scholarly journals Image-plate sensitivity to x rays at 2 to 60 keV

2019 ◽  
Vol 90 (1) ◽  
pp. 013506 ◽  
Author(s):  
M. J. Rosenberg ◽  
D. B. Thorn ◽  
N. Izumi ◽  
D. Williams ◽  
M. Rowland ◽  
...  
Keyword(s):  
X Rays ◽  
Image Plate

Characterization of image plates for neutron diffraction

2009 ◽  
Vol 42 (5) ◽  
pp. 749-757 ◽  
Author(s):  
Clive Wilkinson ◽  
Mogens S. Lehmann ◽  
Flora Meilleur ◽  
Matthew P. Blakeley ◽  
Dean A. A. Myles ◽  
...  
Keyword(s):  
Point Spread Function ◽  
X Rays ◽  
Image Plate ◽  
Point Spread ◽  
Spread Function ◽  
Luminescent Signal ◽  
Diffraction Patterns ◽  
Integrated Intensities ◽  
Ccd Detectors ◽  
Lower Limits

A method to measure the overall gain and point-spread function of an image-plate detector system (converter, phosphor, readout electronics) online from single-crystal diffraction patterns is derived. Only with a knowledge of these quantities can one estimate without bias the true standard deviations of the observed integrated intensities of Bragg reflections measured with such a detector. The gain corrected for the point-spread function should ideally be approximately 1.0 to avoid loss of data or precision due to the upper and lower limits of digitization of the diffraction patterns. The gain and the point-spread function are derived for several configurations of the three neutron Laue image-plate diffractometers, LADI, VIVALDI and LADI-III, at the Institut Laue–Langevin. The detective quantum efficiencies (DQE) of these instruments have been measured to be 0.16 (1), 0.57 (2) and 0.46 (3), respectively. It has also been found that the DQE is effectively constant for different times of exposure, despite the fading of the photostimulated luminescent signal during that time. While the results described in this paper concern neutron detection by image plates, the method is equally valid for other integrating detectors and radiations,e.g.CCD detectors and X-rays.

Problems in measuring diffuse X-ray scattering

2005 ◽  
Vol 220 (12) ◽  
Author(s):  
T. Richard Welberry ◽  
Darren J. Goossens ◽  
Aidan P. Heerdegen ◽  
Peter L. Lee
Keyword(s):  
X Rays ◽  
X Ray ◽  
Image Plate ◽  
X Ray Scattering ◽  
Weak Scattering ◽  
Strong Scattering ◽  
Photon Source ◽  
Image Plate Detector ◽  
Ray Scattering

AbstractProblems encountered in making measurements of diffuse X-ray scattering are discussed. These generally arise from the need to measure very weak scattering in the presence of very strong scattering (Bragg peaks) using multi-detectors of various kinds. The problems are not confined to synchrotron experiments but may even occur using a tube source in the home laboratory. Specific details are given of experiments using 80.725 keV X-rays and a mar345 Image Plate detector on the 1-ID beamline of XOR at the Advanced Photon Source. In these a severe ‘blooming’ artefact which occurred around some strong Bragg peaks was traced to fluorescence from a steel mounting plate in the detector when strong Bragg peaks were incident. Algorithms developed to remove these artefacts from the data are described.

scholarly journals Erratum: “Image-plate sensitivity to x rays at 2 to 60 keV” [Rev. Sci. Instrum. 90, 013506 (2019)]

2019 ◽  
Vol 90 (2) ◽  
pp. 029902
Author(s):  
M. J. Rosenberg ◽  
D. B. Thorn ◽  
N. Izumi ◽  
D. Williams ◽  
M. Rowland ◽  
...  
Keyword(s):  
X Rays ◽  
Image Plate

High-energy X-ray diffuse scattering using Weissenberg flat-cone geometry

2000 ◽  
Vol 33 (4) ◽  
pp. 1046-1050 ◽  
Author(s):  
B. D. Butler ◽  
D. R. Haeffner ◽  
P. L. Lee ◽  
T. R. Welberry
Keyword(s):  
Diffuse Scattering ◽  
High Energy ◽  
Reciprocal Space ◽  
Irregular Shape ◽  
X Rays ◽  
Storage Phosphor ◽  
X Ray ◽  
Image Plate ◽  
X Ray Scattering ◽  
Disordered Crystal

A technique for the measurement of diffuse X-ray scattering on individual reciprocal-space planes using high-energy X-ray photons is described. The method is demonstrated using a disordered crystal of the compound TlSbOGeO4and compared to data collected with a sealed-tube Cu anode source. Measurements were made on a synchrotron undulator beamline at an energy of 45 keV using Weissenberg flat-cone geometry and a storage phosphor (image) plate to detect the scattered X-rays. Advantages of the method include: extension of the accessible diffraction space to both higherandlower wavevectors, the ability to use crystals of irregular shape without the need for complicated absorption corrections, less need to prepare sample surfaces carefully, and the ability to filter fluorescence simply.

