Microstructural evolution of a nickel-based superalloy

Author(s):  
Waldemar A. Monteiro ◽  
Ingrid A. Dos Santos

Superalloys are indispensable for the superior perfomance and efficien of jet engine turbine disks,turbine blades,combustors,roket shells and many other devices and components used in various industries, in Cluding nuclear, space and aeronautics.Over the last thirty years,nickel-base superalloys has undergone more structural studies than any other superalloy as a result of attempts to correlate its properties to microstructure and heat treatment. To avoid contradictory or inconsistent findings, it is also necessary a carefully microstructural observation of the employed starting materials. In the present paper,we report morphologies relating to the as cast , forged and heat-treated Ni-base superalloy by transmission and scanning electron microscopy. This superalloy contain intermettallic compounds and carbides. The alloy in study was an as cast and also forged Ni-Fe based superalloy with the following chemical composition:

2017 ◽  
Vol 891 ◽  
pp. 420-425
Author(s):  
Sureerat Polsilapa ◽  
Aimamorn Promboopha ◽  
Panyawat Wangyao

Cast nickel based superalloy, Grade Inconel 738, is a material for turbine blades. Its rejuvenation heat treatment usually consist of solution treatment condition with temperature range of 1125-1205 oC for 2-6 hours. Then it is following with double aging process including primary aging at 1055oC for 1 hour and secondary aging at 845oC for 24 hours. However, the various selected temperature dropping program were performed during solution treatment to simulate the possible error of heating furnace. The maximum number of temperature dropping during solution treatment is varied from 1-3 times From all obtained results, the various temperature dropping during solution treatment conditions showed extremely the significant effect on the final rejuvenated microstructures and long-term gamma prime stability after heating at temperature of 900oC for 200 hours.


2015 ◽  
Vol 816 ◽  
pp. 551-556
Author(s):  
Su Gui Tian ◽  
Bao Shuai Wang ◽  
Xin Ding ◽  
De Long Shu ◽  
Jing Wu

Creep behavior of a heat treated single crystal nickel base superalloy containing Re/Ru under the test condition of 1100°C/137MPa high temperatures was investigated. The experimental results showed that the segregation extent of elements in the dendrite and inter-dendrite regions of single crystal superalloy decreases by heat treatment at high temperature. The creep life of the alloy at 1100°C/137MPa was measured to be 321 h displaying a better creep resistance. Wherein, significant amount of fine cubiodal γ′ particles precipitated in the γ matrix channels are considered to be the main reason of the alloy having the better creep resistance. The deformation feature of the alloy during steady state creep is dislocations slipping in the γ matrix and climbing over the rafted γ′ phase. But in the latter stage of creep, the deformation feature of the alloy is dislocations shearing into the rafted γ′ phase. As creep goes on, the main / secondary slipping dislocations in the alloy are alternately activated to result in the initiation and propagation of the cracks along the interface of the rafted γ′/γ phase up to fracture, which is thought to be the fracture mechanism of the alloy during creep.


2021 ◽  
pp. 3-15
Author(s):  
N.V. Petrushin ◽  
◽  
E.M. Visik ◽  
E.S. Elyutin ◽  
◽  
...  

Results of design and experimental studies of a nickel-based superalloy VZhL20 with a density of 8.04 g/cm3 for the manufacture of turbine blades with a columnar granular structure and a single-crystal structure are presented. It is shown that alloy VZHL20 with a single-crystal structure of the crystallographic orientation [001] in the heat-treated state possesses high phase stability, and enhanced short-term strength ( = 950 MPa, = 1130 MPa), and long-term strength ( = 340 MPa, = 185 MPa).


2014 ◽  
Vol 782 ◽  
pp. 578-583 ◽  
Author(s):  
Juraj Belan

The aerospace industry is one of the biggest consumers of advanced materials because of its unique combination of mechanical and physical properties and chemical stability. Highly alloyed stainless steel, titanium alloys and nickel based superalloys are mostly used for aerospace applications. The aim of the work is to evaluate protective Al Si coating applied by diffusion annealing on substrate, Ni base superalloy ZS6K. This superalloy is used for turbine blade production in aero jet engine DV 2. Using of protective alitize coating provides an increasing of heat resistance of superalloy surface and increases working temperature up to 800°C. However, overcrossing of working temperature range (for ZS6K turbine blades it is from 705°C to 750°C) sometimes happen and that is the reason for detailed study of protective coating degradation. The alitize coating were evaluated in starting stage and after various time of regular loading in real aero jet engines DV 2. Coating and its degradation was evaluated with help of quantitative metallography methods (metallography software NIS Elements) and colour contrast as well.


