Wear and Friction of AA5052-Al3Zr In Situ Composites Synthesized by Direct Melt Reaction

2015 ◽  
Vol 138 (2) ◽  
Author(s):  
Gaurav Gautam ◽  
Anita Mohan
Keyword(s):  
Wear Rate ◽  
Three Dimensional ◽  
Aluminum Matrix ◽  
Aluminum Matrix Composites ◽  
Sliding Velocity ◽  
Volume Percent ◽  
Wear Coefficient ◽  
Morphological Studies ◽  
Wear And Friction

Particulate aluminum matrix composites (PAMCs) with different volume percent of Al3Zr particles have been developed by direct melt reaction (DMR). Wear and friction have been studied in detail for all compositions under dry sliding conditions. Results indicate that the wear rate, normalized wear rate, and wear coefficient of PAMCs decrease continuously with increase in volume percent of Al3Zr particles, however, with applied load and sliding distance, wear continuously increases. Wear rate and wear coefficient with sliding velocity initially decrease for all compositions, attains minima, and then increase sharply. However, coefficient of friction shows increasing trend with composition and sliding velocity but with load it shows a decreasing trend and with distance slid it fluctuates within a value of ±0.025. At low load and sliding velocity three-dimensional (3D)-profilometer, scanning electron microscope (SEM), and debris studies show low Ra values and mild wear dominated by oxidative nature, whereas at high loads and sliding velocities high Ra values and wear nature change to severe wear with mixed mode (oxidative–metallic) and surface with deep grooves is observed. Further, it is also important to note from morphological studies that refinement of matrix phase takes place with in situ formation of Al3Zr particles, which helps to improve hardness and tensile properties finally contributing to low wear rate.

Fabrication and characterization of TiB2-reinforced functionally graded aluminum matrix material

2020 ◽  
Vol 72 (10) ◽  
pp. 1147-1152
Author(s):  
Ömer Savaş
Keyword(s):  
Wear Rate ◽  
Abrasive Wear ◽  
Peer Review ◽  
Centrifugal Force ◽  
Matrix Material ◽  
Aluminum Matrix ◽  
Functionally Graded ◽  
Aluminum Matrix Composites ◽  
Content Type

Purpose This study aims to investigate the production and abrasive wear rate of functionally graded TiB2/Al composites. TiB2 particles have been spontaneously formed in liquid matrix using in situ technique. The properties of composites such as hardness, abrasive wear rate and microstructure have been examined. Design/methodology/approach In situ TiB2 reinforcement phase was synthesized by using a liquid Al–Ti–B system. A semi-solid composite (Al(l)-TiB2(s)) prepared at 900°C was solidified under a centrifugal force to both grade functionally and give the final shape to materials. Abrasive wear test of materials was conducted using the pin-on-disk method at room temperature. The wear tests were carried out with two different loads of 1 Newton (N) and 2 N, a sliding velocity of 3.5 m s−1 and a sliding distance of 75 m. Findings This research provided the following findings; TiB2 particles can be successfully synthesized with in situ reaction technique in molten aluminum. It was determined that abrasive wear rate increases with increasing load and decreases with increasing TiB2 reinforcement content within matrix. Originality/value In previous studies, there have been many trials on the in situ production of TiB2-reinforced aluminum matrix composites. However, there are few studies on production of in situ TiB2-reinforced aluminum matrix functionally graded materials. At the same time, there is no study that the properties of composite, such as hardness and abrasive wear rate, are examined together according to centrifugal force. Peer review The peer review history for this article is available at: https://publons.com/publon/10.1108/ILT-12-2019-0538/

High-Temperature Tribology of AA5052/ZrB2 PAMCs

2016 ◽  
Vol 139 (1) ◽  
Author(s):  
Narendra Kumar ◽  
Gaurav Gautam ◽  
Rakesh Kumar Gautam ◽  
Anita Mohan ◽  
Sunil Mohan
Keyword(s):  
High Temperature ◽  
Wear Rate ◽  
Aluminum Matrix ◽  
Aluminum Matrix Composites ◽  
Unreinforced Alloy ◽  
Volume Percentage ◽  
Increase With Increase ◽  
Wear And Friction ◽  
Wear Mode ◽  
Worn Surface

AA5052/ZrB2 particulate aluminum matrix composites (PAMCs) have been produced by in situ reaction of K2ZrF6 and KBF4 compounds with molten alloy at about 860 °C. Dry sliding wear and friction of composites have been investigated for a particular sliding velocity and sliding distance at different loads from ambient temperature to 200 °C. It is revealed that for a particular load and temperature, wear rate and normalized wear rate decrease with increase in the volume percentage of ZrB2 particles whereas coefficient of friction (COF) shows a reverse trend. Wear rate and COF also increase with increase in temperature for a constant load and composition. Whereas with load for a particular temperature, wear rate and wear rate per unit vol. % ZrB2 increase while COF decreases. Worn surface and wear debris morphology examined under scanning electron microscopy (SEM) and profilometer to understand the wear mechanism revealed that wear mode transition takes place from mild-oxidative to severe-metallic at 100 °C for unreinforced alloy, whereas a shifting is observed in transition temperature from 100 to 150 °C for composite with 9 vol. % ZrB2 particles. Energy dispersive spectroscopy (EDS) analysis of worn surface confirms the oxidative wear mode. Profilometry results indicate that wear surface has higher surface roughness at higher values of load and temperatures. Prior to wear and friction studies, composites were also characterized by X-ray diffraction (XRD) and SEM for morphology and microstructural characteristics to correlate with wear results. The findings are very helpful to make the AA5052/ZrB2 composites suitable for the applications, where high-temperature wear is a limiting factor.

