scholarly journals Processing and properties of hollow glass microsphere particulate-filled PA2200 composites produced by selective laser sintering

2021 ◽  
Vol 261 ◽  
pp. 02016
Author(s):  
Dong Ye ◽  
Lihua Yu ◽  
Gaoyan Hou ◽  
Hong Zhu
Keyword(s):  
Volume Fraction ◽  
Selective Laser Sintering ◽  
Tensile Modulus ◽  
Laser Sintering ◽  
Glass Microsphere ◽  
Hollow Glass Microsphere ◽  
Matrix Composites ◽  
Scanning Calorimetry ◽  
Hollow Glass ◽  
Tensile Experiment

Selective laser sintering (SLS) to prepare composites by adding filler into polymer is an effective method to save costs and reinforce the sintered parts. This article investigated the fabrication of PA2200 composites filled with different volume fractions of hollow glass microsphere (HGM) by SLS. HGM was prepared by silane coupling agent surface treatment. The particle size distribution, microstructure, thermal and mechanical properties of PA2200/HGM composites were studied by scanning electron microscopy (SEM), differential scanning calorimetry (DSC) and tensile experiment. The results indicated that the density of the composite was significantly reduced compared to the neat PA2200 and the density decreased with the HGMs content increasing. HGM improved the warping deformation in the process of sintering. The tensile modulus increased while tensile strength and elongation at break decreased as a function of HGM volume fraction in a certain range. This work indicated that thermal properties and tensile properties of polyamide-matrix composites can be reinforced by adjusting HGM content, and PA2200/HGM composite powder is a good material for SLS with less density and lower cost.

Investigation of flexural properties of hollow glass microsphere filled resin-matrix composites

2016 ◽  
Vol 45 (6) ◽  
pp. 426-430 ◽  
Author(s):  
Yingjie Qiao ◽  
Xiaodong Wang ◽  
Xiaohong Zhang ◽  
Zhipeng Xing
Keyword(s):  
Volume Fraction ◽  
Resin Matrix ◽  
Future Research ◽  
Flexural Properties ◽  
Flexural Property ◽  
Hollow Glass Microsphere ◽  
Matrix Composites ◽  
Syntactic Foams ◽  
Content Type ◽  
Hollow Glass

Purpose The purpose of this paper is to investigate the preparation and the flexural property of hollow glass microspheres (HGMs) filled resin-matrix composites, which have been widely applied in deep-sea fields. Design/methodology/approach The composites with different contents of HGMs from 47 to 57 Wt.% were studied. The voids in syntactic foams and their flexural properties were investigated. Findings The results showed that the voids quantity increased because of the increment of HGM content, whereas the exural strength and the exural modulus decreased. The fracture mechanism of the composites was also investigated by scanning electron microscope, which indicated that the composites failed by the crack extending through the microspheres. Research limitations/implications The advantages of HGMs with similar hollow spheres will be further investigated in a future research. Practical implications Results demonstrated that the properties of the composite might be tailored for specific application conditions by changing the HGM volume fraction. Originality/value The HGM filled resin-matrix composite materials have their unique properties and significant application potential. In this work, the resin-HGM composites were synthesized by mechanically mixing defined quantities of HGMs into epoxy resin, by which a kind of syntactic foams with good flexural properties could be obtained.

Study in performance and morphology of polyamide 12 produced by selective laser sintering technology

2018 ◽  
Vol 24 (5) ◽  
pp. 813-820 ◽  
Author(s):  
Junjie Wu ◽  
Xiang Xu ◽  
Zhihao Zhao ◽  
Minjie Wang ◽  
Jie Zhang
Keyword(s):  
Selective Laser Sintering ◽  
Polarized Light ◽  
Chain Scission ◽  
High Energy ◽  
Laser Sintering ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
Content Type ◽  
X Ray ◽  
Polyamide 12

Purpose The purpose of this paper is to investigate the effect of selective laser sintering (SLS) method on morphology and performance of polyamide 12. Design/methodology/approach Crystallization behavior is critical to the properties of semi-crystalline polymers. The crystallization condition of SLS process is much different from others. The morphology of polyamide 12 produced by SLS technology was investigated using scanning electron microscopy, polarized light microscopy, differential scanning calorimetry, X-ray diffraction and wide-angle X-ray diffraction. Findings Too low fill laser power brought about bad fusion of powders, while too high energy input resulted in bad performance due to chain scission of macromolecules. There were three types of crystal in the raw powder material, denoted as overgrowth crystal, ring-banded spherulite and normal spherulite. Originality/value In this work, SLS samples with different sintering parameters, as well as compression molding sample for the purpose of comparison, were made to study the morphology and crystal structure of sintered PA12 in detail.

Effect of titanium doping on the compositional homogeneity of hollow glass microsphere

2017 ◽  
Vol 458 ◽  
pp. 52-60 ◽  
Author(s):  
Fang Li ◽  
Jing Li ◽  
Jianhong Feng ◽  
Zhanwen Zhang ◽  
Meifang Liu ◽  
...  
Keyword(s):  
Glass Microsphere ◽  
Hollow Glass Microsphere ◽  
Hollow Glass ◽  
Titanium Doping ◽  
Compositional Homogeneity

Loading Effect of Hollow Glass Microsphere (HGM) and Foam Microstructure on the Specific Mechanical Properties and Water Absorption of Syntactic Foam Composite

2021 ◽  
Vol 56 ◽  
pp. 34-50
Author(s):  
Olusegun Adigun Afolabi ◽  
Krishnan Kanny ◽  
Turup Mohan
Keyword(s):  
Water Absorption ◽  
Volume Fraction ◽  
Syntactic Foam ◽  
Density Variation ◽  
Absorption Capacity ◽  
Neat Epoxy ◽  
Hollow Glass Microsphere ◽  
Hollow Glass ◽  
Marine Application ◽  
Foam Composite

AbstractEpoxy syntactic foams (SF) filled with hollow glass microspheres (HGM) were prepared by simple resin casting method and characterization in this study. The effect of varying the amount of HGM on the specific mechanical and water absorption properties of SF composites were investigated. Five different composition of SF (SFT60-0.5 to SFT60-2.5) were compared with the neat epoxy matrix. The wall thickness of the microballoons differ because of its different percentile size distribution (10th, 50th and 90th), which reflects in its density variation. The results show that the specific tensile and flexural strength increases with an increasing filler (HGM) content. The density of SF filled with HGM reduces with increasing volume fraction of filler content. Scanning electron microscopy was done on the failed samples to examine the fractured surfaces. The water absorption capacity of the SF was also investigated as it relates to the HGM volume fraction variation. All the syntactic foam composition shows a better diffusion coefficient capacity than the neat epoxy resin. This makes it applicable in structural purposes and several marine application products such as Autonomous Ultimately Vehicle (AUV).

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