Nanomechanical behaviour of ZrO2 dispersed sisal-based polymeric composites

2021 ◽  
pp. 146442072110160
Author(s):  
Bhabatosh Biswas ◽  
Biplab Hazra ◽  
Nillohit Mukherjee ◽  
Arijit Sinha
Keyword(s):  
Mechanical Properties ◽  
Wear Rate ◽  
Dynamic Mechanical Analysis ◽  
Unsaturated Polyester ◽  
Mechanical Analysis ◽  
Indentation Creep ◽  
Dynamic Mechanical ◽  
Recovery Index ◽  
Nanoindentation Technique ◽  
Reduced Modulus

Alkali-treated sisal fibre-incorporated silanized ZrO2 dispersed unsaturated polyester composites were fabricated with a filler loading of 5, 15, 25, 35, 45 wt%, respectively. The mechanical characterization of the composites was suitably executed at the sub-micron scale using the nanoindentation technique. Various mechanical properties were derived from the standard nanoindentation measurements namely, nanohardness, reduced modulus, recovery index, residual depth, wear rate and indentation creep, respectively. A marked improvement in the mechanical properties of the unsaturated polyester matrix due to the incorporation of the fillers (sisal and/or ZrO2) was observed through indentation-derived parameters namely, nanohardness (∼186%), reduced modulus (∼175%), recovery index (∼62%), wear rate (∼63%) and indentation creep (∼33%), respectively. A simulated dynamic mechanical analysis was performed using the sinus mode of the nanoindentation technique. A similar enhancement in the dynamic mechanical properties of the matrix was further observed through dynamic mechanical analysis as storage modulus (∼71%), loss modulus (∼60%), loss factor (∼150%) and specific damping coefficient (∼200%), respectively.

scholarly journals A pilot study of solvent-based cleaning of yellow ochre oil paint: effect on mechanical properties

2021 ◽  
Vol 9 (1) ◽  
Author(s):  
Ashley Amanda Freeman ◽  
Judith Lee ◽  
Cecil Krarup Andersen ◽  
Naoki Fujisawa ◽  
Michał Łukomski ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Pilot Study ◽  
Dynamic Mechanical Analysis ◽  
Mechanical Analysis ◽  
Deionized Water ◽  
Dynamic Mechanical ◽  
Yellow Ochre ◽  
Mineral Spirits ◽  
Paint Films

AbstractNanoindentation and dynamic mechanical analysis were used to measure changes in the surface and bulk mechanical properties of Winsor & Newton Yellow Ochre oil paint films following exposure to deionized water, aliphatic mineral spirits (Shellsol D40™), and D5 silicone solvent (decamethylcyclopentasiloxane). Yellow ochre paint films were exposed to the selected solvents by 24-h immersion, and sponge-cleaning. 24-h immersion in deionised water and Shellsol D40 caused measurable changes to bulk and surface mechanical properties. However, there were no measurable changes to the bulk or surface mechanical properties following sponge cleaning.

Univariate and Multivariate Gauge Repeatability and Reproducibility Analysis on the High Frequency Dynamic Mechanical Analysis (DMA) Measurement System

2019 ◽  
Author(s):  
Roja Esmaeeli ◽  
Haniph Aliniagerdroudbari ◽  
Seyed Reza Hashemi ◽  
Hammad Al-Shammari ◽  
Muapper Alhadri ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Dynamic Mechanical Analysis ◽  
Analysis Of Variance ◽  
Measurement System ◽  
High Frequency ◽  
Mechanical Analysis ◽  
Viscoelastic Materials ◽  
High Frequencies ◽  
Dynamic Mechanical ◽  
Repeatability And Reproducibility

Abstract The quality of the collected data from a measurement system affects eventual decision making process. Therefore, the reliability of any measurement system is an important factor to be studied. Gauge repeatability and reproducibility (Gauge R&R) is the standard method to evaluate the measurement system and assess the adequacy of variation in the measurement data. Gauge R&R is a statistical tool which evaluates two main characteristics of the measurement system: repeatability and reproducibility. The Dynamic Mechanical Analysis (DMA) is a common measurement system for studying the dynamic mechanical properties of viscoelastic materials such as polymers. The newly developed High Frequency Dynamic Mechanical Analysis (HFDMA) is able to directly run the simple shear test at high frequencies without changing the specimen temperature. The complex shear modulus and damping factor of the viscoelastic materials are reported by the HFDMA system. In this study the uni-variable Gauge R&R study based on Analysis of Variance (ANOVA) is done on each measured characteristic of the HFDMA measurement system. The source of variations for each characteristic is distinguished. Then the multivariate Gauge R&R based on the Multivariate Analysis of Variance (MANOVA) is done and the percentage of multivariate Gauge R&R for the measurement with the multiple variables is reported. The results indicate that the HFDMA measurements are both repeatable and reproducible. Thus, the new HFDMA can be used as a measurement system to measure the mechanical properties of viscoelastic materials at high frequencies.

