Hydration forces between aligned DNA helices undergoing B to A conformational change: In-situ X-ray fiber diffraction studies in a humidity and temperature controlled environment

2017 ◽  
Vol 200 (3) ◽  
pp. 283-292 ◽  
Author(s):  
Ryan Case ◽  
Hauke Schollmeyer ◽  
Phillip Kohl ◽  
Eric B. Sirota ◽  
Roger Pynn ◽  
...  
Keyword(s):  
Conformational Change ◽  
Controlled Environment ◽  
X Ray ◽  
Fiber Diffraction ◽  
Temperature Controlled ◽  
Hydration Forces

Controlled Environment Specimen Transfer

2014 ◽  
Vol 20 (4) ◽  
pp. 1038-1045 ◽  
Author(s):  
Christian D. Damsgaard ◽  
Henny Zandbergen ◽  
Thomas W. Hansen ◽  
Ib Chorkendorff ◽  
Jakob B. Wagner
Keyword(s):  
Electron Microscope ◽  
Transmission Electron Microscope ◽  
Elevated Temperatures ◽  
Controlled Environment ◽  
Ambient Atmosphere ◽  
Air Exposure ◽  
X Ray ◽  
Environmental Transmission ◽  
Transmission Electron

AbstractSpecimen transfer under controlled environment conditions, such as temperature, pressure, and gas composition, is necessary to conduct successive complementary in situ characterization of materials sensitive to ambient conditions. The in situ transfer concept is introduced by linking an environmental transmission electron microscope to an in situ X-ray diffractometer through a dedicated transmission electron microscope specimen transfer holder, capable of sealing the specimen in a gaseous environment at elevated temperatures. Two catalyst material systems have been investigated; Cu/ZnO/Al2O3 catalyst for methanol synthesis and a Co/Al2O3 catalyst for Fischer–Tropsch synthesis. Both systems are sensitive to ambient atmosphere as they will oxidize after relatively short air exposure. The Cu/ZnO/Al2O3 catalyst, was reduced in the in situ X-ray diffractometer set-up, and subsequently, successfully transferred in a reactive environment to the environmental transmission electron microscope where further analysis on the local scale were conducted. The Co/Al2O3 catalyst was reduced in the environmental microscope and successfully kept reduced outside the microscope in a reactive environment. The in situ transfer holder facilitates complimentary in situ experiments of the same specimen without changing the specimen state during transfer.

scholarly journals IN-SITU COMPRESSION TEST OF ARTIFICIAL BONE FOAMS IN CONTROLLED ENVIRONMENT USING X-RAY MICRO-COMPUTED TOMOGRAPHY

2019 ◽  
Vol 25 ◽  
pp. 48-51
Author(s):  
Jonathan Glinz ◽  
Daniel Kytýř ◽  
Tomáš Fíla ◽  
Jan Šleichrt ◽  
Andreas Schrempf ◽  
...  
Keyword(s):  
Computed Tomography ◽  
Haptic Feedback ◽  
Controlled Environment ◽  
Artificial Bone ◽  
Micro Computed Tomography ◽  
Foaming Agent ◽  
X Ray ◽  
Surgical Simulators ◽  
Liquid Immersion

In this study, we investigated specimens of artificial bone foams, developed by the research group for surgical simulators at the UAS Linz, which are used to mimic the haptic feedback of physiologic and pathologic bone for more realistic surgery training. Specimens with two kinds of mineral filler material as well as different amounts of foaming agent were tested in an environmental in-situ loading stage developed by the ITAM CAS and scanned via X-ray micro-computed tomography. In this in-situ stage, specimens can be immersed in liquid and tested under temperature-controlled conditions. Consequently, a total amount of 12 specimens was subjected to compression loading; half of them immersed in water at 36.5◦C and half in dry condition. Results showed that there is no significant influence of liquid immersion to the compression outcome. However, foams with less amount of foaming agent appeared to have smaller pores resulting in higher compression strength.

A temperature-controlled sample stage for in situ micro-X-ray diffraction: Application to Mars analog mirabilite-bearing perennial cold spring precipitate mineralogy

2014 ◽  
Vol 99 (5-6) ◽  
pp. 943-947 ◽  
Author(s):  
M. S. Bramble ◽  
R. L. Flemming ◽  
J. L. Hutter ◽  
M. M. Battler ◽  
G. R. Osinski ◽  
...  
Keyword(s):  
X Ray Diffraction ◽  
X Ray ◽  
Cold Spring ◽  
Mars Analog ◽  
Temperature Controlled

The Use of Advanced Analytical Techniques for Characterization of the Chemical, Physical, and Crystallographic Nature of a Surface

1973 ◽  
Vol 31 ◽  
pp. 132-133 ◽  
Author(s):  
R. E. Herfert
Keyword(s):  
Surface Characterization ◽  
Analytical Techniques ◽  
X Ray Diffraction ◽  
Depth Of Penetration ◽  
X Ray ◽  
The Past ◽  
Transmission Electron ◽  
Scanning Electron

Studies of the nature of a surface, either metallic or nonmetallic, in the past, have been limited to the instrumentation available for these measurements. In the past, optical microscopy, replica transmission electron microscopy, electron or X-ray diffraction and optical or X-ray spectroscopy have provided the means of surface characterization. Actually, some of these techniques are not purely surface; the depth of penetration may be a few thousands of an inch. Within the last five years, instrumentation has been made available which now makes it practical for use to study the outer few 100A of layers and characterize it completely from a chemical, physical, and crystallographic standpoint. The scanning electron microscope (SEM) provides a means of viewing the surface of a material in situ to magnifications as high as 250,000X.

In Situ X-Ray Absorption Studies of the Electrochemical Reduction of Hydroxocobalamin

1997 ◽  
Vol 7 (C2) ◽  
pp. C2-619-C2-620 ◽  
Author(s):  
M. Giorgett ◽  
I. Ascone ◽  
M. Berrettoni ◽  
S. Zamponi ◽  
R. Marassi
Keyword(s):  
Electrochemical Reduction ◽  
X Ray ◽  
Absorption Studies ◽  
X Ray Absorption

A Revised O2 Reduction Model in Li-O2 Batteries as Revealed by in Situ Small Angle X-Ray Scattering

2019 ◽  
Author(s):  
Christian Prehal ◽  
Aleksej Samojlov ◽  
Manfred Nachtnebel ◽  
Manfred Kriechbaum ◽  
Heinz Amenitsch ◽  
...  
Keyword(s):  
Small Angle ◽  
Wide Angle ◽  
Reduction Mechanism ◽  
Reduction Model ◽  
X Ray ◽  
X Ray Scattering ◽  
O2 Reduction ◽  
Ray Scattering

<b>Here we use in situ small and wide angle X-ray scattering to elucidate unexpected mechanistic insights of the O2 reduction mechanism in Li-O2 batteries.<br></b>

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