scholarly journals On rheological, mechanical, thermal, wear and morphological properties of melamine formaldehyde reinforced recycled ABS for sustainable manufacturing

2021 ◽  
Vol 309 ◽  
pp. 01081
Author(s):  
Gulraj Singh ◽  
Gurinder Singh Brar ◽  
Rupinder Singh
Keyword(s):  
Thermal Stability ◽  
Heat Capacity ◽  
Wear Behavior ◽  
Minimum Weight ◽  
Morphological Properties ◽  
Flow Index ◽  
Fused Deposition Modelling ◽  
Melamine Formaldehyde ◽  
Fused Deposition ◽  
Thermal Wear

This study outline the procedure of filament fabrication for fused deposition modelling (FDM), based upon rheological, mechanical, thermal, wear and morphological characterization as a case study of acrylonitrile butadiene styrene (ABS) - melamine formaldehyde (MF) composite. It has been ascertained that with increase in proportion of MF in ABS, viscosity is improved and melt flow index (MFI) is reduced significantly. As regards to the wear behavior is concerned it has been observed that ABS-MF (12.5 wt.%) composite has shown minimum weight loss and porosity. For the mechanical properties of the composite, experimental results show increased brittleness of the samples with addition of MF reinforcement. The thermal stability analysis was performed using differential scanning calorimetry (DSC) for virgin ABS and samples having 12.5% MF in ABS and results show the increased heat capacity of the material with increase in MF percentage. Further for sustainability analysis (based upon thermal stability), matrix of ABS-MF12.5% was subjected to three repeated thermal (heating-cooling) cycles and it has been ascertained that no significant loss was noticed in heat capacity of recycled composite matrix. The results are also supported by Fourier transform infrared spectroscopy (FTIR) analysis. Overall the results of the rheological, mechanical, wear, morphological and thermal properties suggested that 12.5% proportion of MF can be reinforced into selected grade of ABS thermoplastic for 3D printing as a sustainable solution.

Comparison of mechanical and morphological properties of 3-D printed functional prototypes: Multi and hybrid blended thermoplastic matrix

2020 ◽  
pp. 089270572092513 ◽  
Author(s):  
Sudhir Kumar ◽  
Rupinder Singh ◽  
TP Singh ◽  
Ajay Batish
Keyword(s):  
Fused Deposition Modeling ◽  
Melt Flow Index ◽  
Tensile Specimen ◽  
Morphological Properties ◽  
Flow Index ◽  
Fused Deposition ◽  
Type Iv ◽  
Deposition Modeling ◽  
American Society ◽  
Functional Prototype

This article reports the comparison for mechanical and morphological properties of 3-D printed tensile specimen with fused deposition modeling by using multiblended and hybrid blended polylactic acid (PLA) matrix. The multiblended PLA matrix was 3-D printed as tensile specimen (as per American Society for Testing and Materials 638 type IV) comprising of 06 layers (01 layer PLA + 01 layer of PLA + polyvinyl chloride + 02 layers of PLA + wood powder + 02 layers of PLA + Fe3O4) each with layer thickness of 0.53 mm. The hybrid blended PLA matrix was also 3-D printed with similar dimensions and printing conditions. The composition/proportion of hybrid blended and multimaterial blended matrix has been selected on the basis of similar melt flow index (MFI) range and the final matrix was compared on basis of equal number of layers (06), similar rheological range (MFI: 40–45 g/10 min) and volume of product (same dimension of prototype). The results of study suggested that the 3-D printed functional prototype of multiblended PLA matrix has better mechanical and morphological properties than hybrid blended PLA matrix. The peak strength and break strength of hybrid blend-based prototype were observed to be 29.56 MPa and 26.60 MPa, respectively, whereas for the multimaterial-based functional prototypes, it was 46.28 MPa and 41.65 MPa, respectively. The results are also supported with scanning electron microscopy-based images, 3-D rendered images, and energy-dispersive X-ray analysis analysis.

