A mechanism of grain nucleation during relaxation of the latent energy of junction disclinations in the course of plastic deformation

2005 ◽  
Vol 31 (12) ◽  
pp. 1015-1018 ◽  
Author(s):  
T. S. Orlova ◽  
A. E. Romanov ◽  
A. A. Nazarov ◽  
N. A. Enikeev ◽  
I. V. Alexandrov ◽  
...  
2021 ◽  
Vol 83 (3) ◽  
pp. 285-293
Author(s):  
Yu.V. Svirina ◽  
S.V. Kirikov ◽  
V.N. Perevezentsev

Plastic deformation of polycrystalline solids is accompanied by the appearance of linear rotational-type mesodefects at grain boundary ledges and triple junction of grains, such as starin induced junction disclinations. Junction disclinations generate long-range spatially inhomogeneous fields of elastic stresses, which significantly influence on the structure formation, strain hardening and fracture of materials. In present work a comparative analysis of the contributions of junction disclinations of different sign and strength to the plastic flow stress of a polycrystal is performed. The results of calculationsshow, that when a pile-up of lattice dislocations passes through the elastic field of disclinations, general regularities are observed.Regardless of the sign of disclination, it has a retarding effect on the plastic shear. The equilibrium distributions of the linear density and the density of the Burgers vector of dislocations pile-upretarded by the elastic field of disclination are calculated.It is shown that the largest number of dislocations is concentrated not in the pile-up head, as in classical dislocation pile-upsstoped near impenetrable barriers, but in its central part. The dependences of the critical stress of the passage of the head dislocation of the pile-up through the force barrier of disclination are calculated depending on the strength and sign of disclination, the number of dislocations in the pile-up, and the distance between the disclination and the slip plane of lattice dislocations.It is shown that the change in the sign of disclination significantly influences on the form of the equilibrium distribution of dislocations along the length of the pile-up, but practically does not affect the value of the critical shear stress. It is shown that for a fixed number of dislocations in the pile-up, the critical shear stress increases with the distance between the slip plane and disclination. Thus, when plastic deformation is localized, the greatest strengthening effect from the elastic field of junction disclination is achieved not near the boundary, but far from it.


The work of Taylor & Quinney quoted by Dr Bowden shows that after a certain amount of plastic deformation has occurred all the subsequent work of deformation appears as heat. Thus the mechanism by which heat is developed during plastic deformation is identical with that involved in the production of frictional heat. With continual sliding over the same surface, the of friction will be equal to the work of friction, the total amount of latent energy having been absorbed in the first period of sliding.


2021 ◽  
Vol 83 (3) ◽  
pp. 276-284
Author(s):  
A.S. Pupynin ◽  
S.V. Kirikov ◽  
V.N. Perevezentsev

The conditions of diffusional cavity nucleation in submicrocrystalline materials processed by the methods of intensive plastic deformation (equal-channel angular pressing, multiaxial forging, high pressure torsion, etc.) are analyzed. To date, the question of the mechanism of nucleation of cavities in such materials remains debatable due to the fact that the processing of materials by the methods of intensive plastic deformation is carried out at high hydrostatic pressures that prevent the appearance of pores. The possibility of diffusive nucleation of nanopores in the region of triple junctions of grains containing negative strain-induced wedge disclinations, generating high tensile stresses in the vicinity of triple junctions, comparable in magnitude to external hydrostatic pressure, is shown. Such junction disclinations inevitably occur at the grain junctions due to the heterogeneity of the plastic deformation through the ensemble of polycrystal grains. It is shown that an important condition for the nucleation of cavities is not only the presence of high internal tensile stresses from junction disclinations, but also an extremely high concentration of nonequilibrium strain-induced vacancies characteristic of submicrocrystalline metals, comparable in values to the vacancy concentration, at temperatures close to solidus. The influence of the strength of junction disclinations, the value of external hydrostatic pressure and the degree of supersaturation of the material by nonequilibriumstrain-induced vacancies on the rate of diffusional nucleation and the volume of critical pore nuclei is analyzed. It is established that in order to effectively suppress the process of pore formation in the grain boundary triple junctions, it is necessary to apply an external hydrostatic pressure that compensates for internal elastic fields from junction disclinations.


2008 ◽  
Vol 137 ◽  
pp. 1-8
Author(s):  
Ayrat A. Nazarov ◽  
Ramil’ T. Murzaev

Junction disclinations are important elements of the structure of nanostructured metals produced by severe plastic deformation (SPD). Effect of these defects on the formation energy of vacancies in grain boundaries (GBs) is studied by means of atomistic computer simulations. Estimates based on the calculations of vacancy formation energies suggest that at least two orders of magnitude increase of the GB diffusion coefficient can be expected due to junction disclinations in nanostructured metals.


Author(s):  
J. Temple Black

There are two types of edge defects common to glass knives as typically prepared for microtomy purposes: 1) striations and 2) edge chipping. The former is a function of the free breaking process while edge chipping results from usage or bumping of the edge. Because glass has no well defined planes in its structure, it should be highly resistant to plastic deformation of any sort, including tensile loading. In practice, prevention of microscopic surface flaws is impossible. The surface flaws produce stress concentrations so that tensile strengths in glass are typically 10-20 kpsi and vary only slightly with composition. If glass can be kept in compression, wherein failure is literally unknown (1), it will remain intact for long periods of time. Forces acting on the tool in microtomy produce a resultant force that acts to keep the edge in compression.


