Compression molding of algae fiber and epoxy composites: Modeling of elastic modulus

2016 ◽  
Vol 37 (19) ◽  
pp. 1202-1216 ◽  
Author(s):  
Alejandra Constante ◽  
Selvum Pillay

The demand for natural fiber composites in the automotive industry in both Europe and the United States has been forecasted to increase in the coming years. The natural fiber composites based on highly commercialized fibers such as flax, hemp, and sisal has grown to become an important sector of polymeric composites. However, little attention has been addressed to expanding natural fiber composites to include new sources of emerging natural reinforcements, such as reclaimed algae fibers, that have a multiple environmental benefits. Not only are extracted algae fibers biodegradable, the reclamation process has the added benefit of restoring health of waterways choked with algae. This study focuses on the processability of algae fiber–epoxy composites. Short fibers, chemically extracted from raw reclaimed algae, were prepared for natural fiber composite products in two ways. First, randomly oriented mats were produced using the wet-laid process to create layered, compression-molded laminates. Second, loose fibers were dispersed directly into the thermoset matrix to produce a bulk molding compound that was further compression molded into composite lamina. The effect of processing variables such as compaction pressure, temperature, and time were addressed. Moreover, the effect of fiber volume fraction ( υf) and fiber form were considered. Enhanced mechanical properties were found when 56% υf algae fiber was used for the compression-molded laminates composite. This variant exhibited an improvement on the flexural and tensile modulus of 70% and 86% when compared to the neat epoxy. However, the volume of porosity on the same variant was 11% due to lack of compression in some of the fibers. The effect of porosity on the theoretical stiffness was estimated by using the Cox–Krenchel model. Furthermore, an empirical exponential model was formulated to characterize the multi-scale effect of compaction pressure on the overall fiber volume fraction, υf.

2021 ◽  
Vol 6 (1) ◽  
pp. 30-37
Author(s):  
Sri Hastuti ◽  
Herru Santosa Budiono ◽  
Diki Ilham Ivadiyanto ◽  
Muhammad Nurdin Nahar

Inovasi baru serat dari sabut kelapa dimanfaatkan untuk meningkatkan nilai ekonomis dari serat sabut kelapa, oleh karena itu dirancanglah pendayagunaan serat dari sabut kelapa untuk penguat komposit dengan material serat alam yang biodegradable. Hal ini untuk mendukung penggunaan komposit yang ramah terhadap lingkungan dan mengurangi penggunaan material komposit serat sintetis yang polutan. Tujuan penelitian adalah menganalisis sifat mekanik pada komposit serat alam bermaterial serat dari sabut kelapa yang ramah lingkungan. Metode penelitian pembuatan komposit berpenguat serat dari sabut kelapa dilakukan treatment NaOH 15% selama 5 jam dan fraksi volume serat 10 %, 15 %, dan 20 %. Komposit  serat dari sabut kelapa dengan matriks UPRs 157 BQTN dengan hardener MEXPO. Pengujian mekanik dilakukan uji bending menggunakan standar ASTM D790 dan uji impak  menggunakan standar ASTM D5941.  Pengujian impak komposit serat alam menunjukkan ketangguhan impak komposit pada fraksi volume serat 20% dengan nilai 0.017588J/mm2. Hasil pengujian menunjukkan peningkatan fraksi volume serta berpengaruh terhadap peningkatan kekuatan bending komposit serat dari sabut kelapa  dengan kekuatan optimum bending pada fraksi volume serat 10% dengan nilai 44,33N/mm2. Hal ini menunjukkan peningkatan fraksi volume serat dengan perendaman NaOH 15% akan meningkatkan sifat mekanik bending dan impak komposit. Perendaman NaOH memberikan pengaruh daya serap sabut kelapa terhadap matrik Unsaturated Polyester yang dapat meningkatkan daya rekat antara penguat serat dengan matrik sehingga meningkatkan sifat mekanik bending dan impak komposit. ABSTRACT The innovation of coco fiber is used to increase the economic value of coconut coir, therefore the utilization of coconut fiber for reinforcing composites with biodegradable natural fiber material is designed. This is to support the use of composites that are friendly to the environment and reduce the use of pollutant synthetic fiber composite materials. The research objective was to analyze the mechanical properties of natural fiber composites with environmentally friendly coconut fiber as material. The research method of making fiber-reinforced composites from coconut coir was carried out by 15% NaOH treatment for 5 hours and a fiber volume fraction of 10%, 15%, and 20%. Composite fiber from coconut coir with UPRs 157 BQTN matrix with MEXPO hardener. Mechanical testing is carried out using the ASTM D790 standard and the impact test using the ASTM D5941 standard. The impact test of natural fiber composites showed the impact toughness of the composite at a fiber volume fraction of 20% with a value of 0.017588 J/ mm2. The test results showed an increase in volume fraction and an effect on the increase in the bending strength of coconut fiber composites with the optimum bending strength at a fiber volume fraction of 10% with a value of 44.33N /mm2. This shows that the increase in fiber volume fraction by immersion in 15% NaOH will increase the bending mechanical properties and the impact of the composite. Soaking NaOH has an effect on the absorption power of coconut coir on the Unsaturated Polyester matrix which can increase the adhesion between the fiber reinforcement and the matrix thereby increasing the bending mechanical properties and impact of the composite.