Mechanical Properties of Coil Coating Evaluated with Dynamic Mechanical Analysis in Daul Cantilever

2007 ◽  
Vol 353-358 ◽  
pp. 1729-1732 ◽  
Author(s):  
Lei Chen ◽  
Hong Liang Pan
Keyword(s):  
Mechanical Properties ◽  
Dynamic Mechanical Analysis ◽  
Loss Modulus ◽  
Paint Layer ◽  
Mechanical Analysis ◽  
Curing Temperature ◽  
Mode Analysis ◽  
Dynamic Mechanical ◽  
Preparation Conditions ◽  
Coil Coating

The storage modulus, loss modulus, loss tangent (tanδ), stress and strain have been determined for painted steel specimens by dynamic mechanical analysis (DMA) operated in Dual Cantilever mode. Analysis of the composite system enabled the elastic modulus of the paint layer to be calculated and the result can be useful to analyze the mechanical properties of the coil coating. The calculation was found to be very sensitive to the geometry (especially thickness of the substrate and coating) and properties of the substrate and coating, leading to considerable variability in the calculated coating modulus. The DMA method was successful in detecting the glass transition temperature (Tg) as a peak in the tanδ curve. The value of Tg is sensitive to the preparation conditions (e.g. curing temperature) and composition of the paint. The results show that DMA in Dual Cantilever can be useful as a characterization tool for painted steel.

Dynamic Mechanical Properties of Radial Curtain Plybamboo

2014 ◽  
Vol 488-489 ◽  
pp. 289-292
Author(s):  
Chun Gui Du ◽  
Zhe Wang ◽  
Ren Li ◽  
Ming Zhao ◽  
Chun De Jin
Keyword(s):  
Mechanical Properties ◽  
Dynamic Mechanical Analysis ◽  
Dynamic Mechanical Properties ◽  
Mechanical Analysis ◽  
Experimental Temperature ◽  
Dynamic Mechanical

Dynamic mechanical properties of radial curtain plybamboo and its constitution unit-radial bamboo strip were studied using dynamic mechanical analysis (DMA). The results showed: experimental temperature had great effect on dynamic mechanical properties, the shape and alignment of radial bamboo strips were closely related the dynamic mechanical properties of radial curtain plybamboo.

Dynamic Mechanical Analysis of ABS From Hybrid Additive Manufacturing by Fused Filament Fabrication and Shot Peening

2020 ◽  
Author(s):  
Haitham Hadidi ◽  
Brady Mailand ◽  
Tayler Sundermann ◽  
Ethan Johnson ◽  
Rakeshkumar Karunakaran ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Additive Manufacturing ◽  
Dynamic Mechanical Analysis ◽  
Shot Peening ◽  
Extrusion Process ◽  
Dynamic Mechanical Properties ◽  
Mechanical Analysis ◽  
Layer By Layer ◽  
Fused Filament Fabrication ◽  
Dynamic Mechanical

Abstract The mechanical properties of 3D printed polymers parts are process parameter dependent. Defects such as inadvertent voids between deposited rasters and layers lead to weakness in produced parts, which results in inferior mechanical properties as compared to injection molding. An alternative method to change energy absorption and stiffness of a polymer is hybrid additive manufacturing (AM). Hybrid-AM is the use of additive manufacturing with one or more secondary processes that are fully coupled and synergistically affect part quality, functionality, and/or process performance. In this study, fused filament fabrication (FFF) was coupled with layer-by-layer shot peening to study the dynamic mechanical properties of ABS 430 polymer using dynamic mechanical analysis (DMA). FFF is a heated extrusion process. Shot peening is a mechanical surface treatment that impinges a target with a stochastically dispersed, high velocity stream of beads. Compressive residual stress was imparted to preferential layer intervals during printing to modify the elasticity (stiffness), viscosity, toughness, and glass transition temperature. Viscoelastic and dynamic mechanical properties are important to the performance of polymers in automotive, aerospace, electronics, and medical components. Coupling printing and peening increased the storage and loss moduli as well as the tangent delta. DMA results suggest that preferential layer sequences exist that possess higher elasticity and better absorb energy upon sinusoidal dynamic loading.

Influence of Diisocyanates on Dynamic Mechanical Properties of Castable Polyurethane Elastomers

2012 ◽  
Vol 217-219 ◽  
pp. 563-566
Author(s):  
Xiao Dong Chen ◽  
Yu Hua Yi
Keyword(s):  
Mechanical Properties ◽  
Dynamic Mechanical Analysis ◽  
Dynamic Mechanical Properties ◽  
Mechanical Analysis ◽  
Toluene Diisocyanate ◽  
Diphenylmethane Diisocyanate ◽  
Analysis Method ◽  
Polyurethane Elastomers ◽  
Dynamic Mechanical ◽  
Soft Segments

A series of castable polyurethane elastomers, based on polytetramethylene glycol as soft segments and toluene diisocyanate, 4, 4’-diphenylmethane diisocyanate, P-phenylene diisocyanate as diisocyanates respectively, were synthesized. The dynamic mechanical analysis method was utilized to determine tan delta property (tanδ). Also the influence of diisocyanates on the dynamic mechanical properties of castable polyurethane elastomers was analyzed. It can be concluded that the P-phenylene diisocyanate system elastomers have the most excellent dynamic mechanical properties.

Sign in / Sign up

Export Citation Format

Share Document