Microhardness and yield stress of cold rolled pure aluminum up to very high deformation

1983 ◽  
Vol 17 (2) ◽  
pp. 221-226 ◽  
Author(s):  
M. Zehetbauer ◽  
W. Pfeiler ◽  
J. Schrank
Crystals ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1428
Author(s):  
Yunlei Wang ◽  
Liping Ren ◽  
Jingren Dong ◽  
Chuanchuan Cao

In order to study the microstructure evolution rule of pure aluminum plates during different cold-rolled (CR) deformation degrees and annealing processes, samples with aCR deformation of 50~85%, heating rates of 60~100 °C/min and annealing at the target temperature of 350~500 °C were investigated. The microstructure, crystallite dimension and grain boundary characteristics were characterized by the methods of polarizing microscope (PM) and electron backscattered diffraction (EBSD). The results showed that the crystallite dimension of the initial state was 102 μm and ends up completely broken with an increase in the CR deformation degree. When the CR deformation increases to 85%, the deformed micro-bands were very small, with a band spacing of 5~10 μm. At this time, the grain distortion is more serious, there are more high-density grain defects, such as dislocations, and there is a high deformation of the storage energy, which is the energy preparation for the subsequent finished products to withstand the annealing process. The recrystallization fraction was higher with an increase in annealing temperature. After completed recrystallization, the grains showed an equiaxed shape. Orientation imaging and misorientation angle analysis showed that the red-oriented grains of the (001) plane, which had preferred nucleation, recrystallization and rapid grain growth. Final grains of the completed recrystallization are relatively coarse. Under the same deformation, the average crystallite dimension of the recrystallized grains decreases with an increase in annealing heating rate.


2005 ◽  
Vol 495-497 ◽  
pp. 603-608 ◽  
Author(s):  
Atsushi Todayama ◽  
Hirosuke Inagaki

On the basis of Taylor-Bishop-Hill’s theory, many previous theoretical investigations have predicted that, at high rolling reductions, most of orientations should rotate along theβfiber from {110}<112> to {123}<634> and finally into the {112}<111> stable end orientations. Although some exceptions exist, experimental observations have shown, on the other hand, that the maximum on the β fiber is located still at about {123}<634> even after 97 % cold rolling. In the present paper, high purity Al containing 50 ppm Cu was cold rolled up to 99.4 % reduction in thickness and examined whether {112}<111> stable end orientation could be achieved experimentally. It was found that, with increasing rolling reduction above 98 %, {110}<112> decreased, while orientations in the range between {123}<634> and {112}<111> increased, suggesting that crystal rotation along the βfiber from {110}<112> toward {123}<634> and {112}<111> in fact took place. At higher rolling reductions, however, further rotation of this peak toward {112}<111> was extremely sluggish, and even at the highest rolling reduction, it could not arrive at {112}<111>. Such discrepancies between theoretical predictions and experimental observations should be ascribed to the development of dislocation substructures, which were formed by concurrent work hardening and dynamic recovery. Since such development of dislocation substructures are not taken into account in Taylor-Bishop-Hill’s theory, it seems that they can not correctly predict the development of rolling textures at very high rolling reductions, i. e. stable end orientations. On annealing specimens rolled above 98 % reduction in thickness, cube textures were very weak, suggesting that cube bands were almost completely rotated into other orientations during cold rolling. {325}<496>, which lay at an intermediate position between {123}<634> and {112}<111> along theβfiber, developed strongly in the recrystallization textures.


2007 ◽  
Vol 558-559 ◽  
pp. 329-332 ◽  
Author(s):  
Toshiya Shibayanagi ◽  
Masahiro Tsukamoto ◽  
Nobuyuki Abe ◽  
Takamasa Matsumoto ◽  
Y. Soga

Spot heating system utilizing a fiber-laser has been developed in order to control recrystallization, grain growth process and texture development. The newly developed system enables the laser beam to be focused onto the surface of specimen with a minimum diameter of around 10 m. The maximum power of laser in the present system is 100W. Specimens of cold rolled pure aluminum plates of 1mm thick are used for local recrystallization treatment by the spot heating. After laser-spot heating, preferentially recrystallized grains appeared in the irradiated and heat affected region with a diameter depending on the laser power density. The present system enables spot heating on any critical points of the specimen surface. Some laser-heated specimen show locally recrystallized regions occupied by almost single grain having similar crystallographic orientation as that of cold rolled matrix. But the orientation of recrystallized grain is not always the same as that of the matrix. Selective spot heating on grains having peculiar orientation would bring about a possibility of texture control that has not been achieved by means of conventional materials processing.


