Microstructure Evolution of High Capacity Anode Electrode By in-Situ and in-Operando X-Ray Nano-CT

2016 ◽  
Keyword(s):  
Microstructure Evolution ◽  
High Capacity ◽  
X Ray ◽  
Anode Electrode ◽  
In Operando

scholarly journals Microstructure evolution during the isostructural decomposition of TiAlN—A combined in-situ small angle x-ray scattering and phase field study

2013 ◽  
Vol 113 (21) ◽  
pp. 213518 ◽  
Author(s):  
A. Knutsson ◽  
J. Ullbrand ◽  
L. Rogström ◽  
N. Norrby ◽  
L. J. S. Johnson ◽  
...  
Keyword(s):  
Field Study ◽  
Microstructure Evolution ◽  
Phase Field ◽  
Small Angle ◽  
X Ray ◽  
X Ray Scattering ◽  
Ray Scattering

Versatile variable temperature insert at the DEIMOS beamline forin situelectrical transport measurements

2016 ◽  
Vol 23 (3) ◽  
pp. 652-657 ◽  
Author(s):  
L. Joly ◽  
B. Muller ◽  
E. Sternitzky ◽  
J.-G. Faullumel ◽  
A. Boulard ◽  
...  
Keyword(s):  
Absorption Spectroscopy ◽  
Electrical Transport ◽  
Tunnel Junctions ◽  
Variable Temperature ◽  
Electronic Devices ◽  
X Ray ◽  
In Operando ◽  
X Ray Absorption ◽  
Multifunctional Properties

The design and the first experiments are described of a versatile cryogenic insert used for its electrical transport capabilities. The insert is designed for the cryomagnet installed on the DEIMOS beamline at the SOLEIL synchrotron dedicated to magnetic characterizations through X-ray absorption spectroscopy (XAS) measurements. This development was spurred by the multifunctional properties of novel materials such as multiferroics, in which, for example, the magnetic and electrical orders are intertwined and may be probed using XAS. The insert thus enables XAS toin situprobe this interplay. The implementation of redundant wiring and careful shielding also enables studies on operating electronic devices. Measurements on magnetic tunnel junctions illustrate the potential of the equipment toward XAS studies ofin operandoelectronic devices.

Quick scanning monochromator for millisecond in situ and in operando X-ray absorption spectroscopy

2015 ◽  
Vol 86 (9) ◽  
pp. 093905 ◽  
Author(s):  
O. Müller ◽  
D. Lützenkirchen-Hecht ◽  
R. Frahm
Keyword(s):  
Absorption Spectroscopy ◽  
X Ray ◽  
In Operando ◽  
X Ray Absorption

scholarly journals Functional materials analysis usingin situandin operandoX-ray and neutron scattering

IUCrJ ◽  
2015 ◽  
Vol 2 (2) ◽  
pp. 292-304 ◽  
Author(s):  
Vanessa K. Peterson ◽  
Christine M. Papadakis
Keyword(s):  
Neutron Scattering ◽  
State Of The Art ◽  
Functional Materials ◽  
Materials Analysis ◽  
X Ray ◽  
Materials Research ◽  
Recent Developments ◽  
In Operando ◽  
Types Of Information

In situandin operandostudies are commonplace and necessary in functional materials research. This review highlights recent developments in the analysis of functional materials using state-of-the-artin situandin operandoX-ray and neutron scattering and analysis. Examples are given covering a number of important materials areas, alongside a description of the types of information that can be obtained and the experimental setups used to acquire them.

In Situ X-Ray Techniques for Electrochemical Interfaces

2021 ◽  
Vol 14 (1) ◽  
Author(s):  
Bruna F. Baggio ◽  
Yvonne Grunder
Keyword(s):  
Annual Review ◽  
Publication Date ◽  
Time Resolved ◽  
X Ray ◽  
X Ray Scattering ◽  
Recent Developments ◽  
In Operando ◽  
Electrochemical Interfaces ◽  
Ray Scattering

This article reviews progress in the study of materials using X-ray-based techniques from an electrochemistry perspective. We focus on in situ/in operando surface X-ray scattering, X-ray absorption spectroscopy, and the combination of both methods. The background of these techniques together with key concepts is introduced. Key examples of in situ and in operando investigation of liquid–solid and liquid–liquid interfaces are presented. X-ray scattering and spectroscopy have helped to develop an understanding of the underlying atomic and molecular processes associated with electrocatalysis, electrodeposition, and battery materials. We highlight recent developments, including resonant surface diffraction and time-resolved studies. Expected final online publication date for the Annual Review of Analytical Chemistry, Volume 14 is June 2021. Please see http://www.annualreviews.org/page/journal/pubdates for revised estimates.

scholarly journals In situ electron microscopy and X-ray photoelectron spectroscopy for high capacity anodes in next-generation ionic liquid-based Li batteries

2018 ◽  
Vol 279 ◽  
pp. 136-142 ◽  
Author(s):  
Tetsuya Tsuda ◽  
Akihito Imanishi ◽  
Teruki Sano ◽  
Amane Sawamura ◽  
Toshiki Kamidaira ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Ionic Liquid ◽  
Photoelectron Spectroscopy ◽  
High Capacity ◽  
Next Generation ◽  
X Ray ◽  
In Situ Electron Microscopy ◽  
Li Batteries
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