Synthesis and properties of modified PBT for FDM

2017 ◽  
Vol 23 (4) ◽  
pp. 804-810 ◽  
Author(s):  
Shiqing Cao ◽  
Dandan Yu ◽  
Weilan Xue ◽  
Zuoxiang Zeng ◽  
Wanyu Zhu
Keyword(s):  
Mechanical Properties ◽  
Impact Strength ◽  
Fused Deposition Modeling ◽  
Complex Structure ◽  
Three Dimensional ◽  
Sebacic Acid ◽  
Wire Drawing ◽  
Content Type ◽  
Fused Deposition ◽  
Deposition Modeling

Purpose The purpose of this paper is to prepare a new modified polybutylene terephalate (MPBT) for fused deposition modeling (FDM) to increase the variety of materials compatible with printing. And the printing materials can be used to print components with a complex structure and functional mechanical parts. Design/methodology/approach The MPBT, poly(butylene terephalate-co-isophthalate-co-sebacate) (PBTIS), was prepared for FDM by direct esterification and subsequent polycondensation using terephthalic acid (PTA), isophthalic acid (PIA), sebacic acid (SA) and 1,4-butanediol (BDO). The effects of the content of PIA (20-40 mol%) on the mechanical properties of PBTIS were investigated when the mole per cent of SA (αSA) is zero. The effects of αSA (0-7mol%) on the thermal, rheological and mechanical properties of PBTIS were investigated at nPTA/nPIA = 7/3. A desktop wire drawing and extruding machine was used to fabricate the filaments, whose printability and anisotropy were tested by three-dimensional (3D) printing experiments. Findings A candidate content of PIA introducing into PBT was obtained to be about 30 per cent, and the Izod notched impact strength of PBTIS increased with the increase of αSA. The results showed that the PBTIS (nPTA/nPIA = 7/3, αSA = 3-5mol%) is suitable for FDM. Originality/value New printing materials with good Izod notched impact strength were obtained by introducing PIA and SA (nPTA/nPIA = 7/3, αSA = 3-5 mol%) into PBT and their anisotropy are better than that of ABS.

scholarly journals Process Parameter Optimization in Fused Deposition Modeling (FDM) Using Response Surface Methodology (RSM)

2020 ◽  
Author(s):  
Muhammad Salman Mustafa ◽  
Muhammad Qasim Zafar ◽  
Muhammad Arslan Muneer ◽  
Muhammad Arif ◽  
Farrukh Arsalan Siddiqui ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Response Surface Methodology ◽  
Impact Strength ◽  
Response Surface ◽  
Layer Thickness ◽  
Fused Deposition Modeling ◽  
Experimental Results ◽  
Fused Deposition ◽  
Deposition Modeling ◽  
Printing Parameters

Abstract Fused Deposition Modeling (FDM) is a widely adopted additive manufacturing process to produce complex 3D structures and it is typically used in the fabrication of biodegradable materials e.g. PLA/PHA for biomedical applications. However, FDM as a fabrication process for such material needs to be optimized to enhance mechanical properties. In this study, dogbone and notched samples are printed with the FDM process to determine optimum values of printing parameters for superior mechanical properties. The effect of layer thickness, infill density, and print bed temperature on mechanical properties is investigated by applying response surface methodology (RSM). Optimum printing parameters are identified for tensile and impact strength and an empirical relation has been formulated with response surface methodology (RSM). Furthermore, the analysis of variance (ANOVA) was performed on the experimental results to determine the influence of the process parameters and their interactions. ANOVA results demonstrate that 44.7% infill density, 0.44 mm layer thickness, and 20C° printing temperatures are the optimum values of printing parameters owing to improved tensile and impact strength respectively. The experimental results were found in strong agreement with the predicted theoretical results.

