Measurement of the stacking-fault energy of gold using the weak-beam technique of electron microscopy

1972 ◽  
Vol 26 (3) ◽  
pp. 747-751 ◽  
Author(s):  
M. L. Jenkins

The weak-beam method of electron microscopy (Cockayne, Ray & Whelan 1969, 1970) has been used to investigate the dissociation of dislocations in silicon. Total dislocations with a/2<110> Burgers vectors were found to be dissociated into Shockley partial dislocations, with a separation of 7.5 +0.6 nm (75 + 6 Å) for the pure edge orientation and 4.1 +0.6 nm (41+ 6 Å) for the pure screw orientation. The intrinsic stacking-fault energy, calculated from the measured dissociation width using anisotropic elasticity theory, is 51 + 5 mJ m -2 (51 + 5 erg cm -2 ). The method has also been used to image partial dislocations at threefold dislocation nodes in silicon. All nodes in the specimens examined were found to be extended, and of about the same size, indicating that the intrinsic and extrinsic stacking-fault energies are comparable. Measurements of the radii of curvature of partial dislocations at the nodes gave a value of 50+15 mJ m -2 (50+15 erg cm -2 ) for the intrinsic stacking fault energy, using the method of Whelan (1959) as modified by Brown & Thölén (1964). Dislocations in silicon specimens annealed at a high temperature were found to be constricted along segments of the dislocation line. Evidence is presented which suggests that the constricted segments have climbed out of the slip plane.


Weak-beam electron microscopy has been applied to study the dissociation of dislocations in a type II a diamond. Dislocations with Burgers vector ½[11̅0] on (111) glide planes have been found to be dissociated into two Shockley partials, with separations between 2.5 and 4.3 nm, and extended nodes and dissociated dipoles have also been observed. The stacking fault energy has been determined from the mean and distribution of the separ­ations of the partials to be 279 ± 41 mJ m -2 . The behaviour of dislocations in diamond appears to be similar to that of dislocations in Ge and Si.


Author(s):  
K. Z. Botros ◽  
S. S. Sheinin

The main features of weak beam images of dislocations were first described by Cockayne et al. using calculations of intensity profiles based on the kinematical and two beam dynamical theories. The feature of weak beam images which is of particular interest in this investigation is that intensity profiles exhibit a sharp peak located at a position very close to the position of the dislocation in the crystal. This property of weak beam images of dislocations has an important application in the determination of stacking fault energy of crystals. This can easily be done since the separation of the partial dislocations bounding a stacking fault ribbon can be measured with high precision, assuming of course that the weak beam relationship between the positions of the image and the dislocation is valid. In order to carry out measurements such as these in practice the specimen must be tilted to "good" weak beam diffraction conditions, which implies utilizing high values of the deviation parameter Sg.


Further experiments by transmission electron microscopy on thin sections of stainless steel deformed by small amounts have enabled extended dislocations to be observed directly. The arrangement and motion of whole and partial dislocations have been followed in detail. Many of the dislocations are found to have piled up against grain boundaries. Other observations include the formation of wide stacking faults, the interaction of dislocations with twin boundaries, and the formation of dislocations at thin edges of the foils. An estimate is made of the stacking-fault energy from a consideration of the stresses present, and the properties of the dislocations are found to be in agreement with those expected from a metal of low stacking-fault energy.


1981 ◽  
Vol 66 (2) ◽  
pp. 425-429 ◽  
Author(s):  
M. K. Agarwal ◽  
J. V. Patel ◽  
N. G. Patel

1967 ◽  
Vol 45 (2) ◽  
pp. 787-795 ◽  
Author(s):  
A. W. Ruff Jr. ◽  
L. K. Ives

Direct measurements by transmission electron microscopy on extended dislocation nodes in alloys of tin in silver have led to values for the intrinsic stacking-fault energy. The values decreased smoothly from 23 erg/cm2 for pure silver to 4.2 erg/cm2 for 7.8 at.% tin. The results are compared with previous determinations in other silver-base alloys.


Author(s):  
C.B. Carter ◽  
D. Cherns ◽  
P.B. Hirsch ◽  
H. Saka

The mechanism of climb of dissociated dislocations in f.c.c. metals and alloys is not well understood. Climb of dislocations by absorption or emission of vacancies at existing jogs in dissociated dislocations has been observed using the “weak-beam” technique of electron microscopy, but the mechanism of nucleation of jogs is not clear. In this paper we report some results of experiments designed to study the nucleation problem, and more generally the mechanism of absorption of point defects under conditions of high supersaturation.Thin (111) sections of deformed single crystals of Cu-Al alloys, of various compositions, have been electron irradiated in an AEI EM7 HVEM up to 1 MeV, either at room temperature, or elevated temperatures up to 200°C, using a goniometer heating stage. Observations under weak beam conditions have been made a) in situ in the HVEM b) at 100kV in an JEM100B, following irradiation in the HVEM. Interstitials produced by the irradiation are expected to be preferentially attracted to the dislocations because of the strong dislocation-interstitial interaction.


1989 ◽  
Vol 03 (17) ◽  
pp. 1359-1362 ◽  
Author(s):  
FANG LIU ◽  
HUI GU ◽  
TIAN XIAO LIN ◽  
JIN LONG ZHANG ◽  
GUANG CHENG XIONG ◽  
...  

Transmission electron microscopy (TEM) shows that the dislocation on basal plane (001) of high T c BiSrCaCuO can dissociate into 2 partials of the type [Formula: see text]. The related stacking fault energy is estimated of the order about µb/365 similar to that observed in Cu and implication of this finding has been discussed.


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