Visualization Study on Two-Phase Flow Behaviors in the Gas-Liquid-Solid Microreactor for Hydrogenation of Nitrobenzene

Author(s):  
Hao Feng ◽  
Xun Zhu ◽  
Rong Chen ◽  
Qiang Liao

In this study, visualization study on the gas-liquid two phase flow characteristics in a gas-liquid-solid microchannel reactor was carried out. Palladium nanocatalyst was coated onto the polydopamine functionalized surface of the microchannel through eletroless deposition. The materials characterization results indicated that palladium nanocatalyst were well dispersed on the modified surface. The effects of both the gas and liquid flow rates as well as inlet nitrobenzene concentration on the two-phase flow characteristics were studied. The experimental results revealed that owing to the chemical reaction inside the microreactor, the gas slug length gradually decreased along the flow direction. For a given inlet nitrobenzene concentration, increasing the liquid flow rate or decreasing the gas flow rate would make the variation of the gas slug length more obvious. High inlet nitrobenzene concentration would intensify both the nitrobenzene transfer efficiency and gas reactants consumption, and thereby the flow pattern in the microchannel was transferred from Taylor flow into bubble flow. Besides, the effect of both flow rate and original nitrobenzene concentration on the variation of nitrobenzene conversion and the desired product aniline yield were also discussed.

2011 ◽  
Vol 383-390 ◽  
pp. 4922-4927
Author(s):  
Peng Xia Xu ◽  
Yan Feng Geng

Wet gas flow is a typical two-phase flow with low liquid fractions. As differential pressure signal contains rich information of flow parameters in two-phase flow metering, a new method is proposed for wet gas flow metering based on differential pressure (DP) and blind source separation (BSS) techniques. DP signals are from a couple of slotted orifices and the BSS method is based on time-frequency analysis. A good relationship between the liquid flow rate and the characteristic quantity of the separated signal is established, and a differential pressure correlation for slotted orifice is applied to calculate the gas flow rate. The calculation results are good with 90% relative errors less than ±10%. The results also show that BSS is an effective method to extract liquid flow rate from DP signals of wet gas flow, and to analysis different interactions among the total DP readings.


Author(s):  
Rinaldo Antonio de Melo Vieira ◽  
Mauricio Gargaglione Prado

The effect of free gas on the Electrical Submersible Pump (ESP) performance is well known. At a constant rotational speed and constant liquid flowrate, small amount of gas causes a mild head reduction when compared to the single phase liquid head. However, at higher gas rates, a drastic reduction in the head is observed. This critical condition, known as surging point, is a combination of liquid and gas flow rates that cause a maximum in the head performance curve. The first derivative of the head with respect to the liquid flow rate change sign as the liquid flow rate crosses the surging point. In several works on ESP two-phase flow performance, production conditions to the left of the surging region are described or reported as unstable operational conditions. This paper reviews basic concepts on stability of dynamical systems and shows through simulation that ESP oscillatory behavior may result from two-phase flow conditions. A specific drift flux computation code was developed to simulate the dynamic behavior of ESP wells producing without packer.


2021 ◽  
Author(s):  
Ekhwaiter Abobaker ◽  
Abadelhalim Elsanoose ◽  
Mohammad Azizur Rahman ◽  
Faisal Khan ◽  
Amer Aborig ◽  
...  