Deposition-induced effects of isotactic polypropylene and polycarbonate composites during fused deposition modeling

2017 ◽  
Vol 23 (5) ◽  
pp. 869-880 ◽  
Author(s):  
Ying-Guo Zhou ◽  
Bei Su ◽  
Lih-sheng Turng
Keyword(s):  
Mechanical Properties ◽  
Design Methodology ◽  
Fused Deposition Modeling ◽  
Content Type ◽  
Fused Deposition ◽  
Close Relationship ◽  
Molded Parts ◽  
Deposition Modeling ◽  
Injection Molded ◽  
First Time

Purpose Although the feasibility and effectiveness of the fused deposition modeling (FDM) method have been proposed and developed, studies of applying this technology to various materials are still needed for researching its applicability, especially with regard to polymer blends and composites. The purpose of this paper is to study the deposition-induced effect and the effect of compatibilizers on the mechanical properties of polypropylene and polycarbonate (PP/PC) composites. Design/methodology/approach For this purpose, three different deposition modes for PP/PC composites with or without compatibilizers were used for the FDM method and tested for tensile properties. Also, parts with the same materials were made by injection molding and used for comparison. In addition, different deposition speeds were used to investigate the different deposition-induced effects. Furthermore, the behavior of the mechanical properties was clarified with scanning electron microscope images of the fracture surfaces. Findings The research results suggest that the deposition orientation has a significant influence on the mechanical behavior of PP/PC composite FDM parts. The results also indicate that there is a close relationship between the mechanical properties and morphological structures which are deeply influenced by compatibilization. Compared with injection molded parts, the ductility of the FDM parts can be dramatically improved due to the formation of fibrils and micro-fibrils by the deposition induced during processing. Originality/value This is the first paper to investigate a PP/PC composite FDM process. The results of this paper verified the applicability of PP/PC composites to FDM technology. It is also the first time that the deposition-induced effect during FDM has been investigated and studied.

Effect of layer thickness on irreversible thermal expansion and interlayer strength in fused deposition modeling

2017 ◽  
Vol 23 (5) ◽  
pp. 943-953 ◽  
Author(s):  
Anthony A. D’Amico ◽  
Analise Debaie ◽  
Amy M. Peterson
Keyword(s):  
Mechanical Properties ◽  
Thermal Expansion ◽  
Flexural Strength ◽  
Layer Thickness ◽  
Fused Deposition Modeling ◽  
Thermal Strain ◽  
Content Type ◽  
Fused Deposition ◽  
Deposition Modeling ◽  
The Impact

Purpose The aim of this paper is to examine the impact of layer thickness on irreversible thermal expansion, residual stress and mechanical properties of additively manufactured parts. Design/methodology/approach Samples were printed at several layer thicknesses, and their irreversible thermal expansion, tensile strength and flexural strength were determined. Findings Irreversible thermal strain increases with decreasing layer thickness, up to 22 per cent strain. Tensile and flexural strengths exhibited a peak at a layer thickness of 200 μm although the maximum was not statistically significant at a 95 per cent confidence interval. Tensile strength was 54 to 97 per cent of reported values for injection molded acrylonitrile butadiene styrene (ABS) and 29 to 73 per cent of those reported for bulk ABS. Flexural strength was 18 to 41 per cent of reported flexural strength for bulk ABS. Practical implications The large irreversible thermal strain exhibited that corresponding residual stresses could lead to failure of additively manufactured parts over time. Additionally, the observed irreversible thermal strains could enable thermally responsive shape in additively manufactured parts. Variation in mechanical properties with layer thickness will also affect manufactured parts. Originality/value Tailorable irreversible thermal strain of this magnitude has not been previously reported for additively manufactured parts. This strain occurs in parts made with both high-end and consumer grade fused deposition modeling machines. Additionally, the impact of layer thickness on tensile and flexural properties of additively manufactured parts has received limited attention in the literature.

