Volta potential of second phase particles in extruded AZ80 magnesium alloy

2006 ◽  
Vol 51 (17) ◽  
pp. 3551-3557 ◽  
Author(s):  
F. Andreatta ◽  
I. Apachitei ◽  
A.A. Kodentsov ◽  
J. Dzwonczyk ◽  
J. Duszczyk
2011 ◽  
Vol 686 ◽  
pp. 6-10 ◽  
Author(s):  
Ya Qin Yang ◽  
Zhi Min Zhang ◽  
Bao Cheng Li

The precipitation mechanism of secondary-precipitated phase β in AZ80 magnesium alloy during the hot compression deformation under different temperature was investigated. The results show that there are β-Mg17Al12 phases with different morphology and precipitation mechanism in the microstructure of AZ80 alloy deformed both in two-phase region、critical region and single-phase region. β-Mg17Al12 phases were directly deformed and broken to be strip form during the compression under 200、250、300 and 350°C. A lot of fine granular second phase particles precipitated with the grain refinement simultaneously in AZ80 alloy deformed in two-phase region with tremendous deformation. There are also fine granular second phase particles precipitated in the alloy deformed in critical region. There are massive β-Mg17Al12 phases precipitated in the alloy deformed under higher temperature such as 350 and 400°C during the water cooling after the compression, the high power observation of which is fine and tightly lamellar microstructure. Compared with coarse reticular β-Mg17Al12 phases in the as-cast microstructure of AZ80 alloy, the morphology of β-Mg17Al12 phases precipitated during the hot compression has obvious improvement.


2011 ◽  
Vol 291-294 ◽  
pp. 1082-1086
Author(s):  
Yao Jin Wu ◽  
Zhi Ming Zhang ◽  
Bao Cheng Li ◽  
Bao Hong Zhang ◽  
Jian Min Yu ◽  
...  

In the present research, the influences of different extrusion ratios (15, 30, 45, 60, and 75) and extrusion temperature (300°C, 330°C, 360°C, 390°C, 420°C) on the mechanical properties and microstructure changes of AZ80 magnesium alloy have been investigated through tensile test and via ZEISS digital metallographic microscope observation. Research indicates that the alloy’s plasticity gradually decreases as the temperature increases, and that the alloy’s tensile strength varies with the extrusion ratio. At 330°C, the alloy’s particle grain is small and a small amount of black hard and brittle second-phase β (Mg17Al12) are precipitated uniformly along the grain boundary causing the gradual increase of the alloy’s tensile strength. When the extrusion temperature is up to 390°C, the grain size increases significantly, but the second phase precipitation along grain boundaries transforms into continuous and uniform-distribution precipitation within the grain. In this case, when the extrusion ratio is 60, the alloy’s tensile strength reaches its peak 390 Mpa. As the extrusion temperature increases, inhomogeneous precipitation of the second-phase along grain boundaries increases, causing the decrease of the alloy’s strength. At the same temperature, both the tensile strength and plasticity increases firstly and then decreases as extrusion ratio increases. With the gradual increase of the refinement grain, the dispersed precipitates increase and the alloy’s tensile strength and plasticity reach their peaks when the extrusion temperature is 390°C. As the grain grows, the second phase becomes inhomogeneous distribution, and the alloy’s strength and plasticity gradually decrease.


Metals ◽  
2020 ◽  
Vol 10 (6) ◽  
pp. 777
Author(s):  
Yun Zhang ◽  
Haitao Jiang ◽  
Yujiao Wang ◽  
Zhe Xu

As an important fabrication process, annealing treatment is conducted to eliminate distortion in magnesium alloy sheets. Second-phase particles can provide nucleation sites for recrystallization grains, and the basal texture is related to the recrystallization behavior. Three experimental Mg-2Zn-based magnesium alloy sheets were investigated by the salt bath annealing process. Combined with variations in hardness softening, evolution of microstructure and basal texture, the effect of second-phase particles on microstructure evolution was analyzed. The results showed that the significant influence of size and distribution of second-phase particles on static recrystallization in magnesium alloy sheets was exhibited, which lead to the formation of two stages in the annealing process, combined with static recovery behavior. Second phase particles with coarse size were beneficial to recrystallization grains’ nucleation and increased recrystallization behavior in the initial stage of annealing. Second-phase particles with fine size inhibited recrystallization behavior and weakened the softening of hardness. The basal texture was weakened by second phase particles at the stage of recrystallization nucleation. The change in basal texture at the stage of grain growth was related to the size of second-phase particles. The regulation of basal texture enhancement can be envisioned by modifying second-phase particles.


