Charles Glover Barkla, 1877-1944

1947 ◽  
Vol 5 (15) ◽  
pp. 341-366 ◽  

The name of Barkla will always be distinguished on account of his fundamental researches on Rontgen rays. In 1905 he made the discovery that scattered X-rays are polarized, but only to a certain degree. He also established the fact that each chemical element can radiate Röntgen rays having properties characteristic of that element, and in this way he anticipated the assignment to each element of an ‘atomic number’, the number being, in general, about one-half the atomic weight. For these discoveries he was admitted a Fellow of the Society in 1912, his investigations having resulted in the most important additions to our knowledge of the Röntgen rays since their discovery. Barkla consistently adopted the electromagnetic wave or pulse theory of the nature of the rays. At the end of the year 1912, von Laue put forward his theory of the diffraction of X-rays by transmission through a crystal regarded as a three-dimensional grating, thus introducing an entirely new’ method of investigation.

Radiation that, on passage through matter, produces ions by knocking electrons out of their orbits is called ionizing radiation. This radiation is produced through decomposition of unstable, naturally occurring or synthetic elements referred to as radionuclides. The four types of radiation are ∝-particles, β-particles, γ-rays, and neutrons. The ∝-particles have a mass of two protons and two neutrons and a charge of +2; β -particles are electrons with a mass of 0.00055 atomic mass unit (amu) and a charge of –1; γ -rays and X-rays are high-frequency electromagnetic waves with no mass and no charge. The difference between γ -rays and X-rays is that γ -rays occur naturally, whereas X-rays are generated. In addition, γ -rays are of higher frequency than X-rays. Release of an ∝ -particle leads to the formation of a daughter element with an atomic number 2 units lower and an atomic weight 4 units lower than that of the parent nuclide. Similarly, release of a β -particle from the nucleus causes conversion of a neutron to a proton, producing a daughter element with the same atomic weight as the parent nuclide but with its atomic number increased by 1 unit. Neutron radiation does not occur naturally and is released only from synthetic radionuclides. Neutrons, which have no charge, are formed from protons. This conversion is accompanied by the release of an orbital electron from the atom. Neutrons produce ions indirectly, by collisions with hydrogen atoms. The impact knocks out protons, which in turn produce ions on passage through matter. Capture of a neutron forms an isotope of the parent nuclide with its atomic weight increased by 1 unit. The mode of action of particles (∝ and β ) varies from that of photons (γ - and X-rays). When ∝- or β -particles travel through matter, their electric charges (positive or negative) cause ionization of the atoms in the matter. This is called a direct effect. Whereas the track of ∝- particles is short and straight, β -particles scatter, frequently producing a wavy track. Gamma- and X-rays act indirectly.


Author(s):  
John C. Russ

Three-dimensional (3D) images consisting of arrays of voxels can now be routinely obtained from several different types of microscopes. These include both the transmission and emission modes of the confocal scanning laser microscope (but not its most common reflection mode), the secondary ion mass spectrometer, and computed tomography using electrons, X-rays or other signals. Compared to the traditional use of serial sectioning (which includes sequential polishing of hard materials), these newer techniques eliminate difficulties of alignment of slices, and maintain uniform resolution in the depth direction. However, the resolution in the z-direction may be different from that within each image plane, which makes the voxels non-cubic and creates some difficulties for subsequent analysis.


Author(s):  
Werner P. Rehbach ◽  
Peter Karduck

In the EPMA of soft x rays anomalies in the background are found for several elements. In the literature extremely high backgrounds in the region of the OKα line are reported for C, Al, Si, Mo, and Zr. We found the same effect also for Boron (Fig. 1). For small glancing angles θ, the background measured using a LdSte crystal is significantly higher for B compared with BN and C, although the latter are of higher atomic number. It would be expected, that , characteristic radiation missing, the background IB (bremsstrahlung) is proportional Zn by variation of the atomic number of the target material. According to Kramers n has the value of unity, whereas Rao-Sahib and Wittry proposed values between 1.12 and 1.38 , depending on Z, E and Eo. In all cases IB should increase with increasing atomic number Z. The measured values are in discrepancy with the expected ones.