Elastic behavior of composites reinforced by 3D printed tubular lattice braid textures

2020 ◽  
Vol 26 (7) ◽  
pp. 1277-1288
Author(s):  
Mohammad Amin Rahiminia ◽  
Masoud Latifi ◽  
Mojtaba Sadighi
Keyword(s):  
High Performance ◽  
Fused Deposition Modeling ◽  
Mechanical Test ◽  
Complex Structure ◽  
Elastic Behavior ◽  
Fibrous Materials ◽  
Content Type ◽  
Fused Deposition ◽  
Deposition Modeling ◽  
Tubular Lattice

Purpose The purpose of this paper is to introduce an innovative transversal tubular braid texture and to study the elastic behavior of its 3 D printed structure comparatively to 3 D printed longitudinal tubular braid texture (maypole) to be used as reinforcement. Design/methodology/approach Regarding the lack of proper machines for the production of the proposed texture, the structure of samples was produced as a tubular lattice braid texture using a 3 D printer with the fused deposition modeling method subsequent to simulation by Rhinoceros software. The produced specimens were composited by polyurethane resin. The composite samples were evaluated by the split disk mechanical test to obtain their hoop stress. The structures of the reinforced composites were theoretically analyzed by ANSYS software. Findings The results of the mechanical test and theoretical analysis showed that the composites reinforced with transversal tubular lattice braid have higher strength compared to the composites reinforced with longitudinal ones. This assured that the composite reinforced by transversal tubular lattice braid is reliable to be used as high-performance tube for different applications. Originality/value Further work is carried out to produce the innovated complex structure continuously by a specially designed machine and fibrous materials to reinforce tubular composites in an industrial continual process to be applied for high-pressure fluids flows.

Property Enhancement of Carbon Fiber-Reinforced Polylactic Acid Composites Prepared by Fused-Deposition Modeling

2020 ◽  
pp. 455-478
Author(s):  
Pravin R. Kubade ◽  
Hrushikesh B. Kulkarni ◽  
Vinayak C. Gavali
Keyword(s):  
Mechanical Properties ◽  
Additive Manufacturing ◽  
Carbon Fiber ◽  
Polylactic Acid ◽  
Fused Deposition Modeling ◽  
Three Dimensional ◽  
Fiber Reinforced ◽  
Fused Deposition ◽  
Deposition Modeling ◽  
Properties Of Composites

Additive Manufacturing or three-dimensional printing refers to a process of building lighter, stronger three-dimensional parts, manufactured layer by layer. Additive manufacturing uses a computer and CAD software which passes the program to the printer to build the desired shape. Metals, thermoplastic polymers, and ceramics are the preferred materials used for additive manufacturing. Fused deposition modeling is one additive manufacturing technique involving the use of thermoplastic polymer for creating desired shape. Carbon fibers can be added into polymer to strengthen the composite without adding additional weight. Present work deals with the manufacturing of Carbon fiber-reinforced Polylactic Acid composites prepared using fused deposition modeling. Mechanical and thermo-mechanical properties of composites are studied as per ASTM standards and using sophisticated instruments. It is observed that there is enhancement in thermo-mechanical properties of composites due to addition reinforcement which is discussed in detail.

An approach for mechanical property optimization of fused deposition modeling with polylactic acid via design of experiments

2016 ◽  
Vol 22 (2) ◽  
pp. 387-404 ◽  
Author(s):  
Jonathan Torres ◽  
Matthew Cole ◽  
Allen Owji ◽  
Zachary DeMastry ◽  
Ali P. Gordon
Keyword(s):  
Mechanical Properties ◽  
Polylactic Acid ◽  
Fused Deposition Modeling ◽  
Mechanical Tests ◽  
Content Type ◽  
Fused Deposition ◽  
Structural Applications ◽  
3D Printers ◽  
Deposition Modeling