Author(s):  
Ernst E. Affeldt

TMF tests were conducted with bare and aluminide coated single crystal nickel-based superalloy specimens. Temperature cycling was between 400°C and 1100°C with a phase shift (135°) which is typical for damaged locations on turbine blades. Stress response is characterized by a constant range and the formation of a tensile mean stress as a result of relaxation in the high temperature part of the cycle which is in compression. Bare specimens showed crack initiation from typical oxide hillocks. Coated specimens showed life reduction with respect to the bare ones caused by brittle cracking of the coating in the low temperature part of the cycle. Isothermal bending tests of coated specimens confirmed the low ductility of the coating at tempeatures below 600°C but quantitative correlation with the TMF test results failed.


2017 ◽  
Vol 891 ◽  
pp. 433-437 ◽  
Author(s):  
Nattapol Kontikame ◽  
Sureerat Polsilapa ◽  
Panyawat Wangyao

This research work has an aim to investigate the effect of precipitation aging temperatures of 845°C, 865°C, 885°C and 905°C for 24 hours after solutioning treatment at temperature of 1145°C for 4 hours on final microstructure of cast nickel base superalloy, grade Inconel 738, which is used as a material for turbine blades in land base gas turbine engines to generate electricity in power plants. Further interesting is also extended to study and evaluate the phase stability of precipitated gamma prime particles after long-term heating at tempeatures of 900°C and 1000°C for 200 hours of all received final microstructures after various reheat treatment conditions. From all obtained results, it was found that the higher precipitation aging temperatures provided the more coarsening size of both coarse and fine gamma prime particles. Furthermore, after long-term exposure at high temperatures, this resulted in an increasing of both area density and size of gamma prime particles.


2006 ◽  
Vol 321-323 ◽  
pp. 509-512 ◽  
Author(s):  
Jung Seob Hyun ◽  
Gee Wook Song ◽  
Young Shin Lee

A more accurate life prediction for gas turbine blade takes into account the material behavior under the complex thermo-mechanical fatigue (TMF) cycles normally encountered in turbine operation. An experimental program has been carried out to address the thermo-mechanical fatigue life of the IN738LC nickel-base superalloy. High temperature out-of-phase and in-phase TMF experiments in strain control were performed on superalloy materials. Temperature interval of 450-850 was applied to thermo-mechanical fatigue tests. The stress-strain response and the life cycle of the material were measured during the test. The mechanisms of TMF damage is discussed based on the microstructural evolution during TMF. The plastic strain energy based life pediction models were applied to the stress-strain history effect on the thermo-mechanical fatigue lives.


Author(s):  
Björn Buchholz ◽  
Uwe Gampe ◽  
Tilmann Beck

The growing share of power generation from volatile sources such as wind and photovoltaics requires fossil fuel fired power generation units be available and capable of high load flexibility to adjust to the changing capacity of the electrical grid. Additionally, back-up units with quick start capability and energy storage technologies are needed to fill the power shortfall when volatile sources are not available. Gas turbine and combined-cycle gas and steam turbine power plants are able to meet these demands. However, safe component design for improved cycling capability, combined with optimum utilization of material regarding its mechanical properties, requires design procedures and lifing models for the complex loadings resulting from this increased volatility of power demand. Since hot gas path components like turbine blades and vanes are highly stressed by cyclic thermal and mechanical loadings, resulting Thermo-Mechanical Fatigue (TMF), life prediction models such as the classic strain-life Coffin-Manson-Basquin method do not capture the influences of thermal cycling satisfyingly. Advanced TMF prediction models are thus necessary to accurately predict the durability of hot section components. This paper addresses life prediction of the Nickel-base superalloy René 80 at elevated temperature for various loading conditions. For this purpose, isothermal Low Cycle Fatigue (LCF) and corresponding TMF tests, with various temperature ranges and thermal-mechanical phase shifts, have been performed. On this basis, a systematic approach has been developed which allows assessing the key influences on TMF life. Moreover, a generalized model for fatigue has been derived, which has the potential to predict TMF life on the basis of LCF data. The knowledge gained from the model development allows an improved life prediction and better utilization of the material capabilities. Additionally, the required number of material tests for a general insight in the materials behaviour can be reduced significantly.


1996 ◽  
Vol 78 (1-3) ◽  
pp. 113-123 ◽  
Author(s):  
A.A. Tchizhik ◽  
A.I. Rybnikov ◽  
I.S. Malashenko ◽  
S.A. Leontiev ◽  
A.S. Osyka

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