Fabrication of Custom Pattern Reinforced AZ31 Multilayer Composite Using Ultrasonic Spray Deposition

2016 ◽  
Author(s):  
Mina Bastwros ◽  
Gap-Yong Kim

Mimicking the unique hierarchical, multiscale structures of natural biological materials is a promising approach to create novel materials with outstanding properties. One of the challenges, however, is the lack of scalable fabrication methods capable of making such complex structures. In this study, a multilayer nanocomposite has been synthesized by incorporating an ultrasonic spray deposition technique. The spray deposition system was used to deposit nanoparticles on substrate foils, which were consolidated to synthesize the multilayer composite. A patterned mask was used to create micro-patterns with nanoscale structures. A magnesium alloy, AZ31, foils were used as the matrix material. A mixture of nano-silicon carbide (nano-SiC) and aluminum alloy, Al6061, particles was used as the reinforcement phase in the deposited patterns. A three point bend test and a small punch test were carried out to evaluate the mechanical properties. A multilayer composite consisting of circular micro-patterns with SiC nano-structure was successfully created. The patterned composite showed an enhancement in the flexural yield strength and the flexural ultimate strength of 43% and 30% respectively, compared with the uniform multilayer composite without the patterns.

Author(s):  
Mina Bastwros ◽  
Gap-Yong Kim ◽  
Jie Wang

Reinforcement with nano-sized particles offers a promising potential to significantly enhance the mechanical, electrical, and thermal properties of a metal matrix composite (MMC). One of the challenges of synthesizing nanocomposites, however, has been the dispersion and control of the nano-reinforcement materials. In this study, a laminate nanocomposite has been synthesized by incorporating ultrasonic spray deposition technique. An ultrasonic spray deposition system was used to deposit nano-particles on substrate foils, which were consolidated to synthesize a laminate composite. Aluminum 6061 (Al6061) alloy foils were used as the matrix material. Nano-silicon carbide (SiC) particles were used as the reinforcement phase (deposited layer). The sprayed foils were stacked together to form the composite. The composite was then consolidated by hot compaction in the semi-solid regime of the Al6061. A three point bend test was carried out to evaluate the mechanical properties. In addition, the suspension and spraying parameters that control the deposited microstructure was studied to help control the final properties of the deposited structure. The yield and ultimate flexural strength of the SiC sprayed Al6061 laminate composite showed an increase (32% and 15%, respectively) compared with that of the unsprayed sample (reference sample) processed at the same condition.


Materials ◽  
2003 ◽  
Author(s):  
Michael H. Santare ◽  
Wenzhong Tang ◽  
John E. Novotny ◽  
Suresh G. Advani

High-density polyethylene (HDPE) was used as the matrix material for a carbon nanotube (CNT) polymer composites. Multi-wall carbon nanotube composite films were fabricated using the melt processing method. Composite samples with 0%, 1%, 3% and 5% nanotube content by weight were tested. The mechanical properties of the films were measured by the small punch test and wear resistance was measured with a block-on-ring wear tester. Results show increases in the stiffness, peak load, work-to-failure and wear resistance with increasing nanotube content.


2016 ◽  
Vol 256 ◽  
pp. 205-215
Author(s):  
Mina M.H. Bastwros ◽  
Gap Yong Kim

Semi-solid sintering technique has been introduced to alter the interfaces of a metal laminate composite material. A thin layer of reinforcement nanoparticles was applied on substrate metallic sheets using an ultrasonic spray deposition method. The sheets were then stacked, pressed, and sintered in the semi-solid regime of the metallic sheet. The liquid phase present in the matrix material penetrates and diffuses into the nanoparticle layer during consolidation and helps to form a gradual, nanostructured interface. Aluminum (Al6061) and magnesium (AZ31) alloy foils were used as the matrix sheets while various species of reinforcement particles were investigated, including silicon carbide (SiC), silicon (Si), and a mix of Si+SiC. Multilayered metal composites with nanostructured interfaces were successfully consolidated and were evaluated by performing a three-point bend test. AZ31 composites reinforced with SiC nanoparticle interface showed an improvement of 49% in flexural yield strength when compared with a reference sample without such interfaces.