Purpose This paper aims to present the influences of several production variables on the mechanical properties of specimens manufactured using fused deposition modeling (FDM) with polylactic acid (PLA) as a media and relate the practical and experimental implications of these as related to stiffness, strength, ductility and generalized loading. Design/methodology/approach A two-factor-level Taguchi test matrix was defined to allow streamlined mechanical testing of several different fabrication settings using a reduced array of experiments. Specimens were manufactured and tested according to ASTM E8/D638 and E399/D5045 standards for tensile and fracture testing. After initial analysis of mechanical properties derived from mechanical tests, analysis of variance was used to infer optimized production variables for general use and for application/load-specific instances. Findings Production variables are determined to yield optimized mechanical properties under tensile and fracture-type loading as related to orientation of loading and fabrication. Practical implications The relation of production variables and their interactions and the manner in which they influence mechanical properties provide insight to the feasibility of using FDM for rapid manufacturing of components for experimental, commercial or consumer-level use. Originality/value This paper is the first report of research on the characterization of the mechanical properties of PLA coupons manufactured using FDM by the Taguchi method. The investigation is relevant both in commercial and consumer-level aspects, given both the currently increasing utilization of 3D printers for component production and the viability of PLA as a renewable, biocompatible material for use in structural applications.

Fused deposition modeling with polyamide 1012

2019 ◽  
Vol 25 (7) ◽  
pp. 1145-1154 ◽  
Author(s):  
Xia Gao ◽  
Daijun Zhang ◽  
Xiangning Wen ◽  
Shunxin Qi ◽  
Yunlan Su ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Fused Deposition Modeling ◽  
Mechanical Performance ◽  
Content Type ◽  
Good Ductility ◽  
Fused Deposition ◽  
Bed Temperature ◽  
Deposition Modeling ◽  
Nozzle Temperature ◽  
Printing Parameters

Purpose This work aims to develop a new kind of semicrystalline polymer filament and optimize its printing parameters in the fused deposition modeling process. The purpose of this work also includes producing FDM parts with good ductility. Design/methodology/approach A new kind of semicrystalline filaments composed of long-chain polyamide (PA)1012 was prepared by controlling screw speed and pulling speed carefully. The optimal printing parameters for PA1012 filaments were explored through investigating dimensional accuracy and bonding strength of FDM parts. Furthermore, the mechanical properties of PA1012 specimens were also evaluated by varying nozzle temperatures and raster angles. Findings It is found that PA1012 filaments can accommodate for FDM process under suitable printing parameters. The print quality and mechanical properties of FDM parts highly depend on nozzle temperature and bed temperature. Even though higher temperatures facilitate stronger interlayer bonding, FDM parts with excellent tensile strength were obtained at a moderate nozzle temperature. Moreover, a bed temperature well above the glass transition temperature of PA1012 can eliminate shrinkage and distortion of FDM parts. As expected, FDM parts prepared with PA1012 filaments exhibit good ductility. Originality/value Results in this work demonstrate that the PA1012 filament allows the production of FDM parts with desired mechanical performance. This indicates the potential for overcoming the dependence on amorphous thermoplastics as a feedstock in the FDM technique. This work also provides insight into the effect of materials properties on the mechanical performance of FDM-printed parts.

The effects of moisture and temperature on the mechanical properties of additive manufacturing components: fused deposition modeling

2016 ◽  
Vol 22 (6) ◽  
pp. 887-894 ◽  
Author(s):  
Eunseob Kim ◽  
Yong-Jun Shin ◽  
Sung-Hoon Ahn
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Water Absorption ◽  
Fused Deposition Modeling ◽  
Content Type ◽  
Fused Deposition ◽  
Temperature Conditions ◽  
Molded Parts ◽  
Deposition Modeling ◽  
Injection Molded

Purpose This paper aims to investigate the water absorption behaviors and mechanical properties, according to water absorption and temperature, of components fabricated by fused deposition modeling (FDM) and injection molding. The mechanical properties of FDM and injection molded parts were studied under several environmental conditions. Design/methodology/approach FDM components can be used as load-carrying elements under a range of moisture and temperature conditions. FDM parts show anisotropic mechanical properties according to build orientation. Components were fabricated from acrylonitrile-butadiene-styrene in three different orientations. The mechanical properties of parts fabricated by FDM were compared to injection molded components made from the same material. Water absorption tests were conducted in distilled water between 20 and 60°C to identify the maximum water absorption rate. Both moisture and temperature were considered as environmental variables in the tensile tests, which were conducted under various conditions to measure the effects on mechanical properties. Findings The water absorption behavior of FDM components obeyed Fickian diffusion theory, irrespective of the temperature. High temperatures accelerated the diffusion rate, although the maximum water absorption rate was not affected. The tensile strength of FDM parts under dry, room temperature conditions, was approximately 26-56 per cent that of injection molded parts, depending on build orientation. Increased temperature and water absorption had a more significant effect on FDM parts than injection molded components. The tensile strength was decreased by 67-71 per cent in hot, wet environments compared with dry, room temperature conditions. Originality/value The water absorption behavior of FDM components was investigated. The quantitative effects of temperature and moisture on tensile strength, modulus and strain were also measured. These results will contribute to the design of FDM parts for use under various environmental conditions.