Polymers ◽  
2021 ◽  
Vol 13 (8) ◽  
pp. 1271
Author(s):  
Andreas Koenig ◽  
Leonie Schmohl ◽  
Johannes Scheffler ◽  
Florian Fuchs ◽  
Michaela Schulz-Siegmund ◽  
...  

The aim of the study was to investigate the effect of X-rays used in micro X-ray computer tomography (µXCT) on the mechanical performance and microstructure of a variety of dental materials. Standardised bending beams (2 × 2 × 25 mm3) were forwarded to irradiation with an industrial tomograph. Using three-dimensional datasets, the porosity of the materials was quantified and flexural strength was investigated prior to and after irradiation. The thermal properties of irradiated and unirradiated materials were analysed and compared by means of differential scanning calorimetry (DSC). Single µXCT measurements led to a significant decrease in flexural strength of polycarbonate with acrylnitril-butadien-styrol (PC-ABS). No significant influence in flexural strength was identified for resin-based composites (RBCs), poly(methyl methacrylate) (PMMA), and zinc phosphate cement (HAR) after a single irradiation by measurement. However, DSC results suggest that changes in the microstructure of PMMA are possible with increasing radiation doses (multiple measurements, longer measurements, higher output power from the X-ray tube). In summary, it must be assumed that X-ray radiation during µXCT measurement at high doses can lead to changes in the structure and properties of certain polymers.


2021 ◽  
Vol 11 (10) ◽  
pp. 4612
Author(s):  
KweonSoo Seo ◽  
Sunjai Kim

Purpose: The aim of this study was to present a new method to analyze the three-dimensional accuracy of complete-arch dental impressions and verify the reliability of the method. Additionally, the accuracies of conventional and intraoral digital impressions were compared using the new method. Methods: A master model was fabricated using 14 milled polyetheretherketone cylinders and a maxillary acrylic model. Each cylinder was positioned and named according to its corresponding tooth position. Twenty-five definitive stone casts were fabricated using conventional impressions of the master model. An intraoral scanner was used to scan the master model 25 times to fabricate 25 digital models. A coordinate measuring machine was used to physically probe each cylinder in the master model and definitive casts. An inspection software was used to probe cylinders of digital models. A three-dimensional part coordinate system was defined and used to compute the centroid coordinate of each cylinder. Intraclass correlation coefficient (ICC) was evaluated to examine the reliability of the new method. Independent two sample t-test was performed to compare the trueness and precision of conventional and intraoral digital impressions (α = 0.05). Results: ICC results showed that, the new method had almost perfect reliability for the measurements of the master model, conventional and digital impression. Conventional impression showed more accurate absolute trueness and precision than intraoral digital impression for most of the tooth positions (p < 0.05). Conclusions: The new method was reliable to analyze the three-dimensional deviation of complete-arch impressions. Conventional impression was still more accurate than digital intraoral impression for complete arches.


Author(s):  
Theodore J. Heindel ◽  
Terrence C. Jensen ◽  
Joseph N. Gray

There are several methods available to visualize fluid flows when one has optical access. However, when optical access is limited to near the boundaries or not available at all, alternative visualization methods are required. This paper will describe flow visualization using an X-ray system that is capable of digital X-ray radiography, digital X-ray stereography, and digital X-ray computed tomography (CT). The unique X-ray flow visualization facility will be briefly described, and then flow visualization of various systems will be shown. Radiographs provide a two-dimensional density map of a three dimensional process or object. Radiographic images of various multiphase flows will be presented. When two X-ray sources and detectors simultaneously acquire images of the same process or object from different orientations, stereographic imaging can be completed; this type of imaging will be demonstrated by trickling water through packed columns and by absorbing water in a porous medium. Finally, local time-averaged phase distributions can be determined from X-ray computed tomography (CT) imaging, and this will be shown by comparing CT images from two different gas-liquid sparged columns.


Author(s):  
Matija Prka ◽  
Albert Despot ◽  
Alemka Brnčić Fischer ◽  
Herman Haller ◽  
Ana Tikvica Luetić ◽  
...  

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