Author(s):  
L. Andrew Staehelin

Freeze-etched membranes usually appear as relatively smooth surfaces covered with numerous small particles and a few small holes (Fig. 1). In 1966 Branton (1“) suggested that these surfaces represent split inner mem¬brane faces and not true external membrane surfaces. His theory has now gained wide acceptance partly due to new information obtained from double replicas of freeze-cleaved specimens (2,3) and from freeze-etch experi¬ments with surface labeled membranes (4). While theses studies have fur¬ther substantiated the basic idea of membrane splitting and have shown clearly which membrane faces are complementary to each other, they have left the question open, why the replicated membrane faces usually exhibit con¬siderably fewer holes than particles. According to Branton's theory the number of holes should on the average equal the number of particles. The absence of these holes can be explained in either of two ways: a) it is possible that no holes are formed during the cleaving process e.g. due to plastic deformation (5); b) holes may arise during the cleaving process but remain undetected because of inadequate replication and microscope techniques.


Author(s):  
J. Temple Black

The output of the ultramicrotomy process with its high strain levels is dependent upon the input, ie., the nature of the material being machined. Apart from the geometrical constraints offered by the rake and clearance faces of the tool, each material is free to deform in whatever manner necessary to satisfy its material structure and interatomic constraints. Noncrystalline materials appear to survive the process undamaged when observed in the TEM. As has been demonstrated however microtomed plastics do in fact suffer damage to the top and bottom surfaces of the section regardless of the sharpness of the cutting edge or the tool material. The energy required to seperate the section from the block is not easily propogated through the section because the material is amorphous in nature and has no preferred crystalline planes upon which defects can move large distances to relieve the applied stress. Thus, the cutting stresses are supported elastically in the internal or bulk and plastically in the surfaces. The elastic strain can be recovered while the plastic strain is not reversible and will remain in the section after cutting is complete.


Author(s):  
J. Temple Black ◽  
William G. Boldosser

Ultramicrotomy produces plastic deformation in the surfaces of microtomed TEM specimens which can not generally be observed unless special preparations are made. In this study, a typical biological composite of tissue (infundibular thoracic attachment) infiltrated in the normal manner with an embedding epoxy resin (Epon 812 in a 60/40 mixture) was microtomed with glass and diamond knives, both with 45 degree body angle. Sectioning was done in Portor Blum Mt-2 and Mt-1 microtomes. Sections were collected on formvar coated grids so that both the top side and the bottom side of the sections could be examined. Sections were then placed in a vacuum evaporator and self-shadowed with carbon. Some were chromium shadowed at a 30 degree angle. The sections were then examined in a Phillips 300 TEM at 60kv.Carbon coating (C) or carbon coating with chrom shadowing (C-Ch) makes in effect, single stage replicas of the surfaces of the sections and thus allows the damage in the surfaces to be observable in the TEM. Figure 1 (see key to figures) shows the bottom side of a diamond knife section, carbon self-shadowed and chrom shadowed perpendicular to the cutting direction. Very fine knife marks and surface damage can be observed.


Author(s):  
M.A. Mogilevsky ◽  
L.S. Bushnev

Single crystals of Al were loaded by 15 to 40 GPa shock waves at 77 K with a pulse duration of 1.0 to 0.5 μs and a residual deformation of ∼1%. The analysis of deformation structure peculiarities allows the deformation history to be re-established.After a 20 to 40 GPa loading the dislocation density in the recovered samples was about 1010 cm-2. By measuring the thickness of the 40 GPa shock front in Al, a plastic deformation velocity of 1.07 x 108 s-1 is obtained, from where the moving dislocation density at the front is 7 x 1010 cm-2. A very small part of dislocations moves during the whole time of compression, i.e. a total dislocation density at the front must be in excess of this value by one or two orders. Consequently, due to extremely high stresses, at the front there exists a very unstable structure which is rearranged later with a noticeable decrease in dislocation density.


Author(s):  
D. L. Callahan

Modern polishing, precision machining and microindentation techniques allow the processing and mechanical characterization of ceramics at nanometric scales and within entirely plastic deformation regimes. The mechanical response of most ceramics to such highly constrained contact is not predictable from macroscopic properties and the microstructural deformation patterns have proven difficult to characterize by the application of any individual technique. In this study, TEM techniques of contrast analysis and CBED are combined with stereographic analysis to construct a three-dimensional microstructure deformation map of the surface of a perfectly plastic microindentation on macroscopically brittle aluminum nitride.The bright field image in Figure 1 shows a lg Vickers microindentation contained within a single AlN grain far from any boundaries. High densities of dislocations are evident, particularly near facet edges but are not individually resolvable. The prominent bend contours also indicate the severity of plastic deformation. Figure 2 is a selected area diffraction pattern covering the entire indentation area.


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