The Influence of Layer Thickness on Mechanical Properties of the 3D Printed ABS Polymer by Fused Deposition Modeling

2016 ◽  
Vol 706 ◽  
pp. 63-67 ◽  
Author(s):  
Pritish Shubham ◽  
Arnab Sikidar ◽  
Teg Chand
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Impact Strength ◽  
Injection Molding ◽  
Layer Thickness ◽  
Fused Deposition Modeling ◽  
Molding Method ◽  
Fused Deposition ◽  
Deposition Modeling ◽  
3D Printed

3D Printed ABS polymer samples were investigated for understanding the effect of layer thickness on the various mechanical properties of the component. Standard samples with varying layer thickness were prepared by 3D printing machine which works on the principle of Fused Deposition modeling (FDM) method and compared with sample prepared by standard injection molding method. Results show that tensile strength (36 MPa), impact strength (103.6 J/m) and hardness (R107) were highest for the samples made by injection molding method. Furthermore, among 3D printed samples, properties were better with smaller layer thickness. With increase in layer thickness, there was negative effect on mechanical properties as tensile strength, impact strength and hardness decreased. Exception with hardness of 3D printed ABS samples was found; for largest layer thickness hardness further increased instead of decreasing.

An innovative design approach in three-dimensional printing of continuous fiber–reinforced thermoplastic composites via fused deposition modeling process: In-melt simultaneous impregnation

2019 ◽  
Vol 234 (1-2) ◽  
pp. 243-259 ◽  
Author(s):  
Behnam Akhoundi ◽  
Amir Hossein Behravesh ◽  
Arvin Bagheri Saed
Keyword(s):  
Mechanical Properties ◽  
Glass Fiber ◽  
Fused Deposition Modeling ◽  
Three Dimensional ◽  
Thermoplastic Composites ◽  
Fiber Reinforced ◽  
Continuous Fiber ◽  
Fiber Volume ◽  
Fused Deposition ◽  
Deposition Modeling

In this study, an innovative method was devised and implemented to produce continuous glass fiber–reinforced thermoplastic composites via a fused deposition modeling three-dimensional printer to enhance the mechanical properties of the printed products. In the extrusion-based, or filament-based, additive manufacturing process, namely, fused deposition modeling, the parts are basically formed via deposition of the material in the molten state, and thus embedding continuous fiber, in a solid form, is highly challenging. Hence, a nozzle system was designed and manufactured to feed the continuous fiber into the molten polymer simultaneously, which is called, here, in-melt simultaneous impregnation. With the presence of continuous fibers in the nozzle outlet, the feed of filament was calculatedly adjusted in the G-codes depending on the fiber volume percentage, to produce sound flow, and consistent deposition. Composite products were produced with various geometrical shapes. Via analysis and close control of the filament feeding, as a critical requirement to produce a sound printed product, composites with various fiber volume percentages were printed. Also, the mechanical properties of the printed parts with 30% by volume of glass fiber were measured. The results of the tensile test indicated that the continuous fibers were appropriately and effectively embedded that could result in remarkable increases in tensile strength and modulus of the samples, higher than 700%. The resulted values of tensile modulus were consistent with the values calculated via the rule of mixture. In addition, scanning electron microscopic images of the fracture sections suggest a sound adhesion between fibers and the matrix.

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