2013 ◽  
Vol 753 ◽  
pp. 257-262 ◽  
Author(s):  
Wei Min Mao ◽  
Ping Yang

The effects of net driving force for migration of high angle grain boundaries were emphasized beside many other factors which could influence the process of texture formation during recrystallization annealing of 95% cold rolled pure aluminum sheets. The net driving force consists basically of stored energy. However, it could be reduced by recovery, boundary drag, solute drag and Zener drag in different extents, in which only boundary drag is mis-orientation dependent. It was indicated that both oriented nucleation and oriented growth have obvious influence on recrystallization texture, and how far they influence the texture depends also on the level of net driving force when the grain growth starts during annealing. Oriented growth, which is induced by the differences in boundary drag of differently oriented grains, and the corresponding texture formation, could be observed easily when the recrystallization proceeds under relative higher solute drag and Zener drag in commercial purity aluminum. The oriented nucleation process prevails during recrystallization of sufficiently recovered high purity aluminum with very low solute drag and Zener drag, after which strong cube texture forms. In this case the oriented growth indicates limited effect. Both the oriented growth and oriented nucleation will fail if high purity deformation matrix without clear solute drag and Zener drag has not experienced an obvious recovery before recrystallization grain growth, since extremely high net driving force leads to very small critical nucleus size and multiplicity of growing grains, which results in randomization of recrystallization texture.


2008 ◽  
Vol 137 ◽  
pp. 155-162 ◽  
Author(s):  
Agnieszka Mielczarek ◽  
Yvonne Wöckel ◽  
Werner Riehemann

The ductility of Cu – Al – Mn shape memory alloys at room temperature depends on the aluminium content. High aluminium contents make Cu – Al – Mn very brittle and unsuitable for plastic shaping. Two Cu – Al – Mn shape memory alloys were investigated. The ductile alloy CuAl7.8Mn9.5 (all contents in wt. %) could be easily cold rolled by 86 %. The alloy CuAl12Mn4.3 could be cold rolled by only 12 - 14 %. The amplitude dependence of damping of austenitic specimens increased with increasing degree of cold work, whereas the damping of martensiticaustenitic specimens decreased. These observations can be explained by the creation of stress induced martensite and therefore by new moveable interfaces like phase- and twin boundaries, which contribute to damping. Plastic deformation increases the dislocation density, too. Both the increase of dislocation density and the increase of martensite content can lead to a decrease of damping mainly for high deformation degrees. Same shape memory alloys have shown negligible hardness increase during cold rolling, too. This behaviour, untypical for metals, can be explained by the generation of new martensite and by the fact that the hardness of martensite is smaller than the hardness of austenite. Some aging effects of the specimen after cold rolling, which lead to decrease of damping, were detected. This can be explained by pinning of moveable interfaces by point defects and/or retransformation of martensite into austenite.


2013 ◽  
Vol 753 ◽  
pp. 201-206
Author(s):  
Ranjit K. Ray ◽  
Rajib Saha

Less attention has been paid to study the recrystallization and grain growth behavior of severe plastically deformed (SPD) metals specially steels that are deformed to very high strain by conventional rolling method. Present work has been focused on systematic investigation of recrystallization and grain growth behavior of a Aluminium Killed (AK), an Interstitial Free (IF) and an Interstitial Free High Strength (IFHS) steels that were subjected to very high levels of strain (ԑeqv= 4.51) by cold rolling. The cold rolled steels show fine lamellar structure with very strong texture consists of both γ and α fibre. All the steels show formation of ultrafine grains and dramatic rise in the intensity of α fibre component in the early stages of annealing. However, progress of annealing for longer time leads to an increase in the mean grain size as well as γ fibre intensity. The results also indicate that the heavily cold rolled material exhibit selective growth of specific texture components.It appears that microstructure and texture is closely related to the observed phenomenon.


