensitive results were obtained with a linear range of 0.1–10.0 nmol L−1 and a limit of detection value of 0.028 nmol L−1. The SPCE/MWCNTs-COOH also exhibited satisfactory repeatability, reproducibility, and selectivity towards potential interferences. Moreover, for the first time, the electrochemical sensor allows determining the real concentrations of DF in environmental water samples without sample pretreatment steps.


2020 ◽  
Vol 32 (8) ◽  
pp. 1696-1706 ◽  
Author(s):  
Gizem Kaleli‐Can ◽  
Busra Ozlu ◽  
Hatice Ferda Özgüzar ◽  
Baran Onal‐Ulusoy ◽  
Gözde Kabay ◽  
...  

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