Fibers ◽  
2020 ◽  
Vol 8 (10) ◽  
pp. 62
Author(s):  
Mike R. Bambach

Recent decades have seen substantial interest in the use of natural fibers in continuous fiber reinforced composites, such as flax, jute and hemp. Considering potential applications, it is of particular interest how natural fiber composites compare to synthetic fiber composites, such as glass and carbon, and if natural fibers can replace synthetic fibers in existing applications. Many studies have made direct comparisons between natural and synthetic fiber composites via material coupon testing; however, few studies have made such direct comparisons of full structural members. This study presents compression tests of geometrically identical structural channel sections fabricated from fiber-epoxy composites of flax, jute, hemp, glass and carbon. Glass fiber composites demonstrated superior tension material coupon properties to natural fiber composites. However, for the same fiber mass, structural compression properties of natural fiber composite channels were generally equivalent to, or in some cases superior to, glass fiber composite channels. This indicates there is substantial potential for natural fibers to replace glass fibers in structural compression members. Carbon fiber composites were far superior to all other composites, indicating little potential for replacement with natural fibers.


2021 ◽  
pp. 002199832110047
Author(s):  
Mahmoud Mohamed ◽  
Siddhartha Brahma ◽  
Haibin Ning ◽  
Selvum Pillay

Fiber prestressing during matrix curing can significantly improve the mechanical properties of fiber-reinforced polymer composites. One primary reason behind this improvement is the generated compressive residual stress within the cured matrix, which impedes cracks initiation and propagation. However, the prestressing force might diminish progressively with time due to the creep of the compressed matrix and the relaxation of the tensioned fiber. As a result, the initial compressive residual stress and the acquired improvement in mechanical properties are prone to decline over time. Therefore, it is necessary to evaluate the mechanical properties of the prestressed composites as time proceeds. This study monitors the change in the tensile and flexural properties of unidirectional prestressed glass fiber reinforced epoxy composites over a period of 12 months after manufacturing. The composites were prepared using three different fiber volume fractions 25%, 30%, and 40%. The results of mechanical testing showed that the prestressed composites acquired an initial increase up to 29% in the tensile properties and up to 32% in the flexural properties compared to the non-prestressed counterparts. Throughout the 12 months of study, the initial increase in both tensile and flexural strength showed a progressive reduction. The loss ratio of the initial increase was observed to be inversely proportional to the fiber volume fraction. For the prestressed composites fabricated with 25%, 30%, and 40% fiber volume fraction, the initial increase in tensile and flexural strength dropped by 29%, 25%, and 17%, respectively and by 34%, 26%, and 21%, respectively at the end of the study. Approximately 50% of the total loss took place over the first month after the manufacture, while after the sixth month, the reduction in mechanical properties became insignificant. Tensile modulus started to show a very slight reduction after the fourth/sixth month, while the flexural modulus reduction was observed from the beginning. Although the prestressed composites displayed time-dependent losses, their long-term mechanical properties still outperformed the non-prestressed counterparts.


Author(s):  
Faris M. AL-Oqla

The available potential plant waste could be worthy material to strengthen polymers to make sustainable products and structural components. Therefore, modeling the natural fiber polymeric-based composites is currently required to reveal the mechanical performance of such polymeric green composites for various green products. This work numerically investigates the effect of various fiber types, fiber loading, and reinforcement conditions with different polymer matrices towards predicting the mechanical performance of such natural fiber composites. Cantilever beam and compression schemes were considered as two different mechanical loading conditions for structural applications of such composite materials. Finite element analysis was conducted to modeling the natural fiber composite materials. The interaction between the fibers and the matrices was considered as an interfacial friction force and was determined from experimental work by the pull out technique for each polymer and fiber type. Both polypropylene and polyethylene were considered as composite matrices. Olive and lemon leaf fibers were considered as reinforcements. Results have revealed that the deflection resistance of the natural fiber composites in cantilever beam was enhanced for several reinforcement conditions. The fiber reinforcement was capable of enhancing the mechanical performance of the polymers and was the best in case of 20 wt.% polypropylene/lemon composites due to better stress transfer within the composite. However, the 40 wt.% case was the worst in enhancing the mechanical performance in both cantilever beam and compression cases. The 30 wt.% of polyethylene/olive fiber was the best in reducing the deflection of the cantilever beam case. The prediction of mechanical performance of natural fiber composites via proper numerical analysis would enhance the process of selecting the appropriate polymer and fiber types. It can contribute finding the proper reinforcement conditions to enhance the mechanical performance of the natural fiber composites to expand their reliable implementations in more industrial applications.


