POLARIZATION-DEPENDENT SOFT X-RAY SPECTROSCOPIES

1997 ◽  
Vol 04 (02) ◽  
pp. 343-352 ◽  
Author(s):  
MAURIZIO SACCHI

A short overview is given of recent developments in the use of polarized X-rays. A few studies are chosen to exemplify the possible applications and the common underlying ideas of different spectroscopic techniques in the domain of soft X-rays. The analysis of resonant reflectivity of polarized X-rays from a magnetic sample is discussed in more detail.

Author(s):  
Romain Geneaux ◽  
Hugo J. B. Marroux ◽  
Alexander Guggenmos ◽  
Daniel M. Neumark ◽  
Stephen R. Leone

Attosecond science opened the door to observing nuclear and electronic dynamics in real time and has begun to expand beyond its traditional grounds. Among several spectroscopic techniques, X-ray transient absorption spectroscopy has become key in understanding matter on ultrafast time scales. In this review, we illustrate the capabilities of this unique tool through a number of iconic experiments. We outline how coherent broadband X-ray radiation, emitted in high-harmonic generation, can be used to follow dynamics in increasingly complex systems. Experiments performed in both molecules and solids are discussed at length, on time scales ranging from attoseconds to picoseconds, and in perturbative or strong-field excitation regimes. This article is part of the theme issue ‘Measurement of ultrafast electronic and structural dynamics with X-rays’.


1998 ◽  
Vol 4 (S2) ◽  
pp. 378-379
Author(s):  
Z. W. Chen ◽  
D. B. Wittry

A monochromatic x-ray microprobe based on a laboratory source has recently been developed in our laboratory and used for fluorescence excitation. This technique provides high sensitivity (ppm to ppb), nondestructive, quantitative microanalysis with minimum sample preparation and does not require a high vacuum specimen chamber. It is expected that this technique (MMXRF) will have important applications in materials science, geological sciences and biological science.Three-dimensional focusing of x-rays can be obtained by using diffraction from doubly curved crystals. In our MMXRF setup, a small x-ray source was produced by the bombardment of a selected target with a focused electron beam and a toroidal mica diffractor with Johann pointfocusing geometry was used to focus characteristic x-rays from the source. In the previous work ∼ 108 photons/s were obtained in a Cu Kα probe of 75 μm × 43 μm in the specimen plane using the fifth order reflection of the (002) planes of mica.


2018 ◽  
Vol 14 (S346) ◽  
pp. 83-87
Author(s):  
Vikram V. Dwarkadas

AbstractMassive stars lose a considerable amount of mass during their lifetime. When the star explodes as a supernova (SN), the resulting shock wave expands in the medium created by the stellar mass-loss. Thermal X-ray emission from the SN depends on the square of the density of the ambient medium, which in turn depends on the mass-loss rate (and velocity) of the progenitor wind. The emission can therefore be used to probe the stellar mass-loss in the decades or centuries before the star’s death.We have aggregated together data available in the literature, or analysed by us, to compute the X-ray lightcurves of almost all young supernovae detectable in X-rays. We use this database to explore the mass-loss rates of massive stars that collapse to form supernovae. Mass-loss rates are lowest for the common Type IIP supernovae, but increase by several orders of magnitude for the highest luminosity X-ray SNe.


1996 ◽  
Vol 06 (03n04) ◽  
pp. 523-530 ◽  
Author(s):  
M. YONEZAWA ◽  
Y. MATSUDA ◽  
F. NISHIYAMA

It is important for maintenance and understanding of health to make inquiries into the biological defence mechanisms. Yonezawa et al. came across an induction of yet unknown defence mechanisms in mice which acquired two types of radioresistance (decrease in bone-marrow death rate after midlethal exposure): one occured 2 weeks after preirradiation with 0.3–0.5 Gy and the other 2 months after 0.05–0.10 Gy of X-rays. To elucidate the acquired radioresistance induced after preirradiation with 0.5 Gy (in a shorter time case). recovery of blood cell counts after sublethal irradiation were measured in mice of ICR strain. Contrary to the common knowledge on radiation protection. recovery of blood cell counts of thrombocytes. leukocytes and erythrocytes after sublethal irradiation were not stimulated by the preirradiation. This study was planned to find some keys to elucidate the mechanism for the acquired radioresistance. Eleven elements. Cl. K. Ca. Cr. Mn. Fe. Ni. Cu. Zn. Se and Br. were analysed clearly in mice sera by PIXE.