2010 ◽  
Vol 654-656 ◽  
pp. 1486-1491 ◽  
Author(s):  
Y.B. Chun ◽  
S. Lee Semiatin ◽  
Sun Keun Hwang

The recrystallization behavior of cold-rolled, commercial-purity titanium was studied experimentally and with Monte-Carlo (MC) modeling. Utilization of EBSD-OIM as input for MC modeling resulted in realistic predictions of recrystallization kinetics, microstructure and texture, which were in good agreement with experimental results. MC modeling of recrystallization kinetics predicted that the non-uniform stored energy distribution, heterogeneous nucleation of recrystallization and recovery in combination leads to a negative deviation from linear JMAK kinetics. It was found that concurrent recovery that takes place during recrystallization is an important process that controls both the overall recrystallization kinetics and the deviation of linear JMAK kinetics. On the other hand, the non-uniformly distributed stored energy itself has little effect on the negative deviation from JMAK kinetics but intensifies the deviation when heterogeneous nucleation is combined. Modeling results also revealed that heterogeneous nucleation of recrystallized grains and their early impingement in local areas of high deformation are essential for producing a log-normal distribution of grain size and a typical recrystallization texture of rolled titanium.


2008 ◽  
Vol 584-586 ◽  
pp. 327-332 ◽  
Author(s):  
Yun Long Chen ◽  
Ai Dang Shan ◽  
Jian Hua Jiang ◽  
Yi Ding

Asymmetric rolling has been considered as a possible way to obtain severe plastic deformation (SPD) since it will give an extra shear deformation to the processed materials during rolling. Previous researches have confirmed such a shear deformation. Very recently, the method of inserting-block is used to characterize the shear deformation through direct observation, but when the reduction is more than 70%, the lineation scratched on the side face of internal mark becomes vague and illegible. In order to directly observe the shear deformation of metallic material with large reduction, the internal mark method is employed in this research and asymmetric rolling was performed with pure aluminum and iron at room temperature. In severe plastic deformation, the shear deformation caused by asymmetric rolling was clearly observed and measured through employing internal mark method. Remarkable extra shear deformation during asymmetric rolling was confirmed. Very high equivalent strains were achieved when sheet samples were asymmetrically rolled to high reduction ratio. These strain values fall into the range of SPD.


2014 ◽  
Vol 1760 ◽  
Author(s):  
Akira Umise ◽  
Masaki Tahara ◽  
Kenji Goto ◽  
Tomonari Inamura ◽  
Hideki Hosoda

ABSTRACTIn order to improve shape memory properties of Au-Cu-Al based shape memory alloys, the possibility to utilize thermo-mechanical treatment was investigated in this study, and effects of heat-treatment temperature on microstructure, martensitic transformation and mechanical properties of cold-rolled Au-30Cu-18Al-2Fe (AuCuAlFe) alloy were clarified by X-ray diffraction analysis (XRD, differential scanning calorimetry (DSC), scanning electron microscopy (SEM) and tensile tests at room temperature (RT). Here, Fe addition to AuCuAl improves ductility. Cold rolling with the thickness reduction of 30% was successfully carried out in AuCuAlFe at RT. An exothermic heat was observed in DSC at temperature from 402K, suggesting that recovery started at 402K. Besides, the transformation temperature hysteresis increased by the cold-rolling. The alloy was completely recrystallized after the heat treatment at 573K for 3.6ks. Tensile tests revealed that the yield stress was raised by cold rolling and largely by the subsequent heat treatment at 433K, which corresponded to the recovery start temperature by DSC. The yield stress decreased with increasing heat treatment temperature over 453K, probably due to recrystallization. AuCuAlFe cold-rolled and subsequent heat-treated at 573K exhibited the lowest yield stress as well as stress-plateau region, indicating that the thermo-mechanical treatment is effective to improve shape memory properties of Au-Cu-Al based alloys.


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