2018 ◽  
Vol 52 (24) ◽  
pp. 3289-3297 ◽  
Author(s):  
Benoît Cosson

Tracking the variability of natural fiber-based fabrics properties, such as local areal weight, fiber volume fraction, and therefore permeability, is crucial to optimize the parts processing of the bio-composites. This paper aims at developing a cost-effective and efficient optical method in order to predict the permeability of flax fabrics used in liquid composite molding processes. This method using an LCD monitor as light source and a reflex camera as a measurement device is based on light transmission measurement through fabric thickness. The raw data given by the camera are gray scale maps, transformed into areal weight maps. FEM software based on levelset method is finally used to highlight the influence of the local variability of the fiber volume fraction, and of the related fabrics porosity and permeability on the mold filling time. The proposed method can be directly implemented on the manufacturing line of the composites. It can be used to optimize, part-to-part, the resin consumption by predicting the resin flow through perform. Interestingly, this novel optical method is auto-calibrated and does not depend on picture resolution.


Author(s):  
Youssef K. Hamidi ◽  
Sudha Dharmavaram ◽  
Levent Aktas ◽  
M. Cengiz Altan

Effect of fiber volume fraction on occurrence, morphology, and spatial distribution of microvoids in resin transfer molded E-glass/epoxy composites is investigated. Three disk-shaped center-gated composite parts containing 8, 12, and 16 layers of randomly-oriented, E-glass fiber perform are molded, yielding 13.5%, 20.5%, and 27.5% fiber volume fractions. Voids are evaluated by microscopic image analysis of the samples obtained along the radius of these disk-shaped composites. The number of voids is found to decrease moderately with increasing fiber content. Void areal density decreased from 10.5 voids/mm2 to 9.5 voids/mm2 as fiber content is increased from 13.5% to 27.5%. Similarly, void volume fraction decreased from 3.1% to 2.5%. Increasing fiber volume fraction from 13.5% to 27.5% is found to lower the contribution of irregularly-shaped voids from 40% of total voids down to 22.4%. Along the radial direction, combined effects of void formation by mechanical entrapment and void mobility are shown to yield a spatially complex void distribution. However, increasing fiber content is observed to affect the void formation mechanisms as more voids are able to move toward the exit vents during molding. These findings are believed to be applicable not only to resin transfer molding but generally to liquid composite molding processes.


Author(s):  
M. Akif Yalcinkaya ◽  
Gorkem E. Guloglu ◽  
Maya Pishvar ◽  
Mehrad Amirkhosravi ◽  
E. Murat Sozer ◽  
...  

Vacuum-assisted resin transfer molding (VARTM) has several inherent shortcomings such as long mold filling times, low fiber volume fraction, and high void content in fabricated laminates. These problems in VARTM mainly arise from the limited compaction of the laminate and low resin pressure. Pressurized infusion (PI) molding introduced in this paper overcomes these disadvantages by (i) applying high compaction pressure on the laminate by an external pressure chamber placed on the mold and (ii) increasing the resin pressure by pressurizing the inlet resin reservoir. The effectiveness of PI molding was verified by fabricating composite laminates at various levels of chamber and inlet pressures and investigating the effect of these parameters on the fill time, fiber volume fraction, and void content. Furthermore, spatial distribution of voids was characterized by employing a unique method, which uses a flatbed scanner to capture the high-resolution planar scan of the fabricated laminates. The results revealed that PI molding reduced fill time by 45%, increased fiber volume fraction by 16%, reduced void content by 98%, improved short beam shear (SBS) strength by 14%, and yielded uniform spatial distribution of voids compared to those obtained by conventional VARTM.


Author(s):  
Jessica N. McClay ◽  
Peter Joyce ◽  
Andrew N. Smith

Measurements of the in-plane thermal conductivity and the directional dependence of Mitsubishi K63B12 pitch-fiber/Epoxy composite from Newport Composites are reported. This composite is being explored for use in the Avanced Seal Delivery System for effective thermal management. The thermal conductivity was measured using a steady state technique. The experimental results were then compared to a model of the thermal conductivity based on the direction of the fibers. These estimates are based on the properties of the constituent materials and volume of fibers in the sample. Therefore the density and the fiber volume fraction were experimentally measured. The thermal conductivity is clearly greatest in the direction of the fibers and decreases as the fibers are rotated off axis. In the case of pitch fiber composite materials, the contribution of the fibers to the thermal conductivity dominates. The experimental data clearly followed the correct trends; however, the measured values were 25% to 35% lower than predicted.


2019 ◽  
Vol 28 (4) ◽  
pp. 273-284
Author(s):  
Jai Inder Preet Singh ◽  
Sehijpal Singh ◽  
Vikas Dhawan

Rising environmental concerns and depletion of petrochemical resources have resulted in an increased interest in biodegradable natural fiber-reinforced polymer composites. In this research work, jute fiber has been used as a reinforcement and polylactic acid (PLA) as the matrix material to develop jute/PLA green composites with the help of compression molding technique. The effect of fiber volume fraction ranging from 25% to 50% and curing temperature ranging from 160°C to 180°C on different samples were investigated for mechanical properties and water absorption. Results obtained from various tests indicate that with an increase in the fiber volume fraction, tensile and flexural strength increases till 30% fiber fraction, thereafter decreases with further increase in fiber content. Maximum tensile and flexural strength of jute/PLA composites was obtained with 30% fiber volume fraction at 160°C curing temperature. The trend obtained from mechanical properties is further justified through the study of surface morphology using scanning electron microscopy.


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