Effect of Microstructure Evolution and Corrosion Behavior on Phase Transformation of Nanocrystalline SUS304 Prepared by Dry Ice Shot Peening

Microstructure and corrosion behavior of nanocrystalline SUS304 by dry ice shot peening has been investigated in detail in term of phase transformation. SUS304 as metastable austenitic stainless has excellent corrosion resistance and induced martensite by shot peening process. However, the SUS304 has quite low strength which is difficult to wear as metallic component. The dry ice shot peening process was carried out on SUS304 surface for one and three hours. The microstructure was observed by transmission electron microscope (TEM) and scanning electron microscope (SEM) equipped with electron back-scattered diffraction (EBSD). The phase transformation was analyzed by X-ray diffraction (XRD). The corrosion testing was carried out in 3.5% NaCl solution. The result indicated that the grain size of SUS304 surface was finer by deformation due to dry ice shot peened process. The hardness was improved properly by the increasing the shot peened time, and the corrosion resistance was increased. The XRD results showed that three hours shot peening process induced martensite phase of SUS304 by 15 m thickness. It can be summarized that the dry ice shot peening can be induced phase transformation due to high deformation on the SUS304 surface

Magnetic behavior of Magneto-Rheological Foam under Uniaxial Compression Strain

This study reports the development of a Magneto-Rheological Foam, which consists in a porous matrix filled by ferromagnetic particles. The porous matrix of such a composite being easily deformable, large magnetic properties changes are expected. The measurements of the magnetic properties of such a Magneto-Rheological Foam submitted to a compressive strain are reported. Main aspect of the magnetic properties is the low field magnetic permeability as the function of the compression and filling factor. Then, larger field magnetization measurement allowed to investigate the saturation field as a function of the filling factor. Because of the large amount of pores in the material, the magnetic relative permeability, µr, is quite small (µr ~1). However, these materials can be easily deformed over a large range of strain providing important relative variation of the magnetic properties under mechanical solicitation. The composite magnetic permeability is increasing under compression for all the considered filling factors. A model is then developed to understand the variation of the permeability with the strain. Hence, from a simple concept consisting of taking advantage of high deformation of foams, the present study demonstrates the interest of such a highly compressible while cheap composite for obtaining a large magneto-rheological effect.

Influence of Cold Rolled Deformation Degree and Heating Rates on Crystallite Dimension and Recrystallization Fraction of Aluminum Plates

In order to study the microstructure evolution rule of pure aluminum plates during different cold-rolled (CR) deformation degrees and annealing processes, samples with aCR deformation of 50~85%, heating rates of 60~100 °C/min and annealing at the target temperature of 350~500 °C were investigated. The microstructure, crystallite dimension and grain boundary characteristics were characterized by the methods of polarizing microscope (PM) and electron backscattered diffraction (EBSD). The results showed that the crystallite dimension of the initial state was 102 μm and ends up completely broken with an increase in the CR deformation degree. When the CR deformation increases to 85%, the deformed micro-bands were very small, with a band spacing of 5~10 μm. At this time, the grain distortion is more serious, there are more high-density grain defects, such as dislocations, and there is a high deformation of the storage energy, which is the energy preparation for the subsequent finished products to withstand the annealing process. The recrystallization fraction was higher with an increase in annealing temperature. After completed recrystallization, the grains showed an equiaxed shape. Orientation imaging and misorientation angle analysis showed that the red-oriented grains of the (001) plane, which had preferred nucleation, recrystallization and rapid grain growth. Final grains of the completed recrystallization are relatively coarse. Under the same deformation, the average crystallite dimension of the recrystallized grains decreases with an increase in annealing heating rate.

Research on the Controlling Effect of NPR Cables for Anti-Dip Slope Based on the Numerical Simulation

As the scale and depth of mines increase, large deformations of high-steep slopes progressively become prominent. Compared with the ordinary cables, negative Poisson’s ratio (NPR) cables can provide a constant resistance force and high deformation inhibition during slope deformation, avoiding the occurrence of slope instability hazards. Consequently, the control effects on the toppling failures of slopes were necessary to be researched. Changshanhao open-pit gold mine was taken as an example; based on the field geological investigation and rock mechanics testing, a three-dimensional engineering geological model of open-pit mine was constructed. Subsequently, the stability of open pit in current situation and final boundary situation was estimated with FLAC3D software, for the potential slope vulnerable areas to be comprehensively identified. Finally, the control effects of ordinary cables and NPR cables on the instable W13 slope section were compared and studied through FLAC3D simulations, and the reinforcement effects of NPR cable on the anti-dip slope were proved as significant; meanwhile, the corresponding reinforcement methods in the failure mine areas were proposed, laying a reference for the instability failure control and reinforcement of similar anti-dip slopes.

