Study of Ductile-to-Brittle Transition in Single Grit Diamond Scribing of Silicon: Application to Wire Sawing of Silicon Wafers

Author(s):  
Hao Wu ◽  
Shreyes N. Melkote

The ductile-to-brittle cutting mode transition in single grit diamond scribing of monocrystalline silicon is investigated in this paper. Specifically, the effects of scriber tip geometry, coefficient of friction, and external hydrostatic pressure on the critical depth of cut associated with ductile-to-brittle transition and crack generation are studied via an eXtended Finite Element Method (XFEM) based model, which is experimentally validated. Scribers with a large tip radius are shown to produce lower tensile stresses and a larger critical depth of cut compared with scribers with a sharp tip. Spherical tipped scribers are shown to generate only surface cracks, while sharp tipped scribers (conical, Berkovich and Vickers) are found to create large subsurface tensile stresses, which can lead to nucleation of subsurface median/lateral cracks. Lowering the friction coefficient tends to increase the critical depth of cut and hence the extent of ductile mode cutting. The results also show that larger critical depth of cut can be obtained under external hydrostatic pressure. This knowledge is expected to be useful in optimizing the design and application of the diamond coated wire employed in fixed abrasive diamond wire sawing of photovoltaic silicon wafers.

Author(s):  
Biswarup Bhattacharya ◽  
John A. Patten ◽  
Jerry Jacob

Scratching experiments, using diamond styli and single point diamond tools, were performed to simulate Single Point Diamond Turning (SPDT). The results of these experiments were used to determine if a ductile response is possible, and then to determine the critical depth of cut or penetration depth for the ductile to brittle transition (DBT). The depths of the scratches produced at different loads were measured and correlated to the ductile and brittle response of the material. The DBT depth for Chemically Vapor Deposited (CVD) coated Silicon Carbide (SiC) samples was determined. The analysis for the critical depth (DBT) did confirm the possibility for SPDT of CVD coated SiC in the ductile regime. These results were further used for SPDT of CVD SiC. Post experimental analysis of the machined surface did reveal a final surface roughness of 8–20nm, successfully demonstrating ductile regime machining of CVD coated SiC.


Micromachines ◽  
2019 ◽  
Vol 10 (6) ◽  
pp. 382 ◽  
Author(s):  
Peng Chai ◽  
Shujuan Li ◽  
Yan Li

In this paper, a theoretical model of the critical depth of cut of nanoscratching on a 4H-SiC single crystal with a Berkovich indenter is proposed, and a series of scratch tests in a nanomechanical test system was performed. Through nanoindentation experimentation on fused quartz, the Berkovich indenter nose radius was indirectly confirmed using least squares. The range of critical depths of cut at the ductile–brittle transition was obtained by SEM observation, and the size of cracks was amplified with increasing scratching depth. The theoretical result of the critical depth of cut at the ductile–brittle transition for a 4H-SiC single crystal is 91.7 nm, which is close to the first obvious pop-in point of the relation curve between tangential force and lateral displacement. Repeated experimental results show good consistency and good agreement with other references.


2021 ◽  
Author(s):  
Mohammad Rasheed Khan ◽  
Guenther Glatz ◽  
Devon Chikonga Gwaba ◽  
Gallyam Aidagulov

Abstract More than two decades have passed since the introduction of the scratch testing method for rock strength determination. The test method typically involves dragging a rigid-shaped cutter across the rock surface at a fixed cutting depth. This depth determines the failure mechanism of the rock, ductile for shallow depths and brittle for deeper. In the ductile mode, intrinsic specific energy is primarily a measure of the unconfined-compressive-strength (UCS), which is pivotal for rate of penetration (ROP) during drilling and for borehole stability analysis. On the contrary, brittle failure can lead to permanent core damage and is usually not desired as it impacts interpretation of the scratch testing results. Consequently, it is imperative to identify the critical depth, and at which transition from ductile to brittle failure occurs which will help optimize rock testing and tool designs. In this study, a novel methodology is proposed utilizing micro-computed tomography (CT) imaging to determine critical depth through morphological analysis of scratch test cuttings. Scratch tests are carried out on Indiana limestone core samples with the cutter-rock interaction geometry characterized by a cutter width of 10mm and a back-rake angle of 15°. The sample is scratched in the range of 0.05mm to 0.40mm with increments of 0.05mm. Scratch powder is carefully collected after each scratch increment and stored for further analysis. This powder is then loaded into slim rubber tubes and imaged at a high resolution of 1 µm with a helical micro-CT scanner. The scans are then reconstructed using a computer program to initiate the visualization of individual grains from each cutter depth including evaluation of grain morphologies. Finally, the results from this morphological analysis are corroborated and compared with three other methods: force response analysis, force inflection point analysis, and the size effect law (SEL). Based on shape analysis, it was found that the transition from ductile to brittle regime occurs at a depth of 0.25mm. Elongation and appearance of the enhanced degree of angularity of the grains as the depth of cut (DOC) increases past 0.25mm was observed. Moreover, large grain sizes were detected and are representative of formation of chips (typical brittle regime response). Furthermore, it is illustrated that the image analysis helps eliminate the ambiguity of force signal analysis and in combination can aid in the critical depth of cut determination. The other methods involving force alone and the SEL are not able to pin-point onset of brittle regime. Using a similar methodology, creation of a database for various rock types is recommended to develop a guide for the depth of cut selection during scratch testing. This novel methodology utilizing micro-CT analysis and comparative study with other techniques will put in place an accurate strategy to determine the critical depth of cut when designing rock scratch testing programs.