Thermomechanical investigations of PEKK-HAp-CS composites

2019 ◽  
Vol 233 (11) ◽  
pp. 1196-1203
Author(s):  
Rupinder Singh ◽  
Gurchetan Singh ◽  
Jaskaran Singh ◽  
Ranvijay Kumar ◽  
Md Mustafizur Rahman ◽  
...  
Keyword(s):  
Melt Flow Index ◽  
Extrusion Process ◽  
Flow Index ◽  
Fused Deposition Modelling ◽  
Index Test ◽  
Melt Flow ◽  
Scanning Calorimetry ◽  
Fused Deposition ◽  
Ether Ketone ◽  
Input Variables

In this experimental study, a composite of poly-ether-ketone-ketone by reinforcement of hydroxyapatite and chitosan has been prepared for possible applications as orthopaedic scaffolds. Initially, different weight percentages of hydroxyapatite and chitosan were reinforced in the poly-ether-ketone-ketone matrix and tested for melt flow index in order to check the flowability of different compositions/proportions. Suitable compositions revealed by the melt flow index test were then taken forward for the extrusion of filament required for fused deposition modelling. For thermomechanical investigations, Taguchi-based design of experiments has been used with input variables in the extrusion process as follows: temperature, load applied and different composition/proportions. The specimens in the form of feedstock filament produced by the extrusion process were made to undergo tensile testing. The specimens were also inspected by differential scanning calorimetry and photomicrographs. Finally, the specimen showing the best performance from the thermomechanical viewpoint has been selected to extrude the filament for the fused deposition modelling process.

scholarly journals A Study on Melt Flow Index on Copper-ABS for Fused Deposition Modeling (FDM) Feedstock

2015 ◽  
Vol 773-774 ◽  
pp. 8-12 ◽  
Author(s):  
Noor Mu'izzah Ahmad Isa ◽  
Nasuha Sa'ude ◽  
M. Ibrahim ◽  
Saiful Manar Hamid ◽  
Khairu Kamarudin
Keyword(s):  
Injection Molding ◽  
Fused Deposition Modeling ◽  
Acrylonitrile Butadiene Styrene ◽  
Melt Flow Index ◽  
Internal Force ◽  
Flow Index ◽  
Fused Deposition Modelling ◽  
Melt Flow ◽  
Volume Percentage ◽  
Fused Deposition

This paper presents of Polymer Matrix Composite (PMC) as feedstock used in Fused Deposition Modelling (FDM) machine. This study discussed on the development of a new PMC material by the injection molding machine. The material consist of copper powder filled in an acrylonitrile butadiene styrene (ABS), binder and surfactant material. The effect of metal filled in ABS and binder content was investigated experimentally by the Melt Flow Index (MFI) machine. Based on the result obtained, an increment of copper filled in ABS by volume percentage (vol. %) effected on melt flow index results. With highly filled copper in PMC composites increase the melt flow index results. It was concluded that, the propensity of the melt flow allow an internal force in PMC material through the injection molding and FDM machine.

scholarly journals INVESTIGATIONS FOR ENHANCING THE APPLICATION DOMAIN OF FUSED DEPOSITION MODELLING PROCESS

2017 ◽  
Vol 46 (1) ◽  
pp. 36-40
Author(s):  
Rupinder Singh ◽  
Sunpreet Singh
Keyword(s):  
Signal To Noise Ratio ◽  
Research Work ◽  
Melt Flow Index ◽  
Flow Index ◽  
Fused Deposition Modelling ◽  
Application Domain ◽  
Melt Flow ◽  
Recent Past ◽  
Fused Deposition ◽  
Modelling Process

In the recent past, various studies have been reported on the development of in-house fused deposition modelling (FDM) filament, in order to increase the application domain of the process. But hitherto very less have reported on the effect of reinforcement type (such as: SiC, Al2O3 and Fe powder etc.) on the melt flow index (MFI) of the polymer matrix composite (PMC) to be used as FDM filament. In the present research work, an effort has beenmade to investigate the effect of selected proportions of filler, matrix (nylon-6) and extrusion load on the MFI of reinforced FDM filament. Experimental study was conducted on melt flow indexer (MFIer) as per ASTM-D1238-95 standard and signal to noise ratio was calculated to find out the effect of input process parameters on MFI of hybrid filament. It has been found that proportion of filler in matrix, type of filler material and extrusion load contributed about 16.62%, 1.23% and 76.72% respectively.

