scholarly journals Ellipsometry as an express method for determining the pore parameters of ion-track SiO2 templates on a silicon substrate

2019 ◽  
Vol 201 ◽  
pp. 01001 ◽  
Author(s):  
Victoria Bundyukova ◽  
Egor Kaniukov ◽  
Alena Shumskaya ◽  
Andrey Smirnov ◽  
Maksim Kravchenko ◽  
...  

Due to the effective development of ion-track technology, it became possible to produce porous templates with large areas, which are of interest for mass production of nanostructures. Given that the template parameters often define properties of the resulting nanostructures and nanosystems, a reliable method for non-destructive testing is needed for a rapid control of template parameters. Such method could be ellipsometry, allowing for a single measurement to collect statistical information from a large area and to save time for certification. In order to adapt the ellipsometry method for controlling the parameters of ion-track patterns, the first studies of SiO2/Si templates with low porosity were carried out. Using the standard model of the interaction of a polarized light beam with a layered structure of silicon oxide on silicon, the basic parameters of the pores were determined by means of mathematical transformations and subsequently compared with the results of scanning electron microscopy.

2021 ◽  
Vol 26 (3) ◽  
Author(s):  
Andrii M. Bozhuk ◽  
Serhii Rostyslavovych Mikhailov ◽  
Olexandr R. Trofymenko

Research of objects with unilateral access is a promising area for the development of non-destructive testing systems. To create a real system and determine its optimal parameters, it is important to conduct preliminary computer simulations. The paper is devoted to creating a model of a non-destructive system based on backscattered X-rays in the Serpent Monte Carlo code. There are no known studies of the use of Serpent software to build such models. The purpose of the study was to confirm the possibility of detecting a defect, i.e., a material of a different density than the test object, which was placed in this object. A model was created, the main components of which were the radiation source, the object under study, the defect, and the detector of backscattered radiation. Experiments were performed for several combinations of system parameters, in particular when changing the angle of illumination and the distance between the object and the detector. The energy of the radiation source used in the study was 100 keV. The test object of study was a steel plate, which contained a defect — a lead plate. Calculations were performed for six cases at illumination angles of 30 and 45 degrees (scattering angles of 120 and 135 degrees, respectively), and the distance between the object and the detector 1 and 5 cm. The detector was a plane that coincided with a NaI scintillation plate of 60 by 30 cm in size. It was conventionally divided into 1800 elements to detect the flux density of backscattered radiation. A qualitative and quantitative analysis of the results met theoretical expectations. In particular, the Compton equation was fulfilled, which states that as the cosine of the scattering angle \theta increases, the energy of scattered radiation also increases. In the case of θ = 1200, the average flux density of backscattered radiation recorded by the detector was 1.1*10-3 units per square centimeter per second, and in the case of θ = 1350, this value was 7.9*10-4. The results of the study can be used to build real non-destructive testing devices. These devices can be used in medicine, industry, and security systems. The model has some limitations. The radiation source in this model is monoenergetic, in contrast to classical X-ray systems, in which the radiation has a spectrum. Also, a defect is a plate of a large area, which is almost equal to the area of ​​the object under study. For practical use, the device must be capable to detect a defect many times smaller than the object under study, such as a void in the weld, a tumor in the human body, or smuggled substances. The model can be improved in the future.


2013 ◽  
Vol 64 (2) ◽  
pp. 21001 ◽  
Author(s):  
Jean-Luc Bodnar ◽  
Jean-Jacques Metayer ◽  
Kamel Mouhoubi ◽  
Vincent Detalle

2020 ◽  
pp. 54-59
Author(s):  
A. A. Yelizarov ◽  
A. A. Skuridin ◽  
E. A. Zakirova

A computer model and the results of a numerical experiment for a sensitive element on a planar mushroom-shaped metamaterial with cells of the “Maltese cross” type are presented. The proposed electrodynamic structure is shown to be applicable for nondestructive testing of geometric and electrophysical parameters of technological media, as well as searching for inhomogeneities in them. Resonant frequency shift and change of the attenuation coefficient value of the structure serve as informative parameters.


2015 ◽  
Vol 7 (2) ◽  
pp. 1428-1439
Author(s):  
Khurshed Alam ◽  
Md. Sayeedur Rahman ◽  
Md. Mostafizur Rahman ◽  
S. M. Azaharul Islam

A powerful non-destructive testing (NDT) technique is adopted to study the internal defects and elemental distribution/homogeneity and porosity of aerated brick and EPS aggregate poly brick samples. In the present study the internal defects like homogeneity, porosity, elemental distribution, EPS aggregate and aerator distributor in the test samples have been observed by the measurement of gray value/optical density of the neutron radiographic images of these samples. From this measurement it is found that the neutron intensity/optical density variation with the pixel distance of the AOI of the NR images in both expanded polystyrene (EPS) aggregate poly brick and aerated brick samples comply almost same in nature with respect to the whole AOI but individually each AOI shows different nature from one AOI to another and it confirms that the elemental distribution within a AOI is almost homogeneous. Finally it was concluded that homogeneity, elemental distribution in the EPS aggregate poly brick sample is better than that of the aerated brick sample. 


2020 ◽  
Vol 2020 (1) ◽  
pp. 34-52
Author(s):  
Rafał Szymański

AbstractThe article is in line with the contemporary interests of companies from the aviation industry. It describes thermoplastic material and inspection techniques used in leading aviation companies. The subject matter of non-destructive testing currently used in aircraft inspections of composite structures is approximated and each of the methods used is briefly described. The characteristics of carbon preimpregnates in thermoplastic matrix are also presented, as well as types of thermoplastic materials and examples of their application in surface ship construction. The advantages, disadvantages and limitations for these materials are listed. The focus was put on the explanation of the ultrasonic method, which is the most commonly used method during the inspection of composite structures at the production and exploitation stage. Describing the ultrasonic method, the focus was put on echo pulse technique and the use of modern Phased Array heads. Incompatibilities most frequently occurring and detected in composite materials with thermosetting and thermoplastic matrix were listed and described. A thermoplastic flat composite panel made of carbon pre-impregnate in a high-temperature matrix (over 300°C), which was the subject of the study, was described. The results of non-destructive testing (ultrasonic method) of thermoplastic panel were presented and conclusions were drawn.


Sign in / Sign up

Export Citation Format

Share Document