Comparison of diffraction intensity using a monocapillary optic and pinhole collimators in a microdiffractometer with a curved image-plate

2002 ◽  
Vol 17 (2) ◽  
pp. 94-98 ◽  
Author(s):  
Paul J. Schields ◽  
Igor Yu. Ponomarev ◽  
Ning Gao ◽  
Richard B. Ortega
Keyword(s):  
Beam Width ◽  
X Rays ◽  
Average Increase ◽  
Diffraction Intensity ◽  
Image Plate ◽  
Integrated Intensity ◽  
Diffraction Peaks ◽  
Diffraction Patterns ◽  
Image Plate System ◽  
Pinhole Collimators

The performance of a tapered, monocapillary optic was compared to double-pinhole optics by measuring the intensity and widths of powder diffraction peaks generated using Cr Kα and Cu Kα X-rays (46 kV, 46 mA). A microdiffractometer and curved image-plate system was used to collect diffraction patterns displayed by an alumina intensity standard. A monocapillary optic with a 20 μm beam width (measured at half the maximum intensity, FWHM) was compared to collimating pinhole optics with two apertures: one with 30 μm diameter pinholes and another with 50 μm pinholes. The average, integrated intensity of the diffraction peaks in the patterns collected using the 20 μm monocapillary optic was 6 to 7 times greater than the average diffraction intensity obtained with the 50 μm pinhole collimator and 25 times greater than the intensity obtained with the 30 μm collimator. The average increase in the FWHM of the diffraction peaks in the patterns obtained with the monocapillary optic was ∼2 times greater than the pinhole collimators.

White-Light Coronal Structures: Streamers and CMEs

1994 ◽  
Vol 144 ◽  
pp. 82
Author(s):  
E. Hildner
Keyword(s):  
Emission Line ◽  
Electron Density ◽  
White Light ◽  
Coronal Mass Ejections ◽  
X Rays ◽  
Solar Cycles ◽  
Temperature Function ◽  
X Ray ◽  
Eclipse Observations ◽  
Coronal Structures

AbstractOver the last twenty years, orbiting coronagraphs have vastly increased the amount of observational material for the whitelight corona. Spanning almost two solar cycles, and augmented by ground-based K-coronameter, emission-line, and eclipse observations, these data allow us to assess,inter alia: the typical and atypical behavior of the corona; how the corona evolves on time scales from minutes to a decade; and (in some respects) the relation between photospheric, coronal, and interplanetary features. This talk will review recent results on these three topics. A remark or two will attempt to relate the whitelight corona between 1.5 and 6 R⊙to the corona seen at lower altitudes in soft X-rays (e.g., with Yohkoh). The whitelight emission depends only on integrated electron density independent of temperature, whereas the soft X-ray emission depends upon the integral of electron density squared times a temperature function. The properties of coronal mass ejections (CMEs) will be reviewed briefly and their relationships to other solar and interplanetary phenomena will be noted.

Emergence of Twisted Magnetic Flux Related Sigmoidal Brightening

2000 ◽  
Vol 179 ◽  
pp. 263-264
Author(s):  
K. Sundara Raman ◽  
K. B. Ramesh ◽  
R. Selvendran ◽  
P. S. M. Aleem ◽  
K. M. Hiremath
Keyword(s):  
Magnetic Field ◽  
Magnetic Fields ◽  
Magnetic Flux ◽  
Ultra Violet ◽  
Active Regions ◽  
Morphological Properties ◽  
Energy Storage And Conversion ◽  
The Sun ◽  
X Rays ◽  
The Magnetic Field

Extended AbstractWe have examined the morphological properties of a sigmoid associated with an SXR (soft X-ray) flare. The sigmoid is cospatial with the EUV (extreme ultra violet) images and in the optical part lies along an S-shaped Hαfilament. The photoheliogram shows flux emergence within an existingδtype sunspot which has caused the rotation of the umbrae giving rise to the sigmoidal brightening.It is now widely accepted that flares derive their energy from the magnetic fields of the active regions and coronal levels are considered to be the flare sites. But still a satisfactory understanding of the flare processes has not been achieved because of the difficulties encountered to predict and estimate the probability of flare eruptions. The convection flows and vortices below the photosphere transport and concentrate magnetic field, which subsequently appear as active regions in the photosphere (Rust & Kumar 1994 and the references therein). Successive emergence of magnetic flux, twist the field, creating flare productive magnetic shear and has been studied by many authors (Sundara Ramanet al.1998 and the references therein). Hence, it is considered that the flare is powered by the energy stored in the twisted magnetic flux tubes (Kurokawa 1996 and the references therein). Rust & Kumar (1996) named the S-shaped bright coronal loops that appear in soft X-rays as ‘Sigmoids’ and concluded that this S-shaped distortion is due to the twist developed in the magnetic field lines. These transient sigmoidal features tell a great deal about unstable coronal magnetic fields, as these regions are more likely to be eruptive (Canfieldet al.1999). As the magnetic fields of the active regions are deep rooted in the Sun, the twist developed in the subphotospheric flux tube penetrates the photosphere and extends in to the corona. Thus, it is essentially favourable for the subphotospheric twist to unwind the twist and transmit it through the photosphere to the corona. Therefore, it becomes essential to make complete observational descriptions of a flare from the magnetic field changes that are taking place in different atmospheric levels of the Sun, to pin down the energy storage and conversion process that trigger the flare phenomena.