Bakerian Lectures dealing with astronomical topics have occurred roughly every ten years during this century. They have therefore something of the character of reports on progress and one need read no further back than Hoyle’s ‘Review of recent developments in cosmology’ (Hoyle 1968) and Ryle’s ‘The nature of the cosmic radio sources’ (Ryle 1958) to discover the background against which are to be seen the dramatic changes of the ensuing period. It stretches from the conception of X-ray astronomy through its birth, with the discovery of the first non-solar source (Giacconi et al . 1962), to its maturity with the availability of satellites to provide long exposures. Nor is it any accident that the root κóσμoς is prominent in the titles of recent lectures for while those of Jeans, Eddington, Milne and Blacket were concerned with our Galaxy, the drama is now truly cosmic. Cosmic X-ray astronomy grew out of the study of the Sun and for this reason its founding father is Herbert Friedman. Giacconi describes well the early history of the subject (Giacconi & Gursky 1974) and tells how, in June 1962, having been interested in the idea by Rossi in September 1959, he and his colleagues detected flux coming neither from the Sun nor from the Moon. Friedman had discussed as early as 1956 ‘how his group obtained puzzling results, which might have been due to celestial X-ray fluxes’, and reported this at the I. A. U. meeting in Moscow in 1958. Stimulated by our solar studies with the Skylark rocket, similar thinking was taking place under the auspices of this Society. Mention of this was made at a conference in the United States in June 1961 (Boyd 1962) but a meeting of the Astronomy Working Group of the British National Committee on Space Research (N. C. S. P./34, 1959 a ) had discussed, in May 1959, the possibility, of mounting ‘Directive X-ray counters’ on the proposed U. K. -I satellite. The minute read ‘Current theories suggested that there may be objects in the sky with strong X-ray emission although inconspicuous visually. A search for these is a matter of great interest and importance.’ It is noteworthy that Hoyle, who had discussed Friedman’s speculations with him, was present at the meeting.


2020 ◽  
Vol 53 (4) ◽  
pp. 927-936 ◽  
Author(s):  
Andrew J. Morgan ◽  
Kevin T. Murray ◽  
Mauro Prasciolu ◽  
Holger Fleckenstein ◽  
Oleksandr Yefanov ◽  
...  

The ever-increasing brightness of synchrotron radiation sources demands improved X-ray optics to utilize their capability for imaging and probing biological cells, nano-devices and functional matter on the nanometre scale with chemical sensitivity. Hard X-rays are ideal for high-resolution imaging and spectroscopic applications owing to their short wavelength, high penetrating power and chemical sensitivity. The penetrating power that makes X-rays useful for imaging also makes focusing them technologically challenging. Recent developments in layer deposition techniques have enabled the fabrication of a series of highly focusing X-ray lenses, known as wedged multi-layer Laue lenses. Improvements to the lens design and fabrication technique demand an accurate, robust, in situ and at-wavelength characterization method. To this end, a modified form of the speckle tracking wavefront metrology method has been developed. The ptychographic X-ray speckle tracking method is capable of operating with highly divergent wavefields. A useful by-product of this method is that it also provides high-resolution and aberration-free projection images of extended specimens. Three separate experiments using this method are reported, where the ray path angles have been resolved to within 4 nrad with an imaging resolution of 45 nm (full period). This method does not require a high degree of coherence, making it suitable for laboratory-based X-ray sources. Likewise, it is robust to errors in the registered sample positions, making it suitable for X-ray free-electron laser facilities, where beam-pointing fluctuations can be problematic for wavefront metrology.


