scholarly journals Investigating the Three-Dimensional Microstructural Characteristics of Lithium-Sulfur Electrodes with X-ray Micro-Tomography

2017 ◽  
Vol 77 (11) ◽  
pp. 447-455 ◽  
Author(s):  
Chun Tan ◽  
Sohrab Randjbar Daemi ◽  
Daniel J.L. Brett ◽  
Paul R. Shearing
2010 ◽  
pp. 109-117 ◽  
Author(s):  
Neda Motchurova-Dekova ◽  
David Harper

Synchrotron radiation X-ray tomographic microscopy (SRXTM) is a non-destructive technique for the investigation and visualization of the internal features of solid opaque objects, which allows reconstruction of a complete three-dimensional image of internal structures by recording of the differences in the effects on the passage of waves of energy reacting with those structures. Contrary to X-rays, produced in a conventional X-ray tube, the intense synchrotron light beams are sharply focused like a laser beam. We report encouraging results from the use of SRXTM for purely taxonomic purposes in brachiopods: an attempt to find a non-destructive and more efficient alternative to serial sectioning and several other methods of dissection together with the non-destructive method of X-ray computerised micro-tomography. Two brachiopod samples were investigated using SRXTM. In ?Rhynchonella? flustracea it was possible to visualise the 3D shape of the crura and dental plates. In Terebratulina imbricata it was possible to reveal the form of the brachidium. It is encouraging that we have obtained such promising results using SRXTM with our very first two fortuitous samples, which had respectively fine-grained limestone and marl as infilling sediment, in contrast to the discouraging results communicated to us by some colleagues who have tested specimens with such infillings using X-ray micro-tomography. In future the holotypes, rare museum specimens or delicate Recent material may be preferentially subjected to this mode of analysis.


2020 ◽  
Vol 10 (14) ◽  
pp. 4898
Author(s):  
Hailing Shi ◽  
Jerome Hosdez ◽  
Thomas Rougelot ◽  
Shouyi Xie ◽  
Jianfu Shao ◽  
...  

Creep tests are commonly performed to characterize time-dependent deformation of geological materials. Classical measuring methods are not suitable for long term tests and not able to provide full three-dimensional strain fields. In this study, Digital Volume Correlation (DVC) is applied to X-ray micro-tomography (XRMT) images from creep tests on a hard clayey rock. In situ uniaxial compression creep tests are performed under different levels of stress and with different loading orientations with respect to the structural anisotropy of rock. Based on the XRMT images taken during the creep tests, DVC is applied to compute the full three dimensional strain fields and global averages strains of tested samples. The effects of bedding planes and hard inclusions on the non-uniform distribution of strains are analyzed.


2019 ◽  
Vol 21 (8) ◽  
pp. 4145-4154 ◽  
Author(s):  
Chun Tan ◽  
Matthew D. R. Kok ◽  
Sohrab R. Daemi ◽  
Daniel J. L. Brett ◽  
Paul R. Shearing

A sulfur electrode was imaged with X-ray micro and nano computed tomography for the modelling of effective molecular diffusivity and electrical conductivity through flux based simulations.


2014 ◽  
Vol 88 (4) ◽  
pp. 633-635 ◽  
Author(s):  
Imran A. Rahman ◽  
Selena Y. Smith

‘Virtual paleontology’ entails the use of computational methods to assist in the three-dimensional (3-D) visualization and analysis of fossils, and has emerged as a powerful approach for research on the history of life. Three-dimensional imaging techniques allow poorly understood or previously unknown anatomies of fossil plants, invertebrates, and vertebrates, as well as microfossils and trace fossils, to be described in much greater detail than formerly possible, and are applicable to a wide range of preservation types and specimen sizes (Table 1). These methods include non-destructive high-resolution scanning technologies such as conventional X-ray micro-tomography and synchrotron-based X-ray tomography. In addition, form and function can be rigorously investigated through quantitative analysis of computer models, for example finite-element analysis.


2003 ◽  
Vol 788 ◽  
Author(s):  
Predrag Kisa ◽  
Patrick Fisher ◽  
Al Olszewski ◽  
Ian Nettleship ◽  
Nicholas G. Eror

ABSTRACTThis study investigated the microstructural characteristics of directionally solidified freeze-dried silica sols. Porous structures were formed by depositing silica sol on silicon (100) single crystals. The deposited sols were unidirectionaly solidified by placing the silicon substrate on a copper block immersed in liquid nitrogen and then subsequently freeze-dried. Freeze drying removal of ice crystals created three-dimensional pore channels ranging from 3 to10 micrometers in diameter aggregated in grain like colonies 50–100 micrometers in diameter. Pore size, spacing, colony size and microstructure were determined using optical microscopy (OM) and scanning electron microscopy (SEM) while the structure of the amorphous SiO2 was characterized by X-ray diffraction (XRD). The microstructure results are compared and contrasted with silica aerogel obtained through conventional processing using supercritical CO2.


2016 ◽  
Vol 43 (10) ◽  
pp. 1002005 ◽  
Author(s):  
段浩 Duan Hao ◽  
吴圣川 Wu Shengchuan ◽  
徐忠伟 Xu Zhongwei ◽  
张志良 Zhang Zhiliang ◽  
阚前华 Kan Qianhua ◽  
...  

IAWA Journal ◽  
2013 ◽  
Vol 34 (4) ◽  
pp. 408-424 ◽  
Author(s):  
Craig R. Brodersen

High-resolution X-ray micro-tomography (μCT) has emerged as one of the most promising new tools available to wood anatomists to study the three-dimensional organization of xylem networks. This non-destructive method faithfully reproduces the spatial relationships between the different cell types and allows the user to explore wood anatomy in new and innovative ways. With μCT imaging, the sample can be visualized in any plane and is not limited to a single section or exposed plane. Conventional CT software aids in the visualization of wood structures, and newly developed custom software can be used to rapidly automate the data extraction process, thereby accelerating the rate at which samples can be analyzed for research. In this review the origins of xylem reconstructions using traditional methods are discussed, as well as the current applications of μCT in plant biology and an overview of pertinent technical considerations associated with this technique. μCT imaging offers a new perspective on wood anatomy and highlights the importance of the relationships between wood structure and function.


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