Synergistic effect of glass bead and glass fiber on the crystalline structure, thermal stability, and mechanical, rheological, and morphological properties of polyamide 6 composites

2021 ◽  
pp. 002199832110541
Author(s):  
Emel Kuram
Keyword(s):  
Thermal Stability ◽  
Impact Strength ◽  
Glass Fiber ◽  
Crystalline Structure ◽  
Glass Bead ◽  
Hybrid Composites ◽  
Melt Flow Index ◽  
Polyamide 6 ◽  
Morphological Properties ◽  
Flow Index

The effect of filler amount and kind on the crystalline structure, thermal stability, and mechanical, rheological, and morphological properties of polyamide 6 (PA6) was studied in this research. Glass bead and glass fiber were chosen as mineral fillers. They were incorporated to PA6 solely or in mixed formulations at different proportions (hybrid composites). Tensile strain, tensile strength, impact strength, flexural strain, flexural strength, melt flow index, crystallite size, and thermal degradation parameters were determined for all composites. The addition of glass bead or glass fiber increased the brittleness of pure PA6. The incorporation of glass fiber to pure PA6 improved flexural, impact, and tensile strengths, and mixing of glass bead with pure PA6 polymer caused deterioration of both (tensile and flexural) strengths, but enhanced impact strength. Among hybrid composites, the highest flexural, tensile, and impact strength values were achieved with 15 wt% glass bead and 15 wt% glass fiber content. The addition of glass bead and/or glass fiber to PA6 polymer caused a decrement in melt flow index value. X-ray diffraction results indicated that pure PA6 polymer had α- and γ-crystalline forms, and the reinforcement of glass bead or glass fiber would induce the crystallization into γ-form. It was also found that the incorporation of glass bead or glass fiber influenced the lamellar thickness, and pure PA6 gave thicker lamellar crystal than that of glass bead/fiber-reinforced PA6 and its hybrid composites. Higher thermal stability with glass bead or glass fiber incorporation was found as compared to pure PA6 polymer.

scholarly journals Extrusion-Based 3D Printing of CuSn10 Bronze Parts: Production and Characterization

Metals ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1774
Author(s):  
Ahmet Çağrı Kılınç ◽  
Ali Aydın Goktasş ◽  
Özgür Yasin Keskin ◽  
Serhan Köktaş
Keyword(s):  
3D Printing ◽  
Layer Thickness ◽  
Sintering Temperature ◽  
Cost Effective ◽  
Morphological Properties ◽  
Fused Deposition Modelling ◽  
Fused Deposition ◽  
3D Printed ◽  
Part Density ◽  
Printing Speed

The interest in producing cost-effective 3D printed metallic materials is increasing day by day. One of these methods, which has gained much attention recently, is the fused deposition modelling (FDM) method. The parameters used in the FDM method have significant effects on the printed part properties. In this study, CuSn10 bronze alloy was successfully produced. The printing speed and layer thickness were investigated as the printing process parameters, and their effect on morphological properties was characterized by using SEM. As a result, it was observed that the formation of printing-induced voids was prevented by applying a layer thickness of 0.2 mm. Additionally, by increasing printing speed, a slight decrease in product density was observed. Following determination of 3D printing parameters which give the highest printed part density, the parts were debound in hexane solution via solvent debinding. Finally, the parts were sintered at 850, 875 and 900 °C for 5 h to examine effect of sintering temperature on density, porosity, shape deformation and mechanical properties. Although partial slumping started to form over 875 °C, the highest density (94.19% of theoretical density) and strength (212 ± 17.72 MPa) were obtained by using 900 °C as the sintering temperature.

Investigations for tensile, compressive and morphological properties of 3D printed functional prototypes of PLA-PEKK-HAp-CS

2019 ◽  
pp. 089270571987059 ◽  
Author(s):  
Rupinder Singh ◽  
Gurchetan Singh ◽  
Jaskaran Singh ◽  
Ranvijay Kumar
Keyword(s):  
Polylactic Acid ◽  
Design Of Experiment ◽  
Morphological Properties ◽  
Experimental Investigations ◽  
Fused Deposition Modelling ◽  
Fused Deposition ◽  
Type Iv ◽  
3D Printed ◽  
Ether Ketone

This article reports the experimental investigations for tensile, compressive and morphological properties of 3D printed functional prototypes composed of polylactic acid (PLA) reinforced with poly ether ketone ketone (PEKK), hydroxyapatite (HAp) and chitosan (CS). The PLA-PEKK-HAp-CS composite has wide applications as scaffolds in orthopaedics and clinical dentistry. The tensile and compressive specimens were printed (as per ASTM D638 type IV and ASTM D695) with in-house prepared feedstock filament on commercial fused deposition modelling setup by following Taguchi-based design of experiment. The results are also supported by hardness data and photomicrographs.

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