1958 ◽  
Vol 2 ◽  
pp. 303-312 ◽  
Author(s):  
Merlyn L. Salmon

AbstractFluorescent x-ray speorographic studies of mineral systems were begun in the Metallurgy Division of the Denver Research Institute in 1953. These studies were concerned with several techniques but the primary research emphasis was placed on a method involving conjunctive analyses by monochromatic x-ray absorptiometry and fluorescent x-ray spectrography.Experimental data for mineral systems with wide variations in matrix compositions exhibit departures from simple calibration curves relating intensity and concentration for an element in a series of samples analyzed by simple fluorescent x-ray spectrographic procedures.Absorptiometric measurements are made with a thin layer of the mineral sample as an absorption filter for the monochromatic x-rays emitted by the element in question. The results of these measurements provide information for improvement of the simple correlation of intensity and concentration by manipulation of the experimental data with various operations based on Beer's law of radiation absorption.The results of work at the Denver Research Institute indicated the feasibility of the fluorescent x-ray spectrographic-absorptiometric method and the current work is an extension of the study of basic fundamentals, mechanical factors and practical applications of the technique.


2017 ◽  
Vol 9 (5) ◽  
pp. 631-636 ◽  
Author(s):  
Mohamed Faisal Chevidikunnan ◽  
Amer Al Saif ◽  
Harish Pai K ◽  
Lawrence Mathias

AbstractBackgroundThe Q angle is a relevant clinical diagnostic measurement to detect various disorders of the knee. The common method used to measure the Q angle in the routine clinical practice is by radiography. An alternative to radiographic measurement is goniometry, by which exposure to x-rays can be avoided.ObjectivesTo compare and correlate the goniometric measurement of Q angle with radiographic measurement of the Q angle in patients with acute knee pain.MethodsWe selected 45 patient participants with a mean age of 32.5 years who satisfied the inclusion criteria for this study. All the patients underwent goniometric measurement of the Q angle followed by x-ray imaging of the entire lower limb. Later the bony prominences were marked on the x-ray image and the Q angle formed was measured using a protractor. The Pearson correlation coefficient between the goniometric and radiographic measurements was determined.ResultsWe found a significant relationship between Q angles obtained using a goniometer and x-ray imaging in the supine position (r = 0.91, P = 0.001). The mean difference between the goniometric measurement of Q angle and the radiographic measurement was 0.1°, which is not significant.ConclusionsGoniometry can be used to measure Q angle as accurately as radiography, and can be used as an inexpensive and radiation free alternative.


2021 ◽  
Vol 37 (5A) ◽  
pp. 166-171
Author(s):  
Israa S. Abed

The lungs are portion of a complex unit, enlarging and relaxing numerus times every day to supply oxygen and exude CO2. Lung disease might occur from troubles in any part of it. Carcinoma often called Cancer is the generally rising and it is the most harmful disease happened in humankind. Carcinoma occurs because of uncontrolled growth of malignant cells inside the tissues of the lungs. Earlier diagnosis of cancer can help save large numbers of lives, while any delay or fail in detection may cause additional serious problems leading to sudden fatal death. The objective of this study is to design an automated system with an ability to improve the detection process in order to perform advanced recognition of the disease. The diagnosis techniques include: X-rays, MRI, CT images etc. X-ray is the common and low-cost technique that is widely used and it is relatively available for everyone. Rather than new techniques like CT and MRI, X-ray is human dependable, meaning it needs a Doctor and X-ray specialist in order to determine lung cases, so developing a system which can enhance and aid in diagnosis, can help specialist to determine cases in easily.


1995 ◽  
Vol 39 ◽  
pp. 771-779 ◽  
Author(s):  
Christina Streli ◽  
V. Bauer ◽  
P. Wobrauschek

Total Reflection X-ray Fluorescence Analysis (TXRF) has been proved to be well suited for the energy dispersive analysis of light elements, as B, C, N, O, F, Na, Mg,.,. using a special spectrometer. It is equipped with a Ge(HP) detector offering a sufficient detection efficiency from 180 eV upwards. The obtainable detection limits especially of the light elements are mainly influenced by the excitation source, which should provide a large number of photons with an energy near the K-absorption edge of these elements (from 200 eV upwards). Commercially available X-ray tubes do not offer characteristic X-rays in that range. In former experiments a windowless X-ray tube was built to prevent the low energy X-rays from being attenuated in the Be window. Experiments have been performed using Cu as anode material.


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