Facile and rapid fabrication of conductive layers on flexible polymer surfaces and their application to flexible strain sensors

Author(s):  
Dongxue Li ◽  
Dahu Yao ◽  
Xiping Gao ◽  
Chang Lu ◽  
Mengpei Zhang ◽  
...  
Author(s):  
Long Wang ◽  
Kenneth J. Loh ◽  
Ramin Mousacohen ◽  
Wei-Hung Chiang

Strain sensors are one of the most widely used transducers for structural health monitoring, since strain can provide rich information regarding structural integrity. Recently, it has been shown that thin film sensors that incorporate nanomaterials can be engineered to possess unique properties, such as flexibility, high sensitivity, and distributed sensing capabilities, to name a few. To date, a plethora of different nanomaterials have been explored for fabricating strain sensors, such as by using conductive polymers, metal nanowires, and carbon nanotubes, among others. The aim of this work is to leverage the unique properties of graphene to fabricate next-generation thin film strain sensors. While graphene exhibits impressive mechanical and electrical properties, it remains challenging to harness these properties for sensing, primarily because of difficulties associated with high-quality synthesis and to incorporate them in a scalable fashion. In this study, few-layered graphene nano-sheets (GNS) were first synthesized using a low-cost, liquid-phase exfoliation technique. Second, GNS was dispersed in an aqueous solution with a low-concentration polymer acting as the dispersing agent. Third, the dispersion was printed onto flexible polymer substrates to form complex geometrical patterns, such as strain rosettes. Then, the electrical and electromechanical properties of the printed thin film sensors were characterized. It was found that the strain rosettes could resolve multi-axial strains applied during coupon tests. Overall, the GNS-based strain sensors showed excellent signal-to-noise ratio, stable sensing performance, high strain sensitivity, and remarkable reproducibility.


Author(s):  
L.H. Bolz ◽  
D.H. Reneker

The attack, on the surface of a polymer, by the atomic, molecular and ionic species that are created in a low pressure electrical discharge in a gas is interesting because: 1) significant interior morphological features may be revealed, 2) dielectric breakdown of polymeric insulation on high voltage power distribution lines involves the attack on the polymer of such species created in a corona discharge, 3) adhesive bonds formed between polymer surfaces subjected to such SDecies are much stronger than bonds between untreated surfaces, 4) the chemical modification of the surface creates a reactive surface to which a thin layer of another polymer may be bonded by glow discharge polymerization.


Author(s):  
Bruno Schueler ◽  
Robert W. Odom

Time-of-flight secondary ion mass spectrometry (TOF-SIMS) provides unique capabilities for elemental and molecular compositional analysis of a wide variety of surfaces. This relatively new technique is finding increasing applications in analyses concerned with determining the chemical composition of various polymer surfaces, identifying the composition of organic and inorganic residues on surfaces and the localization of molecular or structurally significant secondary ions signals from biological tissues. TOF-SIMS analyses are typically performed under low primary ion dose (static SIMS) conditions and hence the secondary ions formed often contain significant structural information.This paper will present an overview of current TOF-SIMS instrumentation with particular emphasis on the stigmatic imaging ion microscope developed in the authors’ laboratory. This discussion will be followed by a presentation of several useful applications of the technique for the characterization of polymer surfaces and biological tissues specimens. Particular attention in these applications will focus on how the analytical problem impacts the performance requirements of the mass spectrometer and vice-versa.


Author(s):  
Quintin J. Lai ◽  
Stuart L. Cooper ◽  
Ralph M. Albrecht

Thrombus formation and embolization are significant problems for blood-contacting biomedical devices. Two major components of thrombi are blood platelets and the plasma protein, fibrinogen. Previous studies have examined interactions of platelets with polymer surfaces, fibrinogen with platelets, and platelets in suspension with spreading platelets attached to surfaces. Correlative microscopic techniques permit light microscopic observations of labeled living platelets, under static or flow conditions, followed by the observation of identical platelets by electron microscopy. Videoenhanced, differential interference contrast (DIC) light microscopy permits high-resolution, real-time imaging of live platelets and their interactions with surfaces. Interference reflection microscopy (IRM) provides information on the focal adhesion of platelets on surfaces. High voltage, transmission electron microscopy (HVEM) allows observation of platelet cytoskeletal structure of whole mount preparations. Low-voltage, high resolution, scanning electron microscopy allows observation of fine surface detail of platelets. Colloidal gold-labeled fibrinogen, used to identify the Gp Ilb/IIIa membrane receptor for fibrinogen, can be detected in all the above microscopies.


1985 ◽  
Vol 54 (04) ◽  
pp. 842-848 ◽  
Author(s):  
Kandice Kottke-Marchant ◽  
James M Anderson ◽  
Albert Rabinovitch ◽  
Richard A Huskey ◽  
Roger Herzig

SummaryHeparin is known to affect platelet function in vitro, but little is known about the effect of heparin on the interaction of platelets with polymer surfaces in general, and vascular graft materials in particular. For this reason, the effect of heparin vs. citrate anticoagulation on the interaction of platelets with the vascular graft materials expanded polytetrafluoroethylene (ePTFE), Dacron Bionit (DB) and preclotted Dacron Bionit (DB/PC) was studied in a recirculating, in vitro perfusion system. Platelet activation, as shown by a decrease in platelet count, an increase in platelet release and a decrease in platelet aggregation, was observed for all vascular graft materials tested using heparin and was greater for Dacron and preclotted Dacron than for ePTFE. Significant differences between heparin and citrate anticoagulation were seen for platelet release, platelet aggregation and the relative ranking of material platelet-reactivity. However, the trends and time course of platelet activation were similar with both heparin and citrate for the materials tested.


2018 ◽  
Vol 46 (2) ◽  
pp. 78-92 ◽  
Author(s):  
A. I. Kubba ◽  
G. J. Hall ◽  
S. Varghese ◽  
O. A. Olatunbosun ◽  
C. J. Anthony

ABSTRACT This study presents an investigation of the inner tire surface strain measurement by using piezoelectric polymer transducers adhered on the inner liner of the tire, acting as strain sensors in both conventional and dual-chamber tires. The piezoelectric elements generate electrical charges when strain is applied. The inner liner tire strain can be found from the generated charge. A wireless data logger was employed to measure and transmit the measured signals from the piezoelectric elements to a PC to store and display the readout signals in real time. The strain data can be used as a monitoring system to recognize tire-loading conditions (e.g., traction, braking, and cornering) in smart tire technology. Finite element simulations, using ABAQUS, were employed to estimate tire deformation patterns in both conventional and dual-chamber tires for pure rolling and steady-state cornering conditions for different inflation pressures to simulate on-road and off-road riding tire performances and to compare with the experimental results obtained from both the piezoelectric transducers and tire test rig.


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