Quantitative Characterization of True Leak Rate of Micro to Nanoliter Packages Using a Helium Mass Spectrometer

Author(s):  
A. Goswami ◽  
B. Han ◽  
Suk-Jin Ham ◽  
Byung-Gil Jeong

The helium mass spectrometer has been used extensively for qualitative analysis of fine leaks. However, qualitative analysis for the small volumes (typically < 10−3 cc) of MEMS packages can produce erroneous results. In addition, the qualitative use of the helium fine leak test does not allow comparison of two different packages. Nor can the results be correlated with data from accelerated tests such as 85°C/85%RH test. These limitations warrant the development of a method to assess hermeticity quantitatively. This paper proposes a procedure to quantitatively measure the true leak rate of micro to nanoliter packages using the helium mass spectrometer. The proposed method is based on the fact that the profile of the measured leak rate signal depends only on the true leak rate and the volume of the package. Prior knowledge of the volume of the package enables determination of the true leak rate by performing a weighted non-linear regression analysis of the data. The method was implemented to measure the true leak rate of a MEMS RF filter package. The package was tested under three different test conditions yielding three different signal profiles. The method yielded a consistent value for the true leak rate, which verified the robustness of the method. The proposed method provides a true leak rate as a quantitative measure of hermeticity. The accurate true leak rates will help evaluate new bonding materials/processes and package designs fast and effectively.

2018 ◽  
Vol 35 (1) ◽  
pp. 11-16 ◽  
Author(s):  
Janka Mihalčová

AbstractThe contribution describes concrete example of application of tribotechnical methods for the determination of the bearing wear state in aircraft turboshaft engines. Tribotechnical methods, which will be mentioned, deal with qualitative and quantitative characterization of particles occurred in oil. Here belong method optical emission spectrometry method with rotating disc electrode for determination of chemical elements concentration in oil. Method of optical particles counting for detection of particles distribution according to their scale, determination of their number and ferrographic analysis. Exploitation of these methods make it possible to determine quickly and correctly the friction regime and wearing of friction pair that is washed by oil in observed engines.


2015 ◽  
Vol 30 (6) ◽  
pp. 1266-1273 ◽  
Author(s):  
Federica Aureli ◽  
Marilena D'Amato ◽  
Andrea Raggi ◽  
Francesco Cubadda

A reliable and sensitive analytical method for the simultaneous determination of size and mass concentration of silica nanoparticles sized 20–200 nm.


2002 ◽  
Vol 75 (5) ◽  
pp. 865-890 ◽  
Author(s):  
Chenchy J. Lin ◽  
W. L. Hergenrother ◽  
E. Alexanian ◽  
G. G. A. Böhm

Abstract Filler flocculation was followed for silica filled compounds containing various alkoxy silanes and non-silane type polar additives. The methodology employed in this paper permitted a quantitative characterization of filler flocculation and polymer-filler interactions after heating the compound under conditions that simulated vulcanization. With the addition of trialkoxy silanes, the reduction of filler flocculation and the degree of polymer-filler interactions were found to depend on the type and the concentration of silane added, and on the mixing drop temperature (Td) used. Greater polymer-filler interactions and flocculation suppression were obtained with a compound containing a tetrasulfane when compared to that containing either a disulfane or a monofunctional-silane. Polar additives such as an amine compound and a sugar alcohol did not reduce the silica flocculation during simulated vulcanization because they were dewetted from the silica surface upon heating. The filler flocculation process was monitored by following the change of dynamic storage moduli using an on-line rheometer. The flocculation process order and process constant were extracted from the non-linear regression analysis of the kinetic data. These kinetic parameters were used to quantify the suppression of filler flocculation by the additives used. Filler flocculation was found not to be affected by the vulcanization process because it occurred prior to the onset of cure.


Sign in / Sign up

Export Citation Format

Share Document