2008 ◽  
Vol 375-376 ◽  
pp. 206-210
Author(s):  
Hui Ping Zhang ◽  
Zhen Jia Li ◽  
Er Liang Liu ◽  
Guo Liang Wei

This paper deals with chip breaking behaviour of 3-D complex groove inserts in machining carbon constructional steel-45 steel at high cutting speeds .Cutting experiments were performed at eleven different cutting speeds. Firstly, the results showed that by increasing cutting speeds, the changes of the critical feedrate and chip breaking scopes at high cutting speeds machining with 3-D complex groove inserts were nonlinear and not monotonous function relations. Then, mathematic models were built. Secondly, the results showed that the critical depth of cut was a constant value at various cutting speeds. And, the curves of the critical depth of cut were perpendicular lines. For this purpose, the critical depth of cut mathematic model has been built. The study above lays a theory and basis for future investigation of the mechanism of chip breaking with 3-D groove insert in high speed machining.


2016 ◽  
Vol 41 (11) ◽  
pp. 4553-4562 ◽  
Author(s):  
A. K. M. Nurul Amin ◽  
Mst. Nasima Bagum ◽  
Noor Fathiah ◽  
Mohamed Konneh ◽  
Tasnim Firdaus Bt. Mohamed Ariff

2010 ◽  
Vol 431-432 ◽  
pp. 126-129 ◽  
Author(s):  
Ming Zhou ◽  
Peng Jia ◽  
Min Li

In diamond cutting of optical glasses, the magnitude of critical depth of cut for brittle-ductile transition is an important factor affecting the machinability of the work material in terms of production rate and surface quality. In this work, scratching tests with increasing depths of cut were conducted on glass BK7 to evaluate the influence of the cutting fluid properties on the critical depth of cut. Boric acid solutions of different concentrations were selected as cutting fluids in the tests. The resulting scratches were examined utilizing a white light interferometer and the values of the critical depth of cut were determined based on the observations of the micro-morphology of the scratch surfaces produced. Experimental results indicated that compared with the process without cutting fluid action, the critical depth of cut in diamond cutting of glass BK7 can be increased by using boric acid solution as the cutting fluid.


1976 ◽  
Vol 98 (2) ◽  
pp. 563-575 ◽  
Author(s):  
J. D. Stachiw ◽  
O. H. Burnside

Acrylic plastic spherical shell sector windows with 117-deg included angle and outside radius of 24-in. (61 mm), have been impacted at their center, with a 12,500 lb (5662 kg) weight, in a simulated ocean environment. Velocities of impacts ranged from 0.205 to 10.702 ft (0.06 to 3.26 m) per second. It has been found that fracture of windows is initiated by tensile stresses on the concave surface of the window, directly below the point of impact. Compressive stresses, generated by external hydrostatic pressure, decrease the destructive effect of tensile stresses introduced by point impact loading. For 2.25 and 4.0-in. (57 and 101 mm) thick windows the critical impact velocities were found to fall into the 1.5 to 3 ft (0.45 to 0.91 m) per second range, the exact value being a function of window thickness and external hydrostatic pressure. A finite element analysis was found to agree rather well with the experimental. This analysis can be employed to predict, with a reasonable degree of confidence, the critical impact velocities for acrylic plastic spherical windows in the bows of submersibles.


2013 ◽  
Vol 589-590 ◽  
pp. 480-484 ◽  
Author(s):  
Peng Jia

In diamond cutting of optical glasses, the magnitude of critical depth of cut for brittle-ductile transition is an important factor affecting the machinability of the work material in terms of production rate and surface quality. In this work, scratching tests with increasing depths of cut were conducted on glass BK7 to evaluate the influence of the cutting fluid properties on the critical depth of cut. Boric acid solutions of different concentrations were selected as cutting fluids in the tests. The resulting scratches were examined utilizing a white light interferometer and the values of the critical depth of cut were determined based on the observations of the micro-morphology of the scratch surfaces produced. Experimental results indicated that compared with the process without cutting fluid action, the critical depth of cut in diamond cutting of glass BK7 can be increased by using boric acid solution as the cutting fluid.


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