2015 ◽  
Vol 787 ◽  
pp. 442-447 ◽  
Author(s):  
R. Jayaraman ◽  
T. Balusamy ◽  
A.K. Lakshminarayanan

Microstructure, micro hardness and wear resistance of friction stir processed cast magnesium alloy are investigated in this work. Image analysis is used to differentiate the amount of phases present in the base metal and friction stir processed regions. Hardness mapping indicates that the frictions stir processed region has 64 % increase in microhardness compared to the base metal. Wear resistance was evaluated using pin-on-disc testing and it is found that the friction stir processed region has superior wear resistance compared to the base metal. Fine grains with uniformly distributed second phase particles are the reasons for improved microhardness and wear resistance of friction stir processed region.


2021 ◽  
Vol 0 (0) ◽  
Author(s):  
Ankur Kumar ◽  
F. Khan MD ◽  
Sushanta Kumar Panigrahi ◽  
Gajanan P. Chaudhari

Abstract Effect of microstructural changes after friction stir processing (FSP) on the corrosion behaviour of rare earth containing QE22 magnesium alloy is studied. FSP produced ultrafine-grained α-Mg matrix and refined the Mg12Nd precipitates whereas Mg12Nd2Ag precipitates got dissolved in the matrix. Although its hardness increased from 76 to 90 VHN, the FSPed alloy displayed inferior corrosion resistance in 3.5 wt% NaCl solution. This is attributed mainly to the iron contamination from FSP and presence of refined second phase particles which work as active cathodic sites. The role of distributed Mg12Nd precipitates before and after FSP is analysed from micro galvanic corrosion point of view.


2011 ◽  
Vol 239-242 ◽  
pp. 238-242
Author(s):  
Peng Hui Deng ◽  
Tie Cheng Li ◽  
Gang Yi Cai

In this study, the comprehensive performance of AZ80 magnesium alloy was improved by solution treatment and multi-step ageing treatment. The effects of different thermal processing parameters on the microstructure and mechanical properties of AZ80 magnesium alloy were studied. The experimental results show that the optimal process of solution treatment for AZ80 alloy is heated at 420°C for 5h, which the β phase dissolve thoroughly into the α substrate. After first-stage ageing treatment, the hardness of samples varied as the ageing temperature, and had higher hardeness at temprature 180°C. While in the second-stage ageing treatment, the sample got the ageing peak value at 210°C for 10h. After two-stage treatment, the grains of AZ80 magnesium alloy became homogeneous and fine, and the second phase distributes along the grain boundary and plays an important role of dispersion strengthening. Above all, the optimal heat treatment process of AZ80 magnesium is solution treated at 420°C for 5h, as well as ageing at 180°C, 4h and 210°C, 10h.


2007 ◽  
Vol 544-545 ◽  
pp. 419-422 ◽  
Author(s):  
Akira Watazu ◽  
Ichinori Shigematsu ◽  
Xin Sheng Huang ◽  
Kazutaka Suzuki ◽  
Naobumi Saito

Noncombustible Mg-8Al-2Ca rods were processed by RD-ECAP. The magnesium alloy rod had Mg matrix and Al2Ca second phase. Grains with about 20 μm in diameter were observed in the matrix of the raw materials. The grains in matrix had no anisotropy. On the other hand, positions of second phase particles had anisotropy and the second phase particles formed lines. The samples processed by RD-ECAP had no crack and the samples had 20mm diameter. Grains in matrix of the 4 pass RD-ECAP sample had no anisotropy and the grains had under about 5 μm in diameter. The second phase particles had round shapes and were uniformly distributed as compared with the raw material rod. Therefore, the RD-ECAP is useful for forming noncombustible Mg-8Al-2Ca alloy with fine-grains.


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