Different sample preparation methods for the analysis of suspension fertilizers combining LIBS and liquid-to-solid matrix conversion: determination of essential and toxic elements

2017 ◽  
Vol 9 (35) ◽  
pp. 5156-5164 ◽  
Author(s):  
Daniel Fernandes Andrade ◽  
Marco Aurelio Sperança ◽  
Edenir Rodrigues Pereira-Filho

A novel calibration method was developed for the determination of macronutrients in suspension fertilizer samples by laser-induced breakdown spectroscopy (LIBS).

Author(s):  
Raquel C Machado ◽  
Diego Victor Babos ◽  
Daniel Fernandes Andrade ◽  
Edenir Rodrigues Pereira-Filho

Quantitative analysis requires several efforts to obtain an adequate calibration method to overcome matrix effects employing direct solid analysis by laser-induced breakdown spectroscopy (LIBS). To this end, in this study,...


2016 ◽  
Vol 242 (10) ◽  
pp. 1685-1692 ◽  
Author(s):  
Gonca Bilge ◽  
Banu Sezer ◽  
Kemal Efe Eseller ◽  
Halil Berberoğlu ◽  
Hamit Köksel ◽  
...  

Talanta ◽  
2013 ◽  
Vol 117 ◽  
pp. 55-59 ◽  
Author(s):  
David A. Rusak ◽  
Ann E. Zeleniak ◽  
Jillian L. Obuhosky ◽  
Scott M. Holdren ◽  
Craig A. Noldy

2016 ◽  
Vol 8 (37) ◽  
pp. 6705-6710 ◽  
Author(s):  
Pengcheng Han ◽  
Daming Dong ◽  
Xiaofan Du ◽  
Leizi Jiao ◽  
Xiande Zhao

Laser-induced breakdown spectroscopy was used for the fast determination of calcium concentration in the internal tissues of a single seed. Compared with conventional methods, LIBS had obvious advantages, such as a little analysis spot, little ablation, high precision, and small influence on the seed vigor.


1992 ◽  
Vol 46 (9) ◽  
pp. 1382-1387 ◽  
Author(s):  
J. A. Aguilera ◽  
C. Aragón ◽  
J. Campos

Laser-induced breakdown spectroscopy has been used to determine carbon content in steel. The plasma was formed by focusing a Nd:YAG laser on the sample surface. With the use of time-resolved spectroscopy and generation of the plasma in nitrogen atmosphere, a precision of 1.6% and a detection limit of 65 ppm have been obtained. These values are similar to those of other accurate conventional techniques. Matrix effects for the studied steels are reduced to a small slope difference between the calibration curves for stainless and nonstainless steels.


2014 ◽  
Author(s):  
Łukasz Łazarek ◽  
Arkadiusz J. Antończak ◽  
Michał R. Wójcik ◽  
Paweł E. Kozioł ◽  
Bogusz Stępak ◽  
...  

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