Analyzing the critical mixing time for the liquid-phase reduction synthesis of monodisperse gold nanoparticles using glass microfluidics

2022 ◽  
Vol 26 (2) ◽  
Author(s):  
Hiromasa Yagyu ◽  
Mao Hamamoto ◽  
Yuanwei Wang
Proceedings ◽  
2018 ◽  
Vol 2 (13) ◽  
pp. 702
Author(s):  
Yuanwei Wang ◽  
Yu Tanabe ◽  
Hiromasa Yagyu

According to LaMer diagram, a clearly separate of nucleation and grows step is required to synthesis of monodisperse nanoparticles. However, a critical mixing time Tc until the growth process is started, is not clear experimentally. In this paper, we prepared gold nanoparticles (GNPs) by liquid-phase reduction using citric acid on microfluidics with different flow rates. From relationship of the diameter of the prepared nanoparticle and the mixing time, Tc for the preparation of monodisperse GNPs was found for the first time.


2021 ◽  
Vol 125 (9) ◽  
pp. 5349-5362
Author(s):  
Alejandra Londoño-Calderon ◽  
Wenjie Wang ◽  
Jack J. Lawrence ◽  
Wei Bu ◽  
David Vaknin ◽  
...  

Metallurgist ◽  
1999 ◽  
Vol 43 (11) ◽  
pp. 473-477
Author(s):  
E. F. Vegman ◽  
S. E. Lazutkin ◽  
S. S. Lazutkin

2015 ◽  
Vol 10 (17) ◽  
pp. 1347-1356 ◽  
Author(s):  
Jun Jie Jing ◽  
Jimin Xie ◽  
Gao Yuan Chen ◽  
Wen Hua Li ◽  
Ming Mei Zhang

2019 ◽  
Vol 944 ◽  
pp. 650-656
Author(s):  
Ming Rui Zhang ◽  
Yuan Qin ◽  
Dao Zhang ◽  
Guang Yuan Wang ◽  
Sen Yang

The liquid phase reduction-heat treatment has been used to prepare V2O3nanoparticles in this paper. It is a novel method that the precursor was developed by Oxalic acid dehydrate (H2C2O4·2H2O) reduction of V2O5powder in anhydrous ethanol. V2O3nanoparticles were successfully obtained by thermal treatment of the precursor. The phase, composition, structure, and morphology of the as-obtained samples were verified by XRD, XPS, SEM and TEM measurements. Meanwhile, the possible formation mechanism of V2O3in the heat-treatment is briefly discussed by analyzing the DSC.


RSC Advances ◽  
2020 ◽  
Vol 10 (9) ◽  
pp. 5212-5219 ◽  
Author(s):  
Shuyan Gong ◽  
Anqi Wang ◽  
Jilai Zhang ◽  
Jian Guan ◽  
Ning Han ◽  
...  

Dozens of grams of ultra-fine Cu2O with efficient ozone decomposition was prepared by a facile liquid phase reduction method at room temperature.


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