Abstract Perforation is the final stage in well completion that helps to connect reservoir formations to wellbores during hydrocarbon production. The drilling perforation technique maximizes the reservoir productivity index by minimizing damage. This can be best accomplished by attaining a better understanding of fluid flows that occur in the near-wellbore region during oil and gas operations. The present work aims to enhance oil recovery by modelling a two-phase flow through the near-wellbore region, thereby expanding industry knowledge about well performance. An experimental procedure was conducted to investigate the behavior of two-phase flow through a cylindrical perforation tunnel. Statistical analysis was coupled with numerical simulation to expand the investigation of fluid flow in the near-wellbore region that cannot be obtained experimentally. The statistical analysis investigated the effect of several parameters, including the liquid and gas flow rate, liquid viscosity, permeability, and porosity, on the injection build-up pressure and the time needed to reach a steady-state flow condition. Design-Expert® Design of Experiments (DoE) software was used to determine the numerical simulation runs using the ANOVA analysis with a Box-Behnken Design (BBD) model and ANSYS-FLUENT was used to analyses the numerical simulation of the porous media tunnel by applying the volume of fluid method (VOF). The experimental data were validated to the numerical results, and the comparison of results was in good agreement. The numerical and statistical analysis demonstrated each investigated parameter’s effect. The permeability, flow rate, and viscosity of the liquid significantly affect the injection pressure build-up profile, and porosity and gas flow rate substantially affect the time required to attain steady-state conditions. In addition, two correlations obtained from the statistical analysis can be used to predict the injection build-up pressure and the required time to reach steady state for different scenarios. This work will contribute to the clarification and understanding of the behavior of multiphase flow in the near-wellbore region.


2014 ◽  
Vol 136 (4) ◽  
Author(s):  
Rinaldo Antonio de Melo Vieira ◽  
Mauricio Gargaglione Prado

The effect of free gas on electrical submersible pump (ESP) performance is well known. At a constant rotational speed and constant liquid flow rate, a small amount of gas causes a mild head reduction when compared to the single phase liquid head. However, at higher gas rates, a drastic reduction in the head is observed. This critical condition, known as the surging point, is a combination of liquid and gas flow rates that cause a maximum in the head performance curve. The first derivative of the head with respect to the liquid flow rate changes sign as the liquid flow rate crosses the surging point. In several works on ESP two-phase flow performance, production conditions to the left of the surging region are described or reported as unstable operational conditions. This paper reviews basic concepts on stability of dynamical systems and shows through simulation that ESP oscillatory behavior may result from two-phase flow conditions. A specific drift flux computation code was developed to simulate the dynamic behavior of ESP wells producing without packers.


Author(s):  
Takayoshi Kikuchi ◽  
Tatsuya Hazuku ◽  
Yutaka Fukuhara ◽  
Tomoji Takamasa ◽  
Takashi Hibiki

To evaluate the effect of pipe wall surface wettability on flow characteristics in a vertical upward gas-liquid two-phase flow, a visualization study was performed using an acrylic pipe and a hydrophobic pipe. Such basic flow characteristics as flow patterns, pressure drop and void fraction were investigated in these pipes. In the hydrophobic pipe, an inverted-churn flow regime was observed in a region where the churn flow regime was observed in the acrylic pipe, while a droplet flow regime was observed in the region where an annular flow regime was observed in the acrylic pipe. At a high gas flow rate, the average void fraction in the hydrophobic pipe was higher than in the acrylic pipe. The effect of surface wall wettability on frictional pressure loss was confirmed to be insignificant under the present experimental conditions.


Water ◽  
2020 ◽  
Vol 12 (2) ◽  
pp. 388
Author(s):  
Juanli Zuo ◽  
Fengchao Li ◽  
Ning Zhang ◽  
Denghui He ◽  
Wen Wang ◽  
...  

A pneumatic lifting pump is used in sewage treatment, offshore oil production, and other fields because of its simple structure and strong practicability. In order to study its internal hydraulic characteristics and gas-liquid two-phase flow, this paper carries out experimental research on the influence of different air intake modes and riser diameters on the performance of a pneumatic lifting pump. The air-water two-phase flow pattern in the riser and motion characteristics of bubble formation at the nozzle are obtained by a high-speed camera. Through theoretical analysis, the theoretical model of a pneumatic lifting pump is established, and experimental results verify the theoretical model well. The results show that when the submergence ratio is constant, the lifting efficiency decreases with the smaller intake area under different intake areas; and the influences of different holes distributions on liquid flow rate and lifting efficiency are not significant under the same intake area. At the same submergence ratio, the smaller the riser diameter, the smaller the final lifting liquid flow rate and the larger the lifting efficiency peak value.


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