FTIR spectroscopy supported by statistical techniques for the structural characterization of plastic debris in the marine environment: Application to monitoring studies

2016 ◽  
Vol 106 (1-2) ◽  
pp. 155-161 ◽  
Author(s):  
Mauro Mecozzi ◽  
Marco Pietroletti ◽  
Yulia B. Monakhova
2013 ◽  
Vol 2 (2) ◽  
pp. 152-156 ◽  
Author(s):  
Maria Leônia C. Gonzaga ◽  
Thiago M.F. Menezes ◽  
José Roberto R. de Souza ◽  
Nágila M.P.S. Ricardo ◽  
Sandra de A. Soares

2011 ◽  
Vol 324 ◽  
pp. 205-208 ◽  
Author(s):  
Ziyad S. A. Al Sarraj ◽  
Mukhlis M. Ismail ◽  
Sabah M. Ali ◽  
Wan Q. Cao

BaTiO3powders were prepared hydrothermally using TiCl4, Ba(OH)2.8H2O and NH4OH as starting materials at 150°C for 2h. The structure of the prepared nanocystalline BT powders were a metastable cubic perovskite according to XRD and HRTEM analysis, while FT Raman spectra showed that BT powders have a tetragonal structure. Hydroxyl and carbonate groups were observed in all prepared powders that showed in FTIR spectroscopy as vibrational bands. The tetragonal phase of BT powder was identified clearly by slow scan XRD at 2θ between 44.6 to 46°. The crystallite size of BT powders have increased with the increase of annealing temperature from 19 nm at room temperature to 70 nm at 1000°C.


2019 ◽  
Vol 70 (9) ◽  
pp. 3232-3235
Author(s):  
Carmen Mihaela Topala ◽  
Adriana Gabriela Plaiasu ◽  
Catalin Marian Ducu ◽  
Sorin Georgian Moga

Undoped and Al-doped ZnO (AZO) powders have been synthesized by hydrolytic and hydrothermal synthesis from Zn(NO3)2 , AlCl3 using KOH 1M concentraction like hydrolisis agent. The structural properties of prepared powders were studied using XRD and FTIR spectroscopy. Presence of aluminium in the hydrothermal powders is correlated with the presence of Zn-Al hydrotalcite like structure.


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