The Clinical, Roentgenological and Morphological Effects of an Acute Exposure of Phosgene on the Lungs of Dogs

1971 ◽  
Vol 29 ◽  
pp. 236-237
Author(s):  
R. F. Bils ◽  
W. F. Diller ◽  
F. Huth
Keyword(s):  
Latent Period ◽  
Chemical Industry ◽  
Toxic Substance ◽  
Lung Edema ◽  
X Rays ◽  
Beagle Dogs ◽  
Male And Female ◽  
Morphological Alterations ◽  
Before And After ◽  
Electron Microscopes

Phosgene still plays an important role as a toxic substance in the chemical industry. Thiess (1968) recently reported observations on numerous cases of phosgene poisoning. A serious difficulty in the clinical handling of phosgene poisoning cases is a relatively long latent period, up to 12 hours, with no obvious signs of severity. At about 12 hours heavy lung edema appears suddenly, however changes can be seen in routine X-rays taken after only a few hours' exposure (Diller et al., 1969). This study was undertaken to correlate these early changes seen by the roengenologist with morphological alterations in the lungs seen in the'light and electron microscopes.Forty-two adult male and female Beagle dogs were selected for these exposure experiments. Treated animals were exposed to 94.5-107-5 ppm phosgene for 10 min. in a 15 m3 chamber. Roentgenograms were made of the thorax of each animal before and after exposure, up to 24 hrs.

Chemical Species Identification in an SEM by Changes in Emitted X-Ray Energies

1974 ◽  
Vol 32 ◽  
pp. 570-571
Author(s):  
R. H. Duff
Keyword(s):  
Species Identification ◽  
Valence Electron ◽  
Chemical Species ◽  
X Rays ◽  
Chemical Bonds ◽  
Small Shift ◽  
X Ray ◽  
Electron Transitions ◽  
Peak Energy ◽  
Chemical Combination

A material irradiated with electrons emits x-rays having energies characteristic of the elements present. Chemical combination between elements results in a small shift of the peak energies of these characteristic x-rays because chemical bonds between different elements have different energies. The energy differences of the characteristic x-rays resulting from valence electron transitions can be used to identify the chemical species present and to obtain information about the chemical bond itself. Although these peak-energy shifts have been well known for a number of years, their use for chemical-species identification in small volumes of material was not realized until the development of the electron microprobe.

Influence of X-Ray Induced Fluorescence on Energy Dispersive X-Ray Analysis of Thin Foils

1977 ◽  
Vol 35 ◽  
pp. 328-329
Author(s):  
E. A. Kenik ◽  
J. Bentley
Keyword(s):  
Thin Foil ◽  
Electron Excitation ◽  
Simple Approach ◽  
Foil Thickness ◽  
X Rays ◽  
X Ray ◽  
Hole Spectrum ◽  
Illumination System ◽  
Thin Foils ◽  
Intensity Ratios

Cliff and Lorimer (1) have proposed a simple approach to thin foil x-ray analy sis based on the ratio of x-ray peak intensities. However, there are several experimental pitfalls which must be recognized in obtaining the desired x-ray intensities. Undesirable x-ray induced fluorescence of the specimen can result from various mechanisms and leads to x-ray intensities not characteristic of electron excitation and further results in incorrect intensity ratios.In measuring the x-ray intensity ratio for NiAl as a function of foil thickness, Zaluzec and Fraser (2) found the ratio was not constant for thicknesses where absorption could be neglected. They demonstrated that this effect originated from x-ray induced fluorescence by blocking the beam with lead foil. The primary x-rays arise in the illumination system and result in varying intensity ratios and a finite x-ray spectrum even when the specimen is not intercepting the electron beam, an ‘in-hole’ spectrum. We have developed a second technique for detecting x-ray induced fluorescence based on the magnitude of the ‘in-hole’ spectrum with different filament emission currents and condenser apertures.

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