Study on Mechanical Properties of AA6351 Alloy Reinforced with Titanium Di-Boride (TiB2) Composite by In Situ Casting Method

2015 ◽  
Vol 787 ◽  
pp. 583-587 ◽  
Author(s):  
V. Mohanavel ◽  
K. Rajan ◽  
K.R. Senthil Kumar
Keyword(s):  
Tensile Strength ◽  
Aluminum Matrix ◽  
Aluminum Matrix Composites ◽  
Scanning Electron Micrographs ◽  
Matrix Composites ◽  
X Ray Diffraction ◽  
In Situ Reaction ◽  
Halide Salts ◽  
Scanning Electron

In the present study, an aluminum alloy AA6351 was reinforced with different percentages (1, 3 and 5 wt %) of TiB2 particles and they were successfully fabricated by in situ reaction of halide salts, potassium hexafluoro-titanate and potassium tetrafluoro-borate, with aluminium melt. Tensile strength, yield strength and hardness of the composite were investigated. In situ reaction between the inorganic salts K2TiF6 and KBF4 to molten aluminum leads to the formation of TiB2 particles. The prepared aluminum matrix composites were characterized using X-ray diffraction and scanning electron microscope. Scanning electron micrographs revealed a uniform dispersal of TiB2 particles in the aluminum matrix. The results obtained indicate that the hardness and tensile strength were increased with an increase in weight percentages of TiB2 contents.

Reactive hot pressing of aluminum matrix composites

1999 ◽  
Vol 14 (11) ◽  
pp. 4246-4250
Author(s):  
H. J. Brinkman ◽  
J. Duszczyk ◽  
L. Katgerman
Keyword(s):  
Hot Pressing ◽  
Adverse Reactions ◽  
Aluminum Matrix ◽  
Aluminum Matrix Composites ◽  
Matrix Composites ◽  
Processing Step ◽  
Exothermic Process ◽  
Composite Product ◽  
Reactive Hot Pressing

A method is described for the production of dense aluminum matrix composites from elemental powders in one processing step by reactive hot pressing (RHP). It encompasses both the exothermic conversion of reactants to composite product and the following hot compaction of the porous composite product. The RHP method described in this paper takes into account the gas evolution accompanying the exothermic process, ensures complete conversion of reactants, and avoids adverse reactions between aluminum matrix and graphite tooling material. In situ sample temperature measurements enable proper process control, in particular the timing of the full densification step of the hot reaction product.

Laser-ultrasonic study of the local porosity of reactive cast aluminum-matrix composites

2021 ◽  
Vol 87 (5) ◽  
pp. 34-42
Author(s):  
N. B. Podymova ◽  
I. E. Kalashnikov ◽  
L. I. Kobeleva
Keyword(s):  
Metal Matrix Composites ◽  
Metal Matrix ◽  
Aluminum Matrix ◽  
Amplitude Distribution ◽  
Aluminum Matrix Composites ◽  
Matrix Composites ◽  
Cast Aluminum ◽  
Laser Ultrasonic ◽  
Local Porosity

One of the most critical manufacturing defects of cast metal-matrix composites is a non-uniform porosity distribution over the composite volume. Unevenness of the distribution leads not only to local softening, but also plays a key role in the evolution of the damage process under the external loads. The goal of the study is to apply a new laser-ultrasonic method to in-situ study of a local porosity in reactive cast aluminum-matrix composites. The proposed method is based on statistical analysis of the amplitude distribution of backscattered broadband pulses of longitudinal ultrasonic waves in the studied materials. Laser excitation and piezoelectric detection of ultrasound were carried out using a laser-ultrasonic transducer. Two series of reactive cast aluminum-matrix composites were analyzed: reinforced by in situ synthesized Al3Ti intermetallic particles in different volume concentrations and by Al3Ti added with synthetic diamond nanoparticles. It is shown that for both series of the composites, the amplitude distribution of backscattered ultrasonic pulses is approximated by the Gaussian probability distribution applicable for statistics of large number of independent random variables. The empirical dependence of the half-width of this distribution on the local porosity in composites of two series is approximated by the same nearly linear function regardless of the size and fraction of reinforcing particles. This function was used to derive the formula for calculation of the local porosity in the studied composites. The developed technique seems to be promising in revealing potentially dangerous domains with high porosity in reactive-cast metal-matrix composites.

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