Author(s):  
C.T. Hu ◽  
C.W. Allen

One important problem in determination of precipitate particle size is the effect of preferential thinning during TEM specimen preparation. Figure 1a schematically represents the original polydispersed Ni3Al precipitates in the Ni rich matrix. The three possible type surface profiles of TEM specimens, which result after electrolytic thinning process are illustrated in Figure 1b. c. & d. These various surface profiles could be produced by using different polishing electrolytes and conditions (i.e. temperature and electric current). The matrix-preferential-etching process causes the matrix material to be attacked much more rapidly than the second phase particles. Figure 1b indicated the result. The nonpreferential and precipitate-preferential-etching results are shown in Figures 1c and 1d respectively.


Author(s):  
D. E. Luzzi ◽  
L. D. Marks ◽  
M. I. Buckett

As the HREM becomes increasingly used for the study of dynamic localized phenomena, the development of techniques to recover the desired information from a real image is important. Often, the important features are not strongly scattering in comparison to the matrix material in addition to being masked by statistical and amorphous noise. The desired information will usually involve the accurate knowledge of the position and intensity of the contrast. In order to decipher the desired information from a complex image, cross-correlation (xcf) techniques can be utilized. Unlike other image processing methods which rely on data massaging (e.g. high/low pass filtering or Fourier filtering), the cross-correlation method is a rigorous data reduction technique with no a priori assumptions.We have examined basic cross-correlation procedures using images of discrete gaussian peaks and have developed an iterative procedure to greatly enhance the capabilities of these techniques when the contrast from the peaks overlap.


2020 ◽  
Vol 38 (7A) ◽  
pp. 960-966
Author(s):  
Aseel M. Abdullah ◽  
Hussein Jaber ◽  
Hanaa A. Al-Kaisy

In the present study, the impact strength, flexural modulus, and wear rate of poly methyl methacrylate (PMMA) with eggshell powder (ESP) composites have been investigated. The PMMA used as a matrix material reinforced with ESP at two different states (including untreated eggshell powder (UTESP) and treated eggshell powder (TESP)). Both UTESP and TESP were mixed with PMMA at different weight fractions ranged from (1-5) wt.%. The results revealed that the mechanical properties of the PMMA/ESP composites were enhanced steadily with increasing eggshell contents. The samples with 5 wt.% of UTESP and TESP additions give the maximum values of impact strength, about twice the value of the pure PMMA sample. The calcination process of eggshells powders gives better properties of the PMMA samples compared with the UTESP at the same weight fraction due to improvements in the interface bond between the matrix and particles. The wear characteristics of the PMMA composites decrease by about 57% with increases the weight fraction of TESP up to 5 wt.%. The flexural modulus values are slightly enhanced by increasing of the ESP contents in the PMMA composites.


Polymers ◽  
2021 ◽  
Vol 13 (8) ◽  
pp. 1235
Author(s):  
Bidita Salahuddin ◽  
Rahim Mutlu ◽  
Tajwar A. Baigh ◽  
Mohammed N. Alghamdi ◽  
Shazed Aziz

Passive vibration control using polymer composites has been extensively investigated by the engineering community. In this paper, a new kind of vibration dampening polymer composite was developed where oriented nylon 6 fibres were used as the reinforcement, and 3D printed unoriented nylon 6 was used as the matrix material. The shape of the reinforcing fibres was modified to a coiled structure which transformed the fibres into a smart thermoresponsive actuator. This novel self-reinforced composite was of high mechanical robustness and its efficacy was demonstrated as an active dampening system for oscillatory vibration of a heated vibrating system. The blocking force generated within the reinforcing coiled actuator was responsible for dissipating vibration energy and increase the magnitude of the damping factor compared to samples made of non-reinforced nylon 6. Further study shows that the appropriate annealing of coiled actuators provides an enhanced dampening capability to the composite structure. The extent of crystallinity of the reinforcing actuators is found to directly influence the vibration dampening capacity.


2019 ◽  
Vol 809 ◽  
pp. 480-486
Author(s):  
Rohit George Sebastian ◽  
Christof Obertscheider ◽  
Ewald Fauster ◽  
Ralf Schledjewski

The growing use of composite materials has generated interest in improving and optimising composite manufacturing processes such as Liquid Composite Moulding (LCM). In LCM, dry preforms are placed in a mould and impregnated with the matrix material. The efficiency of filling the moulds can be improved by using Computational Fluid Dynamics (CFD) filling simulations during the design of the mould. As part of an on-going effort to develop a CFD tool for the simulation of LCM processes, a volume averaged energy balance equation has been derived and implemented in a custom OpenFOAM solver. The energy balance is implemented in a custom OpenFOAM solver with and without the pressure terms for comparison with results from RTM experiments. It is found that the pressure terms do not significantly influence the results for LCM processes.


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