Effect of recrystallization on degree of sensitization in nickel free austenitic stainless steel

Purpose Effect of grain size on degree of sensitization (DOS) was been evaluated in Nickel free steel. Manganese and nitrogen contained alloy is a Ni-free austenitic stainless steels (ASS) having type 202 grade. The main purpose of this investigation is to find the effect of recrystallization on the DOS of stainless steel after the thermo-mechanical processing (cold work and thermal aging). Design/methodology/approach In the present investigation, the deformation of 202 grade analyzed using X-ray diffraction (XRD) and microstructural testing. Optical microstructure of Ni-free ASS has been done for cold worked samples with thermally aged at 900°C_6 h. Double loop electrochemical potentiodynamic reactivation test used for findings of degree of sensitization. Findings Ni-free ASS appears to be deformed more rapidly due to its higher stacking fault energy which gave results in rapid transformation from strain induced martensite to austenite in form of recrystallized grains, i.e. it concluded that as cold work percentage increases more rapidly recrystallization occurs. XRD results also indicate that more fraction of martensite formed as percentage of CW increases but as thermal aging reverted those all martensite to austenite. So investigation gives the conclusion which suggests that with high deformation at higher temperature and duration gives very less DOS. Originality/value Various literatures available for 300 series steel related to the effect of cold work on mechanical properties and sensitization mechanism. However, no one has investigated the effect of recrystallization through thermomechanical processing on the sensitization of nickel-free steel.

Thermoplastic Composites for Integrally Woven Pressure Actuated Cellular Structures: Design Approach and Material Investigation

The use of pressure-actuated cellular structures (PACS) is an effective approach for the application of compliant mechanisms. Analogous to the model in nature, the Venus flytrap, they are made of discrete pressure-activated rows and can be deformed with high stiffness at a high deformation rate. In previous work, a new innovative approach in their integral textile-based manufacturing has been demonstrated based on the weaving technique. In this work, the theoretical and experimental work on the further development of PACS from simple single-row to double-row PACS with antagonistic deformation capability is presented. Supported by experimental investigations, the necessary adaptations in the design of the textile preform and the polymer composite design are presented and concretized. Based on the results of pre-simulations of the deformation capacity of the new PACS, their performance was evaluated, the results of which are presented.

Initiation and Suppression of Crack Propagation during Magnesium Alloy Rolling

The conventional rolling of magnesium alloy with a single pass and large reduction will cause severe edge cracking. The sheet without cracks can be achieved by limited width rolling. The microstructure evolution of the sheet with cracks after conventional rolling and the sheet without cracks after limited width rolling is explored, and an effective mechanism for solving edge cracks is proposed. Conventional rolling can fully develop twin evolution due to high deformation, and three stages of twinning evolution can be observed and the secondary twins easily become the nucleation points of micro cracks, resulting in a large number of cracks propagating along the twin lamellae. Cracks terminate at dislocation accumulation because the accumulation of a large number of dislocations can hinder propagation. Dislocation shearing of twins to eliminate the high localization caused by twins and induce the tensile twins to weaken the basal surface texture provides an effective plastic deformation mechanism of crack inhibition, which is useful for expanding the engineering application of magnesium alloy rolled sheets.

Can Fluid-Substitution Models Continue to Ignore the Complex Physico-Chemical Properties of Crude Oil?

The mechanical nature of fluid-substitution models has always been recognized as a major cause of their limited predictive power. Saturants, for instance, are typically treated as simple fluids characterized only by their densities, viscosities, and moduli of elasticity; their chemistry is just ignored, even when that fluid is crude oil. However, crude oil is a complex mixture of several thousands of organic compounds characterized by a variety of molecular weights, polarities, and polarizabilities, and the response of its rheological behavior to acoustic wave propagation is difficult to predict, especially when it resides inthe pore space of rocks. Here, we report ultrasonic-velocity measurements performed on carbonate core plugs saturated with brine and with a light crude oil that are mechanically similar (i.e., having comparable densities, viscosities, and moduli of elasticity) and that show a significant and consistent excess of hardening when the saturant is oil. Dispersion and wettability are excluded as explanations for the data. We hypothesize that asphaltene aggregation and adsorption, as well as paraffin-wax crystallization (and possibly volumetric expansion), combine to cause crude oil to exhibit a dilatant-like behavior within the pore space of carbonates at ultrasonic frequencies. Roughly speaking, the observed effect would be similar to the hardening of oobleck at high deformation rates. This hypothesis could betested in the future by an adequate combination of high-resolution imaging and microfluidic setups. This and similar studies would be beneficial in developing physical fluid-substitution models with a more consistent predictive power.

Dislocation Mechanics of Extremely High Rate Deformations in Iron and Tantalum

High strain rate simulations were performed using the multiscale dislocation dynamic plasticity (MDDP) method to calculate different rise times and load durations in mimicking high deformation rate shock or isentropic (ramp) testing of a-iron and tantalum crystals. Focus for both types of loading on both materials was on the inter-relationship between the (dislocation-velocity-related) strain rate sensitivity and the (time-dependent) evolution of dislocation density. The computations are compared with model thermal activation strain rate analysis (TASRA), phonon drag and dislocation generation predictions. The overall comparison of simulated tests and previous experimental measurements shows that the imposition of a rise time even as small as 0.2 ns preceding plastic relaxation via the MDDP method is indicative of relatively weak shock behavior.