scholarly journals The Effect of Fly Ash on Some Surface Characteristics and Microstructure of β-C2S

1997 ◽  
Vol 15 (6) ◽  
pp. 407-417
Author(s):  
Kh.A. Khalil ◽  
A.A. Amer
Keyword(s):  
Electron Microscope ◽  
Fly Ash ◽  
Scanning Electron Microscope ◽  
Specific Surface ◽  
Surface Area ◽  
Nitrogen Adsorption ◽  
Surface Characteristics ◽  
Ash Content ◽  
Sem Investigation ◽  
Scanning Electron

The effect of the addition of fly ash (0–15 wt. %) on the surface characteristics of β-C2S and its microstructure was investigated using nitrogen adsorption at −196°C together with scanning electron microscope (SEM) techniques. The results obtained revealed that the addition of fly ash up to 5 wt. % increased the specific surface area by 32% followed by a decrease of 34% when the fly ash content was increased up to 15 wt. %. SEM investigation showed that the hydrates produced form an outer shell which coats the fly ash particles.

Cypsela morphology of Cirsium sect. Cirsium (Asteraceae) taxa in Turkey

Biologia ◽  
2011 ◽  
Vol 66 (6) ◽  
Author(s):  
Serkan Köstekci ◽  
Turan Arabaci
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Surface Characteristics ◽  
Taxonomic Significance ◽  
Sem Investigation ◽  
Scanning Electron

AbstractIn this study, the cypsela morphology of 21 (14 species) of the 28 (17 species) Turkish Cirsium Mill. sect. Cirsium (Asteraceae) taxa was examined by stereomicroscope and scanning electron microscope (SEM). The shapes of cypselas are oblong, obovate, narrowly obovate and oblanceolate. The taxa were divided into 7 main types according to the results of SEM investigation on cypsela surface characteristics as: scalariform, ribbed, scrobiculate-ribbed, scrobiculate, scrobiculate-reticulate, reticulate and bireticulate. Taxonomic significance of cypsela morphology is discussed. It is shown that cypsela features can be used as distinguishing characteristics in some Cirsium sect. Cirsium species.

scholarly journals Characterization of Alum Sludge for Reuse and Disposal

2012 ◽  
Vol 8 (4) ◽  
Author(s):  
Hanim Awab ◽  
P.T. Thanalechumi Paramalinggam ◽  
Abdull Rahim Mohd Yusoff
Keyword(s):  
Heavy Metals ◽  
Particle Size ◽  
Electron Microscope ◽  
Water Treatment ◽  
Scanning Electron Microscope ◽  
Bulk Density ◽  
Surface Area ◽  
Particle Density ◽  
Ash Content ◽  
Scanning Electron

The properties of spent drinking water treatment sludge (WTS) were investigated to determine its physical and chemical properties. WTS was obtained from the Semanggar Water Treatment Plant, Kota Tinggi, Johore, Malaysia. Bulk density, particle density, porosity, surface area, particle size, moisture content, ash content, chemical composition, leachability of heavy metals, pH and the total organic carbon (TOC) were determined. Surface and other physicochemical properties were also studied using the scanning electron microscope (SEM), field emission scanning electron microscope (FESEM), X-ray diffractometer (XRD), TGA, FTIR, BET single point surface area analyzer, and TOC analyzer. Results showed that the particle size, bulk density and particle density of WTS were 2-5 μm, 0.831 ± 0.061 g/cm3 and 2.66 ± 0.029 g/cm3, respectively. The porosity was 68-69% with surface of 38.92 m2/g and ash content of 67%, reflecting the high TOC of 1440.37±14.71. The sludge contained 29% moisture and showed a pH value of 4.28 in solution. Analysis of acid digest indicated a high content of Al and Fe. The WTS were shown to leach very low levels of selected heavy metals.

Preparation of Pd/PPy/Foam-Ni Electrode and its Electrocatalytic Hydrodechlorination of Dichlorophenols

2021 ◽  
Vol 1035 ◽  
pp. 1078-1088
Author(s):  
Zhen Peng Ma ◽  
Shu Xia Zhang ◽  
Zhi Gang Yang
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Specific Surface ◽  
Surface Area ◽  
Removal Efficiency ◽  
Specific Surface Area ◽  
Supporting Electrolyte ◽  
Electrocatalytic Hydrogenation ◽  
Ni Substrate ◽  
Scanning Electron

Based on mechanism of ECH (Electrocatalytic Hydrogenation),the Pa/PPy/Foam-Ni (Pd/PPY/Ni) prepared by electrical depositing was used as cathode to detoxifythree kinds of dichlorophenol (DCP) and improve their biodegradability. According to the dechloridation ability of electrodes prepared under different conditions, the factors were optimized. The removal efficiency of 2,4-dichlorophenol（2,4-DCP）reaches 64.45% when the supporting electrolyte is p-toluenesulfonic acid and the voltage is 0.6V and polymerizing time is 20mins. Analyzing the photograph from SEM (Scanning Electron Microscope), it shows that PPy (PolyPyrrole) changes depositing properties of Pa on foam-Ni substrate, which increases specific surface area and special ductility so as to benefit Pd to deposite on Ni substrate and improve ECH.

