Solid-liquid interface and growth rate range of Al2O3-based eutectic in situ composites grown by laser floating zone melting

2016 ◽  
Vol 662 ◽  
pp. 634-639 ◽  
Author(s):  
Qun Ren ◽  
Haijun Su ◽  
Jun Zhang ◽  
Bin Yao ◽  
Weidan Ma ◽  
...  
1991 ◽  
Vol 237 ◽  
Author(s):  
Richard D. Robinson ◽  
Ioannis N. Miaoulis

ABSTRACTThis paper presents a new experimental method to investigate solid-liquid interface morphologies during Zone-Melting-Recrystallization at lower than the typical processing temperatures. Gallium films were used as a substitute for silicon films. In situ preliminary investigation identified three phenomena typically occurring during ZMR of silicon films: a) Transition from planar to dendritic to cellular morphologies was observed for different processing conditions; b) cell period proved to be dependant on scanning velocity; c) instabilities at the solidification interface at low heating strip temperatures were caused by supercooling and optical property variations as the material changed phase.


2011 ◽  
Vol 299-300 ◽  
pp. 341-344
Author(s):  
Xu Dong Yue ◽  
Guang Can Jin ◽  
Shu Ying Chen ◽  
Guo Wei Chang

In situ observation of growth process of high temperature phase in 0.15% C carbon steel during solidification concerned with using Confocal Scanning Laser Microscope (CSLM), the growth rate of -phase has been measured. The results indicate that high temperature -phase grows at cell crystal way when the cooling speed reaches 2°C/min in 0.15% C carbon steel. The -phase of round or oval cross-sectional shaped may grow stably. The growth rate of -phase is gradually getting slow along with increasing of curvature radius. The variation of growth speed tends to be similar with different solid-liquid interface shapes of -phase. The growth rate of concave solid-liquid interface is faster than that of convex solid-liquid interface for phase. The smaller radius of curvature of phase is, the faster the growth rate reaches.


2012 ◽  
Vol 562-564 ◽  
pp. 216-219
Author(s):  
Li Xin Li

The δ-phase growth process of Fe-0.2%C-0.6%Mn steel during solidification was in-situ observed using Confocal Scanning Laser Microscope (CSLM). The effects of shape of solid/liquid interface on the growth rate were investigated. The results indicate the growth rate of concave-shaped solid/liquid interface is faster than that of convex-shaped solid/liquid interface at the beginning of δ-phase growth. The two kinds of growth rates decreased both and approached to the same gradually as the solidification continues. The intrinsic reasons were discussed in detail.


2020 ◽  
Vol 10 (16) ◽  
pp. 5362-5385
Author(s):  
Leila Negahdar ◽  
Christopher M. A. Parlett ◽  
Mark A. Isaacs ◽  
Andrew M. Beale ◽  
Karen Wilson ◽  
...  

Many industrially important chemical transformations occur at the interface between a solid catalyst and liquid reactants. In situ and operando spectroscopies offer unique insight into the reactivity of such catalytically active solid–liquid interfaces.


2005 ◽  
Vol 16 (1-4) ◽  
pp. 107-110
Author(s):  
A. P. Shpak ◽  
O. P. Fedorov ◽  
E. L. Zhivolub ◽  
Y. J. Bersudskyy ◽  
O. V. Shuleshova

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