scholarly journals Micropore Structure and Fractal Characteristics of Low-Permeability Coal Seams

2018 ◽  
Vol 2018 ◽  
pp. 1-15 ◽  
Author(s):  
Guang-zhe Deng ◽  
Rui Zheng
Keyword(s):  
Fractal Dimension ◽  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Coal Seam ◽  
Linear Relationship ◽  
Surface Area ◽  
Pore Volume ◽  
Low Permeability ◽  
Coal Seams ◽  
Scanning Electron

With the raw coal from a typical low-permeability coal seam in the coalfield of South Junger Basin in Xinjiang as the research object, this paper examined six kinds of coal samples with different permeabilities using a scanning electron microscope and a low-temperature nitrogen adsorption test that employed a JSM-6460LV high-resolution scanning electron microscope and an ASAP2020 automatic specific surface area micropore analyzer to measure all characteristic micropore structural parameters. According to fractal geometry theory, four fractal dimension calculation models of coal and rock were established, after which the pore structure characteristic parameters were used to calculate the fractal dimensions of the different coal seams. The results show that (1) the low-permeability coal seam in the coalfield of South Junger Basin in Xinjiang belongs to mesoporous medium, with a certain number of large pores and no micropores. The varying adsorption capacities of the different coal seams were positively correlated with pore volume, surface area, and the mesoporous surface area proportions, from which it was concluded that mesopores were the main contributors to pore adsorption in low-permeability coal seams. (2) The raw coal pore fractal dimension had a negative linear relationship to average pore size, a positive linear relationship with total pore volume, total surface area, and adsorption capacity, and a positive correlation with the mesoporous surface area proportion; that is, the higher the fractal dimension, the larger the pore volume and surface area of the raw coal. (3) The permeability of the low-permeability coal seam had a phase correlation with the micropore development degree; that is, the permeability had a phase negative correlation with the pore distribution fractal dimension, and there was a positive correlation between permeability and porosity. These results are of theoretical significance for the clean exploitation of low-permeability coal seam resources.

Geopolymer Microstructure and Hydration Mechanism of Alkali-Activated Fly Ash-Based Geopolymer

2011 ◽  
Vol 374-377 ◽  
pp. 1481-1484 ◽  
Author(s):  
Yao Jun Zhang ◽  
Hai Hong Li ◽  
Ya Chao Wang ◽  
De Long Xu
Keyword(s):  
Electron Microscope ◽  
Fly Ash ◽  
Scanning Electron Microscope ◽  
Average Particle Size ◽  
Three Dimensional ◽  
Alkaline Condition ◽  
Average Particle ◽  
Hydration Mechanism ◽  
Alkali Activated ◽  
Scanning Electron

The microstructure and hydration mechanism of alkali-activated fly ash-based geopolymer were studied by means of scanning electron microscope (SEM) coupled with energy dispersive X-ray analysis (EDXA) and field emission scanning electron microscope (FESEM). The FESEM photomicrographs indicted that the fly ash-based geopolymer showed three dimensional frameworks with an average particle size of 50 nm. EDXA results demonstrated that the Na-PSS type geopolymer was produced via the disintegration of Si-O-Al and Si-O-Si chemical bonds and the polycondensation reaction between [SiO4]4-and [AlO4]5- tetrahedrons in spherical fly ash particles under alkaline condition.

Influence of Mixture Proportion and Curing Condition on Contribution of Fly Ash to Strength of Concrete

2006 ◽  
Vol 302-303 ◽  
pp. 235-241 ◽  
Author(s):  
F.-R. Wu ◽  
Yoshihiro Masuda ◽  
S. Nakamura ◽  
S. Sato
Keyword(s):  
Fly Ash ◽  
Specific Surface ◽  
Surface Area ◽  
Specific Surface Area ◽  
Cement Content ◽  
Ash Content ◽  
K Value ◽  
Fly Ash Concrete ◽  
Curing Condition ◽  
Strength Difference

To investigate the strength efficiency of fly ash in concrete, the contribution of fly ash to strength, k value was calculated with the equation: the strength difference between fly ash concrete and control concrete with no fly ash due to the different fly ash content divides by the strength difference between both control concrete with no fly ash due to the different cement content which equals to the former different fly ash content. The k values were organized with fly ash specific surface area, concrete curing condition and age of specimens. Based on a large number of data collected from several proceedings and journals published in Japan during 1981 to 2003, the influences of fly ash property, mixture proportion and curing condition on k value were investigated. Within the range of study the following observations were made: (1) When fly ash concrete kept in moist curing, the k value of fly ash with specific surface area from 250 to 500 m2/kg is averagely 0.5 to 0.6 or higher at an age of 91 days and later, whereas that of fly ash with specific surface area from 150 to 250 m2/kg is around 0.4 to 0.5, and with some cases contributing little to the strength. (2) In the range of a portland cement content of 250 to 450 kg/m3, the strength contribution tends to increase as the cement content increases. (3) The contributions of fly ash to strength at 91 and 364 days are 1.44 to 1.97 times as large as those at 28 days, respectively, by standard curing, but conversely decrease to 0.75 to 0.79 times those at 28 days by air curing.

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